[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m570-m571
[ doi:10.1107/S1600536813026056 ]

catena-Poly[2,2',2''-nitrilo­tris­(ethan­aminium) [tri-[mu]-oxido-tris­[dioxido­vanadate(V)]] monohydrate]

K. B. Chang, M. D. Smith, M. Zeller and A. J. Norquist


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.12 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O7 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for V1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for V2 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for V3 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 8
Alert level G PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 1 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 11 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? Check PLAT809_ALERT_1_G Can not Parse the SHELXL Weighting Scheme String ! Check PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 89 PLAT929_ALERT_5_G No Weight Pars,Obs and Calc R1,wR2,S not checked ! Info PLAT960_ALERT_3_G Number of Intensities with I < - 2*sig(I) ... 7
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 4 ALERT type 5 Informative message, check

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