Acta Cryst. (2011). E67, m482  [ doi:10.1107/S1600536811010385 ]

[N'-(3,5-Diiodo-2-oxidobenzylidene-O)-4-methylbenzohydrazidato-²N',O](methanol-O)(methanolato-O)oxidovanadium(V)

L. Liu

Online 26 March 2011

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.008 Å
• R factor = 0.041
• wR factor = 0.090
• Data-to-parameter ratio = 17.1

checkCIF/PLATON results

No syntax errors found




Alert level C
SHFSU01_ALERT_2_C  Test not performed. _refine_ls_shift/su_max and
            _refine_ls_shift/esd_max not present.
            Absolute value of the parameter shift to su ratio given   0.001
PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low .......       0.97      
PLAT125_ALERT_4_C No '_symmetry_space_group_name_Hall' Given .....          ?
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          1      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         74      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         38      

Alert level G
PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite          2      
PLAT794_ALERT_5_G Note: Tentative Bond Valency for V1      (IV)          4.96      
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          1      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   6 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   3 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   4 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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