Figure 4
Two-dimensional slices of the reconstructed reciprocal lattice obtained from the 3D-RED data. (a) (hk0), (b) (h0l) and (c) (0kl). Each slice contains all unique reflections (i.e. one complete quadrant) for orthorhombic compounds. The missing reflections are a result of the missing cone. Every second layer (shown in red) in (b) and (c) corresponds to c = 8.2 Å, and these layers are much weaker than the even layers of c = 4.1 Å. |