[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m167
[ doi:10.1107/S1600536813004674 ]

Bis[(E)-3-(4-methoxyphenyl)prop-2-enoato]triphenylantimony(V) benzene monosolvate

P. V. Andreev, N. V. Somov, O. S. Kalistratova, A. V. Gushchin and E. V. Chuprunov


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B Crystal system given = triclinic PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 18
Alert level C PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.5 Ratio PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C7B PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 39 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 6 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 12 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00100 Deg. PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C1F PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C4F PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C1G PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 Perc. PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 8 PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 78 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 4
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 13 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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