Figure 7
Portions of co-refined diffractograms of sample S3 taken from (a) XRD and (b) HRPD. Numbers in brackets indicate the (hkl) indices of the cubic phase to provide comparisons with those of single-phase samples. The letters `c' following the brackets indicate that the reflection belongs to the cubic crystal system only. Upper (lower) reflection markers belong to the cubic (tetragonal) phase. Plus signs (solid lines) indicate the raw data (the fit to the data). The solid lines below the reflection markers signify the difference between the data and the fit. See Table 4 for the refined parameters of interest. |