[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m527
[ doi:10.1107/S1600536813024288 ]

Tricarbonylchlorido(6',7'-dihydro-5'H-spiro[cyclohexane-1,6'-dipyrido[3,2-d:2',3'-f][1,3]diazepine]-[kappa]2N1,N11)rhenium(I)

O. R. Clegg, L. P. Harding, J. W. Miller and C. R. Rice


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.387 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 4 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Re1 -- C1 .. 7.3 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Re1 -- C2 .. 5.8 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Re1 -- C3 .. 5.7 su PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 2
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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