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[Contents scheme]

Acta Cryst. (2013). E69, m581-m582
[ doi:10.1107/S1600536813026901 ]

Tris(cyclo­hexyl­ammonium) cis-di­chlorido­bis­(oxalato-[kappa]2O1,O2)stann­ate(IV) chloride monohydrate

M. Sarr, W. Diallo, A. Diasse-Sarr, L. Plasseraud and H. Cattey


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT243_ALERT_4_C High 'Solvent' Ueq as Compared to Neighbors of C21 Check PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.7 Note PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 5.887 Check PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 9 Why ? PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 34 PLAT975_ALERT_2_C Positive Residual Density at 0.86A from O6 . 0.49 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 0.98A from O3 . 0.44 eA-3 PLAT976_ALERT_2_C Negative Residual Density at 1.08A from O9 . -0.51 eA-3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT007_ALERT_5_G Number of Unrefined Donor-H Atoms .............. 11 Why ? PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ Please Check PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 39.76 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 45
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 8 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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