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Acta Cryst. (2013). E69, m448-m449  [ doi:10.1107/S1600536813018485 ]

(2,2'-Bipyridine-[kappa]2N,N')tetrakis(dimethyl sulfoxide-[kappa]O)copper(II) bis(perchlorate)

T. Iskenderov


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Alert level C PLAT202_ALERT_3_C Isotropic non-H Atoms in Anion/Solvent ......... 4 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 56.543 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 10.119 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.909 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.174 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 8 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2 PLAT975_ALERT_2_C Positive Residual Density at 0.69A from O1 . 0.55 eA-3 PLAT976_ALERT_2_C Negative Residual Density at 0.84A from O6 . -0.44 eA-3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 10 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT128_ALERT_4_G Note: Alternate Setting of Space-group P21/c . P21/n PLAT180_ALERT_4_G Check Cell Rounding: # of Values Ending with 0 = 3 PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of Cl2_1 PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of Cl2_2 PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 50 % PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 7 O4 -CU1 -O1 -S1 58.20 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 11 N2 -CU1 -O2 -S2 131.60 1.10 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 19 N1 -CU1 -O3 -S3 166.90 0.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 28 O1 -CU1 -O4 -S4 -166.60 0.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 30 O3 -CU1 -N1 -C1 154.50 0.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 35 O3 -CU1 -N1 -C9 -23.70 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 39 O2 -CU1 -N2 -C8 18.00 0.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 44 O2 -CU1 -N2 -C10 -3.60 1.20 1.555 1.555 1.555 1.555 PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 10 PLAT794_ALERT_5_G Note: Tentative Bond Valency for Cu1 (II) 2.22 PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 10 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 2092
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 19 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 8 ALERT type 3 Indicator that the structure quality may be low 15 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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