(IUCr) Acta Crystallographica Section B Volume 38, Part 2, February 1982

Acta Cryst. (1982). B38, 351-355
https://doi.org/10.1107/S0567740882002957

Rutile-type compounds. VI. Refinement of VF₂ and computer simulation of V:MgF₂

W. H. Baur, S. Guggenheim and J.-C. Lin

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Structure du décachlorure de tricadmium et de dicalcium octadecahydraté, 2[Ca(H₂O)₈].[Cd₃Cl₁₀]_∞.2H₂O

H. Leligny and J. C. Monier

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Structure of potassium diaquatricuprooctadecatungstodiarsenate(III)(12–) undecahydrate

F. Robert, M. Leyrie and G. Hervé

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Neutron powder diffraction study of two sodium platinum oxides: Na_1.0Pt₃O₄ and Na_0.73Pt₃O₄

K. B. Schwartz, C. T. Prewitt, R. D. Shannon, L. M. Corliss, J. M. Hastings and B. L. Chamberland

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Compounds with perovskite-type slabs. V. A high-temperature modification of La₂Ti₂O₇

N. Ishizawa, F. Marumo, S. Iwai, M. Kimura and T. Kawamura

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Structure du polytype rhomboédrique 3R du sulfure double de fer et de gallium Fe₂Ga₂S₅

L. Dogguy-Smiri and Nguyen-Huy Dung

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The garnet-like cyanide framework of ammonium ferrocyanide hydrate with a channel system for ionic conductivity

E. Hellner and E. Koch

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Structure cristalline d'un oxysulfure isotype de la mélilite, La_3,33Ga₆O₂S₁₂

A. Mazurier, M. Guittard and S. Jaulmes

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Barium thiocyanate trihydrate

K. Mereiter and A. Preisinger

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Structure and high-pressure polymorphism of strontium metasilicate

K.-I. Machida, G.-Y. Adachi, J. Shiokawa, M. Shimada and M. Koizumi

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The Si₅O₁₆ pentamer in zunyite refined and empirical relations for individual silicon–oxygen bonds

W. H. Baur and T. Ohta

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Hydrogen bonds in Na₃AsS₄.8D₂O: neutron diffraction, X-ray diffraction and vibrational spectroscopic studies

K. Mereiter, A. Preisinger, O. Baumgartner, G. Heger, W. Mikenda and H. Steidl

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The electronic factors linking the structures of graphite, arsenic and selenium

J. K. Burdett and J.-H. Lin

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Clathrate inclusion compounds of bis(isothiocyanato)tetrakis(4-methylpyridine)nickel(II). III. Bis(isothiocyanato)tetrakis(4-methylpyridine)nickel(II)–1-methylnaphthalene (1:2)

J. Lipkowski, P. Sgarabotto and G. D. Andreetti

CCDC reference: 1180261

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Orthorhombic and monoclinic allotropes of cis-[PtCl₂(PMePh₂)₂], cis-dichlorobis(methyldiphenylphosphine)platinum(II): structure analyses

K.-C. Ho, G. M. McLaughlin, M. McPartlin and G. B. Robertson

CCDC references: 1107024; 1107025

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The structure of trans-dibromooxo(N-phenylsalicylideneiminato)(triphenylphosphine)rhenium(V)

V. Bertolasi, M. Sacerdoti, G. Gilli and U. Mazzi

CCDC reference: 1105919

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The structure of (2-dimethylaminoethanolato)(trifluoroacetato)copper(II) tetramer

M. Ahlgrén, U. Turpeinen and R. Hämäläinen

CCDC reference: 1113086

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Structure of the copper(II) complex of 1,4,10,13-tetraoxa-7,16-diazacyclooctadecane-7,16-diacetic acid

T. Uechi, I. Ueda, M. Tazaki, M. Takagi and K. Ueno

CCDC reference: 1106969

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The structures of [Ni(C₁₄H₃₂N₆)(NCS)₂].H₂O and [Ni(C₁₄H₃₂N₆)(NO₂)]ClO₄. Conformation and configuration in a tetradentate bis-hydrazone ligand

A. R. Davis, F. W. B. Einstein and A. C. Willis

CCDC references: 1107064; 1107065

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The structures of [Ni(C₁₈H₃₄N₆)](ClO₄)₂ and [{Ni(C₁₈H₃₄N₆)}₂(C₂O₄)](ClO₄)₂.2H₂O. Complexes of a [16]tetraene N₄(N₂) macrocycle produced by a Schiff-base-type condensation

