Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 57| Part 8

ISSN: 2056-9890

August 2001 issue

Highlighted illustration

Cover illustration: This substituted pyrazine, containing only C, H, N and O atoms, is an energetic compound with a density of 1.812 Mg m^-3. See Gilardi & Butcher [Acta Cryst. E57, o738-o740].

inorganic compounds

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Refinement of lithium tetrahydroxoborate with low-temperature CCD data

F. R. Fronczek, D. A. Aubry and G. G. Stanley

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Ba₆₈Pd₃₂O_x, with x $\simeq$ 13.5

M. Mårtensson, E. Wikstad, H. Blomqvist, M. Kritikos and L. Eriksson

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Rerefinement of sodium thiosulfate pentahydrate

S. M. Prasad and A. Rani

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Charge-doped nickel oxide, Y_1.90Ca_0.10BaNiO₅

F.-X. Lannuzel, F. Boucher and C. Payen

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metal-organic compounds

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μ-Succinato-bis[aquanitrato(1,10-phenanthroline)copper(II)]

L.-S. Long, P.-J. Wang, X.-Y. Chen, X.-M. Fang and S. W. Ng

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Bis(2,2′:6′,2′′-terpyridine)copper(II) diperchlorate hemihydrate

J. Valdés-Martínez, R. A. Toscano and D. Salazar-Mendoza

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Potassium trifluoro[(E)-2-phenyl-1-ethenyl]borate

A. N. Thadani, R. A. Batey, D. V. Smil and A. J. Lough

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Layered structure of catena-poly[[bis[1-(2-azidoethyl)tetrazole-N⁴]copper(II)]-di-μ-chloro]

D. O. Ivashkevich, A. S. Lyakhov, P. N. Gaponik, A. N. Bogatikov and A. A. Govorova

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cis-Dicarbonylbis[1,2-ethanediylbis(diphenylphosphine)-P,P′]tungsten(0) benzene sesquisolvate

A. C. Filippou, A. I. Philippopoulos and B. Ziemer

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A one-dimensional coordination polymer with alternating CeN₃O₆ and SrNO₇ polyhedra

S. Sailaja and M. V. Rajasekharan

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trans-Diaquatetrakis(4,4′-methylenediphenylamine-N)cadmium(II) dinitrate dihydrate

R.-H. Wang, M.-C. Hong, J.-B. Weng, R. Cao, Y.-C. Liang and Y.-J. Zhao

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[5,10,15,20-meso-Tetrakis(2-thienyl)porphyrinato-κ⁴N]copper(II)

Y. Diskin-Posner, S. Balasubramanian, G. K. Patra and I. Goldberg

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Bis[4,4′-bipyridinium(2+)] hexacosaoxooctamolybdate

C.-D. Wu, C.-Z. Lu, H.-H. Zhuang and J.-S. Huang

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Carbonyl(ferrocenyldiphenylphosphine)(tropolonato)rhodium(I)

G. Steyl, S. Otto and A. Roodt

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{2-(4,7-Dimethyl-1,4,7-triazacyclonon-1-yl)-N-methyl-N-[(1-methylbenzimidazol-2-yl)methyl]ethylamine}copper(II) bis(perchlorate)

R. I. Daly, D. C. R. Hockless, M. R. Taylor and L. L. Martin

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The sandwich dimeric form of a Cs^I complex of 18-crown-6 with bridging iodide ions

T. H. Kim, K.-M. Park, S. S. Lee, J. S. Kim and J. Kim

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trans-Bis(dicyanamido-N)-trans-bis(imidazole-N′)copper(II)

J.-H. Luo, M.-C. Hong, Y.-C. Liang and R. Cao

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Poly[(2,2′-bipyridine)copper(II)-μ₄-oxalato]

J.-H. Luo, M.-C. Hong, Y.-C. Liang and R. Cao

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trans-Diiodopentakis(tetrahydrofuran)ytterbium(III) tetraiodo-trans-bis(tetrahydrofuran)ytterbium(III)

