Acta Cryst. (2012). E68, m68  [ doi:10.1107/S1600536811053864 ]

cis-Bis(acetonitrile-N)bis(2,2'-bipyridine-²N,N')ruthenium(II) tetrafluoridoborate

Y. Wang, F. Xu and W. Huang

Online 21 December 2011

Key indicators

• Single-crystal X-ray study
• T = 291 K
• Mean (C-C) = 0.007 Å
• R factor = 0.046
• wR factor = 0.121
• Data-to-parameter ratio = 12.6

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of          B1     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of          B2     
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          1      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.595          2      

Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ....          ?
PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still          47 Perc.
PLAT961_ALERT_5_G Dataset Contains no Negative Intensities .......          !

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   4 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   3 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   2 ALERT type 5 Informative message, check

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