[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1540-m1541
[ doi:10.1107/S1600536812046090 ]

Poly[[[[mu]3-(E)-N-(pyridin-4-ylmethylidene)hydroxylaminato-[kappa]3O:N:N'][[mu]2-(E)-N-(pyridin-4-ylmethylidene)hydroxylamine-[kappa]2N:N'][(E)-N-(pyridin-4-ylmethylidene-[kappa]N)hydroxylamine]disilver(I)] nitrate]

S. Gao and S. W. Ng


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for Ag1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for O1 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 4.483 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 6 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 8 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 2 PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 2 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- O1 .. 15.2 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag2 -- O1_d .. 7.1 su PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of N7 PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of N7' PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 Perc. PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 2 N0.50 O1.50 PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 3 N0.50 O1.50 PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 26 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 15
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 17 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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