A. R. Davis, F. W. B. Einstein and A. C. Willis

CCDC references: 1107067; 1107068

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Crystal structures of complexes between alkali-metal salts and cyclic polyethers. 12. The complex between sodium bromide and 2,3-dimethoxybenzo-15-crown-5 {bromo(2,3-dimethoxy-6,7,9,10,12,13,15,16-octahydrobenzo[1,4,7,10,13]pentaoxacyclopentadecene)sodium}

I. R. Hanson, D. G. Parsons and M. R. Truter

CCDC reference: 1106978

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Structure of tris(2-picolylamine)zinc(II) dichloride–ethanol, [Zn (α-pic)₃]Cl₂.EtOH; a complex related to an Fe^II spin crossover complex

M. Mikami-Kido and Y. Saito

CCDC reference: 1106974

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The structures of mono- and bis-arene tungsten derivatives: (I) bis(η⁶-toluene)tungsten, (II) hydridobis(η⁶-toluene)tungsten hexafluorophosphate, (III) hydridobis(η⁶-monofluorobenzene)tungsten hexafluorophosphate, (IV) dichlorohydrido(η⁶-toluene)bis(trimethylphosphine)tungsten hexafluorophosphate, (V) bis(acetonitrile)(η³-allyl)(η⁶-toluene)tungsten hexafluorophosphate

K. Prout, A. Gourdon, C. Couldwell, B. Meunier, FangMing Miao and J. Woolcock

CCDC references: 1107009; 1107010; 1107011; 1107013; 1107015

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Pentameric methylzinc tert-butylsulphide

G. W. Adamson, N. A. Bell and H. M. M. Shearer

CCDC reference: 1215521

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Virgidivarine, a sparteine-type alkaloid

A. J. de Kok, C. Romers and J. L. van Eijk

CCDC reference: 1107006

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1-Benzyl-2-[(hydroxyimino)methyl]pyridinium bromide and 1-benzyl-2-[(hydroxyimino)methyl]pyridinium methylsulphonate

W. Van Havere, A. T. H. Lenstra, H. J. Geise, G. R. Van den Berg and H. P. Benschop

CCDC references: 1107055; 1107059

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Discussion of an order–disorder behaviour near T_c in the chloranil displacive transition

J. L. Baudour and J. Meinnel

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An acetoxy lactam acid from 4-amino-4-deoxymethyleneanhydrolycoctonam

M. Cygler, M. Przybylska and O. E. Edwards

CCDC reference: 1107625

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The structure of anthracene-d₁₀ at 16 K using neutron diffraction

S. L. Chaplot, N. Lehner and G. S. Pawley

CCDC reference: 1103076

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The polymorphs of 2,2'-dinitroxydiethylnitramine (DINA). The structure of DINA (II)

A. Wilkins and R. W. H. Small

CCDC reference: 1225218

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6,9-Dimethoxy-2,13-diaza[4]paracyclo[4](3,5)-pyridinophane-1,14-dione, C₁₉H₂₁N₃O₄, and 19-benzyl-16,19-dihydro-2,13-diaza[4]paracyclo[4](3,5)pyridinophane-1,14-dione, C₂₄H₂₅N₃O₂

A. M. van Herk, K. Goubitz, A. R. Overbeek and C. H. Stam

CCDC references: 1106972; 1106973

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Stereochemistry of a complex diindenopyradione

J. L. Flippen-Anderson and F. D. Mills

CCDC reference: 1180385

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The structure of S,S'-methylenebis(L-cysteine) monohydrochloride

F. Bigoli, M. Lanfranchi, E. Leporati, M. Nardelli and M. A. Pellinghelli

CCDC reference: 1107034

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Structures of E,E-3-(p-tolylimino)-2-butanone oxime and E,Z-4-(p-tolylimino)-2,3-pentanedione 3-oxime. An X-ray crystallographic investigation on bonding in oximes

V. Bertolasi, G. Gilli and A. C. Veronese

CCDC references: 1107021; 1107022

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Dihydroelephantopin, C₁₉H₂₂O₇

W. H. Watson, V. Zabel, T. J. Mabry and G. Yabuta

CCDC reference: 1139977

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Structure of a 1:2 sandwich complex of proflavine and adenosine with an unusual puckering disorder and a site shared by sulfate and water molecules

P. Swaminathan, E. Westhof and M. Sundaralingam

CCDC reference: 1101349

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The structure of a hydrated 1:2 complex of adenylyl(3'-5')adenosine–proflavine hemisulphate

H.-S. Shieh, H. M. Berman, S. Neidle, G. Taylor and M. Sanderson

CCDC reference: 1101343

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Conformational analysis of synthetic androgens. VI. Structure and crystal packing of 17β-hydroxy-7β-methyl-4,14-androstadien-3-one monohydrate

