[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1547
[ doi:10.1107/S1600536812045898 ]

Bis[[mu]-(E)-N-(pyridin-3-ylmethylidene)hydroxyamine]-[kappa]2N1:N3;[kappa]2N3:N1-bis{[(E)-N-(pyridin-3-ylmethylidene-[kappa]N)hydroxyamine]silver(I)} dinitrate

S. Gao and S. W. Ng


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT094_ALERT_2_B Ratio of Maximum / Minimum Residual Density .... 5.10
Alert level C PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of N5 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 3 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 6 PLAT973_ALERT_2_C Large Calcd. Positive Residual Density on Ag1 1.03 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 0.76A from N4 . 0.44 eA-3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 2 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- N2_a .. 9.6 su PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 35
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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