[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1218-m1219
[ doi:10.1107/S1600536812036264 ]

Bis[(cyanido-[kappa]C)bis(1,10-phenanthroline-[kappa]2N,N')copper(II)] pentakis(cyanido-[kappa]C)nitrosoferrate(II) dimethylformamide monosolvate

O. V. Kozachuk, V. N. Kokozay, O. Y. Vassilyeva and B. W. Skelton


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.3 PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -1.839 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 6
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 9 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 6 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 6.06 PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Fe1 -- C28 .. 5.3 su PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 25 Perc. PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 Perc. PLAT794_ALERT_5_G Note: Tentative Bond Valency for Cu1 (II) 2.22 PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 44 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 31
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 11 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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