W. L. Duax, D. C. Rohrer and A. Segaloff

CCDC reference: 1107450

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The structure of 1,5-bis(2,6-dimethylphenyl)-3-nitroformazan

E. Dijkstra, A. T. Hutton, H. M. N. H. Irving and L. R. Nassimbeni

CCDC reference: 1105951

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The structures of five bicyclic lactams: 2-benzyl-3-oxo-2-azabicyclo[2.2.1]hept-6-exo-yl p-toluenesulfonate, 2-benzyl-6-exo-phenoxy-2-azabicyclo[2.2.1]heptan-3-one, 2-benzyl-6-exo-(2-iodo-4-methylphenoxy)-2-azabicyclo[2.2.1]heptan-3-one, 2-benzyl-6-exo-(2,6-diiodo-4-methylphenoxy)-2-azabicyclo[2.2.1]heptan-3-one and 2-benzyl-6-exo-phenoxy-2-azabicyclo[2.2.2]octan-3-one

H. L. Ammon, P. H. Mazzocchi, L. Liu, E. C. Colicelli, R. Doherty and J. M. Stewart

CCDC references: 1107079; 1107080; 1107081; 1107082; 1113304

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Antischistosomal analogs of hycanthone. II. Structure of 2-[2-(diethylamino)ethyl]-2H-[1]benzothiopyrano[4,3,2-cd]indazole-5-methanol monohydrate

C. H. Wei

CCDC reference: 1147819

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Intramolecular hydrogen bonding in 2,2',4,4'-tetrahydroxybenzophenone

E. O. Schlemper

CCDC reference: 1104903

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The structures of 1,8-dimorpholinonaphthalene and 1,8-dipiperidinonaphthalene

W. Wong-Ng, S. C. Nyburg, A. Awwal, R. Jankie and A. J. Kresge

CCDC references: 1107552; 1107554

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The structure of a dinucleoside monophosphate having a high-anti conformation: 8,2'-S-cyclo-2'-thioadenylyl(3'-5')-8,2'-S-cyclo-2'-thioadenosine (A^spA^s) hydrochloride

S. Fujii, K. Hamada, R. Miura, S. Uesugi, M. Ikehara and K.-I. Tomita

CCDC reference: 1114291

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X-ray structure and crystal packing analysis of triphenylchloromethane

A. Dunand and R. Gerdil

CCDC reference: 1320995

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The structure of 9-[3-(3-indolyl)-propyl]adenine. A model for protein/nucleic acid interactions

G. Bunick and D. Voet

CCDC reference: 1180458

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Structure of (13αH,14βH)-jeunicin

A. J. Weinheimer, J. A. Matson, M. Poling and D. van der Helm

CCDC reference: 1107739

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Plucheinol and (3αH)-plucheinol

V. Zabel, W. H. Watson and M. Silva

CCDC references: 1107053; 1235197

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Salignone-A and salignone-H, two diterpene dilactones

W. H. Watson, V. Zabel, M. Silva and M. Bittner

CCDC references: 1107062; 1202287

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Calzirtite – a fluorite-related superstructure

H. J. Rossell

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Structure d'un trimétaphosphate–tellurate de rubidium monohydraté: Te(OH)₆.Rb₃P₃O₉.H₂O

N. Boudjada and A. Durif

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Structure refinement of Ni₃Sn₄

W. Jeitschko and B. Jaberg

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Structure of trirubidium heptabromodimanganate

J. Goodyear, E. M. Ali and H. H. Sutherland

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Cation-site location in a natural chabazite

M. Calligaris, G. Nardin, L. Randaccio and P. C. Chiaramonti

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Palladium metaborate

W. Depmeier and H. Schmid

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Bis(isothiocyanato)tetrakis(4-methylpyridine)nickel(II)–o-xylene (1:2)

J. Lipkowski and G. D. Andreetti

CCDC reference: 1179559

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Structure of nickel uranyl acetate hexahydrate

A. Zalkin, H. Ruben and D. H. Templeton

CCDC reference: 1107026

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catena-μ-Acetato-N,N'-ethylenebis[(2-hydroxy-1-naphthyl)methaniminato]manganese(III)

F. Akhtar and M. G. B. Drew

CCDC reference: 1106977

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Bis(di-n-propyldithiophosphinato)zinc(II)

H. Wunderlich

CCDC reference: 1107447

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Structure of phenyltellurium trichloride

F. W. B. Einstein and T. Jones

CCDC reference: 1226166

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μ-{1,4-Bis[(2-pyridyl)amino]phthalazine-N¹,N³,N⁴,N⁶}-μ-chloro-dichloro-μ-hydroxo-dicopper(II) sesquihydrate

