[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m607
[ doi:10.1107/S1600536813028195 ]

[1,1'-Bis(di­phenyl­phosphan­yl)cobalto­cenium-[kappa]2P,P']([eta]5-cyclo­penta­dien­yl){2-[4-(4-ethynylphen­yl)phen­yl]ethynyl-[kappa]C}ruthenium(II) hexa­fluorido­phosphate

L.-Z. Zeng, Y.-Y. Wu, G.-X. Tian and Z. Li


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C RINTA01_ALERT_3_C The value of Rint is greater than 0.12 Rint given 0.124 PLAT230_ALERT_2_C Hirshfeld Test Diff for C14 -- C15 .. 5.4 su PLAT242_ALERT_2_C Low Ueq as Compared to Neighbors for ..... Ru1 Check PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.1 Note PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 11.082 Check PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.258 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 5
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of P3 Check PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C41 - C42 ... 1.42 Ang. PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C53 - C54 ... 1.42 Ang. PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 147 PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... Please Check
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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