view article
Figure 3
A section of the final observed and calculated plot for the Pawley fit to all five data sets (Rwp = 5.04): 90 K = blue, 120 K = black, 150 K = green, 180 K = pink, 210 K = orange. Note in particular the tickmarks at (i) ∼16.1°, showing reflections 022 and 121 split at 90 K, completely overlapping by 180 K and crossed-over at 210 K; and (ii) ∼17.3°, showing reflections 11[\bar 2] and 0[\bar 2]1 splitting as the temperature is increased from 90 to 210 K.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 41| Part 6| October 2008| Pages 1089-1094
doi:10.1107/S0021889808030872
Follow J. Appl. Cryst.
Sign up for e-alerts
E-alerts
Follow J. Appl. Cryst. on Twitter
Twitter
Follow us on facebook
Facebook
Sign up for RSS feeds
RSS