Acta Cryst. (2012). E68, m47-m48  [ doi:10.1107/S1600536811051658 ]

trans-Bis(ethylenediamine-²N,N')bis(6-methyl-2,2,4-trioxo-3,4-dihydro-1,2⁶,3-oxathiazin-3-ido-N)copper(II)

N. Dege, G. Demirtas and H. Içbudak

Online 14 December 2011

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (C-C) = 0.003 Å
• R factor = 0.024
• wR factor = 0.065
• Data-to-parameter ratio = 13.5

checkCIF/PLATON results

No syntax errors found




Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?
PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size ....       0.75 mm   
PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X)  Cu1    --  N2      ..        6.6 su   
PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X)  Cu1    --  N3      ..        6.6 su   

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   0 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   4 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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