Real-time synchrotron powder X-ray diffraction study of the antisite defect formation during sub- and supercritical synthesis of LiFePO4 and LiFe1−xMnxPO4 nanoparticles

Jensen, K.; Christensen, M.; Tyrsted, C.; Brummerstedt Iversen, B.

doi:10.1107/S0021889811006522

Journal of Applied Crystallography Journal of Applied
Crystallography

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Figure 7
Occupancy of Fe/Mn on the Li site for (a) LiFe_0.75Mn_0.25PO₄, (b) LiFe_0.50Mn_0.50PO₄ and (c) LiFe_0.25Mn_0.75PO₄. Circles show data for 443 K, squares for 543 K, triangles for 618 K and stars for 653 K. For clarity, only every third data point is shown.

JOURNAL OF
APPLIED
CRYSTALLOGRAPHY

ISSN: 1600-5767

Volume 44| Part 2| March 2011| Pages 287-294

doi:10.1107/S0021889811006522

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