G. Marongiu and E. C. Lingafelter

CCDC reference: 1106971

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Another look at the structure of octamethylnaphthalene

G. A. Sim

CCDC reference: 1226042

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3-Dimethylamino-1-phenyl-1-propanone hydrochloride monohydrate

E. O. Schlemper, T. S. Mansour and E. M. Kaiser

CCDC reference: 1107030

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N^α-Acetyl-5-nitro-L-histidine

X. Solans and M. Font-Altaba

CCDC reference: 1104771

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A 2:1 complex of 4-nitro-1,2-benzenediamine and 1,4,7,10,13,16-hexaoxacyclooctadecane (18-crown-6)

G. Weber

CCDC reference: 1107674

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Sulfate de tert-butyl[(dihydroxy-3,5 phényl)-2 hydroxy-2 éthyl]ammonium (sulfate de terbutaline) hydraté

D. Hickel, A. Carpy, M. Laguerre and J.-M. Léger

CCDC reference: 1107675

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Liaisons hydrogène dans les cristaux de noxythioline

A. Terol, S. Alberola, B. Jeanjean, F. Sabon and J. C. Jumas

CCDC reference: 1107017

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8-Chloro-1-methyl-6-phenyl-1,2,3,4-tetrahydro-1,5-benzodiazocin-2-one

A. A. Dvorkin, Yu. A. Simonov, T. I. Malinowsky, S. A. Andronati, A. V. Bogatsky and V. V. Danilin

CCDC reference: 1131204

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The structure of aniline at 252 K

M. Fukuyo, K. Hirotsu and T. Higuchi

CCDC reference: 1107005

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Nouvel affinement de la structure de l'acide dodécanedioïque

M. Vanier and F. Brisse

CCDC reference: 1137740

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Détermination de la structure et configuration absolue du p-chlorobenzylidène-2 épicamphre-(−)-(Z)

R. Roques, C. Bertrand, F. Labruyère, J. P. Declercq and G. Germain

CCDC reference: 1107003

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Photosantonin

R. I. Sheldon, C. G. Shaefer, J. Gulbis, J. R. Ruble, A. W. Burgstahler and B. Lee

CCDC reference: 1107002

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Diethylammonium 2,5-dihydroxy-1,4-benzenedisulphonate

X. Solans, F. Plana and M. Font-Altaba

CCDC reference: 1225920

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A charge-transfer complex: bis(2,4,6-trimethyl-1-pyridyl)iodonium perchlorate

G. D. Brayer and M. N. G. James

CCDC reference: 1107038

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X-ray analysis of 3,4-dihydro-2H-[1]benzothieno[3,2-b]pyran-2-spiro-2'(3'H)-(1-benzothiophen)-3'-one

P. J. Cox and R. A. Howie

CCDC reference: 1285281

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Structure of propionamide at 123 K

A. Usanmaz and G. Adler

CCDC reference: 1319146

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Structure of 7α-methyl-4-androstene-3,17-dione

H. J. deL. Cowe, P. J. Cox and G. A. Sim

CCDC reference: 1107028

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Structure of bis(4-biphenylyl)sulphur diimide

V. Busetti

CCDC reference: 1107029

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Structure of bis(4-methylpyridine)hydrogen(I) tetraphenylborate

C. Glidewell and H. D. Holden

CCDC reference: 1107608

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Ethyl trans-7-benzyloxy-4-hydroxy-6-methoxy-1-(3,4,5-trimethoxyphenethyl)-1,2,3,4-tetrahydro-2-isoquinolinecarboxylate

S. Bellard, R. Elliott and E. McDonald

CCDC reference: 1107731

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Structure of p-nitroaniline hydrochloride

G. Ploug-Sørensen and E. K. Andersen

CCDC reference: 1107018

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Structure of 2,4-dinitroaniline

L. Prasad, E. J. Gabe and Y. Le Page

CCDC reference: 1245056

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Piperidinium tetramethoxyborate

N. W. Alcock, R. M. Hagger, W. D. Harrison and M. G. H. Wallbridge

CCDC reference: 1106996

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Octafluorocyclooctatetraene at 238 K

B. B. Laird and R. E. Davis

CCDC reference: 1107063

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5-Methylthio-6-oxo-6H-1,2-oxazin-3,4-dicarbonsäure-dimethylester. Ein ungewöhnliches Reaktionsprodukt eines Sydnons mit Acetylendicarbonester

H. Gotthardt, O. M. Huss and C. M. Weisshuhn

CCDC reference: 1107004

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Acta Cryst. (1982). B38, 682-685
https://doi.org/10.1107/S056774088200380X

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issue contents

February 1982 issue

research papers

short structural papers