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[Contents scheme]

Acta Cryst. (2012). E68, m1440-m1441
[ doi:10.1107/S1600536812043760 ]

catena-Poly[[[diaqua(1,10-phenanthroline-[kappa]2N,N')cobalt(II)]-[mu]-1H-benzimidazole-5,6-dicarboxylato-[kappa]2N3:O6] sesquihydrate}

D.-B. Xu, Y. Fang, D.-L. Jiang, Y. Zhu and M. Chen

Key indicators

checkCIF/PLATON results

No syntax errors found

Alert level A DIFF019_ALERT_1_A _diffrn_standards_number is missing Number of standards used in measurement. DIFF020_ALERT_1_A _diffrn_standards_interval_count and _diffrn_standards_interval_time are missing. Number of measurements between standards or time (min) between standards. DIFF022_ALERT_1_A _diffrn_standards_decay_% is missing Percentage decrease in standards intensity.
Alert level C PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ ? PLAT417_ALERT_2_C Short Inter D-H..H-D H1A .. H1D .. 2.14 Ang. PLAT417_ALERT_2_C Short Inter D-H..H-D H2D .. H4C .. 2.13 Ang. PLAT976_ALERT_2_C Negative Residual Density at 0.42A from OW3 . -0.44 eA-3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 12 PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 1 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF .... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 9 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT045_ALERT_1_G Calculated and Reported Z Differ by ............ 0.50 Ratio PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Co1 -- OW2 .. 8.8 su PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 33 Perc. PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 4 PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 3 H O0.50 PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 12 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 4
3 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 12 ALERT level G = General information/check it is not something unexpected 6 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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