Real-time synchrotron powder X-ray diffraction study of the antisite defect formation during sub- and supercritical synthesis of LiFePO4 and LiFe1−xMnxPO4 nanoparticles

Jensen, K.; Christensen, M.; Tyrsted, C.; Brummerstedt Iversen, B.

doi:10.1107/S0021889811006522

Journal of Applied Crystallography Journal of Applied
Crystallography

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Figure 3
Time for the formation of LiFePO₄ as a function of synthesis temperature. Squares show data for LiFePO₄ precursor A, circles for LiFePO₄ precursor B, triangles for both LiFe_0.75Mn_0.25PO₄ and LiFe_0.50Mn_0.50PO₄, and stars for LiFe_0.25Mn_0.75PO₄. The lines are guides to the eye. Note the broken y axis for the lowest-temperature data point.

JOURNAL OF
APPLIED
CRYSTALLOGRAPHY

ISSN: 1600-5767

Volume 44| Part 2| March 2011| Pages 287-294

doi:10.1107/S0021889811006522

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