[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m575-m576
[ doi:10.1107/S1600536813026585 ]

Bis[[mu]-N-(pyridin-2-ylmeth­yl)pyridin-3-amine-[kappa]2N:N']disilver(I) bis­(perchlorate) dimethyl sulfoxide disolvate

S.-H. Moon and K.-M. Park

Key indicators

checkCIF/PLATON results

No syntax errors found

Alert level C PLAT717_ALERT_1_C D...A Unknown or Inconsistent Label .......... <I>CG</ PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.796 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 6 PLAT975_ALERT_2_C Positive Residual Density at 1.04A from N3 . 0.47 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 0.95A from O3 . 0.41 eA-3 PLAT976_ALERT_2_C Negative Residual Density at 0.90A from N3 . -0.49 eA-3 PLAT976_ALERT_2_C Negative Residual Density at 0.72A from O3 . -0.46 eA-3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 1 Why ? PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ Please Check PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of Cl1 Check PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 5
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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