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Acta Cryst. (2013). E69, m460-m461  [ doi:10.1107/S1600536813019077 ]

(Methanol-[kappa]O)-cis-dioxido{(4Z,N'E)-N'-[(Z)-4-oxido-4-phenylbut-3-en-2-ylidene]isonicotinohydrazidato}molybdenum(VI)

S. K. Kurapati


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Alert level C PLAT480_ALERT_4_C Long H...A H-Bond Reported H1C .. O2 .. 2.63 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H8 .. O1 .. 2.69 Ang. PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 2 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT128_ALERT_4_G Note: Alternate Setting of Space-group P21/c . P21/n PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Mo1 -- N1 .. 5.6 su PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 13 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 5
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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