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A centrosymmetric hydroxo-bridged pentamethyldiethylenetriamine copper(II) complex, {[(pmdeta)Cu(OH)]₂}²⁺·2Br⁻·2MeCN

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Chloro[N,N′-o-phenylenebis(pyridine-2-carboxamido)]cobalt(III) chloroform disolvate

J. M. Rowland, M. M. Olmstead and P. K. Mascharak

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Di-μ-chloro-bis[(2-pyridinecarboxylato-N,O)(2-pyridinecarboxylic acid-N,O)cadmium(II)] ethanol solvate

M. Odoko, N. Isomoto and N. Okabe

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catena-Poly[[[(1,10-phenanthroline)manganese(II)]-μ-(1-hydroxybenzene-3,5-dicarboxylato)] hydrate]

J. M. S. Skakle, M. R. St J. Foreman and M. J. Plater

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Bis(1,4,7-trithiacyclononane-S,S′,S′′)nickel(II) dibromide tetrahydrate

A. J. Blake, N. R. Brooks, N. R. Champness, P. Hubberstey, I. J. Keppie, M. Schröder and A. C. Marr

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2,2′-Bipyridine(octacarbonyl)dirhenium(Re–Re)

A. J. Blake, M. W. George, E. L. Little and J. J. Turner

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Bis(pyridine-2,4-dicarboxylato)copper(II) dihydrate

Y.-C. Liang, M.-C. Hong, R. Cao and Q. Shi

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Diaquabis(pyridine-2,5-dicarboxylato)cobalt(II)

Y.-C. Liang, R. Cao, M.-C. Hong, Q. Shi, D.-F. Sun and J.-B. Weng

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organic compounds

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2,3-Dimethylquinoxaline–dimethylglyoxime (1/1)

T. Hökelek, H. Batı, Y. Bekdemir and H. Kütük

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DL-Alaninium oxalate

M. Subha Nandhini, R. V. Krishnakumar and S. Natarajan

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Ethyl 2-trans-cinnamoylacetoacetate

A. F. Arrieta and A. Mostad

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1,2:4,5-Di-O-isopropylidene-β-D-erythro-hexo-2,3-diulo-2,6-pyranose

M. Ďurík, V. Langer, D. Gyepesová, J. Mičová, B. Steiner and M. Koóš

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4′-Fluoro-2′-nitroacetanilide

J.-Y. Qi, Z.-Y. Zhou, D.-S. Liu and A. S. C. Chan

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Methyl 2-(2-pyridyl)quinoline-4-carboxylate

A. A. Farah and W. J. Pietro

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Bis(DL-aspartic acid) sulfate

N. Srinivasan, B. Sridhar and R. K. Rajaram

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D-Serinium D-serine nitrate

B. Ravikumar, B. Sridhar and R. K. Rajaram

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Natural diterpenoid ludongnin, octahydro-5′-hydroxy-7a-methyl-8′-methylenespiro[isobenzofuran-4(1H),4′(3′H)-[1H-7,9a]methanocyclohepta[c]pyran]-1′,3,9′(3aH,4′aH)-trione

H. Shi, Y. J. Pan and Z. M. Jin

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Tetra-n-butylammonium phenyltrifluoroborate

T. D. Quach, R. A. Batey and A. J. Lough

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Tris(2-succinimidoethyl)amine hydrate (1/0.075)

A. J. Blake, D. M. J. Doble, W.-S. Li and M. Schröder

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The racemate of pinoresinol

R. Stomberg, V. Langer, S. Li and K. Lundquist

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A phthaloyl-linked benzotriazole corrosion inhibitor: 1,1′-(phthaloyl)bis(benzotriazole)

G. Smith, S. E. Bottle, D. A. Reid, D. P. Schweinsberg and R. C. Bott

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(R)-1,3-Thiazolidin-3-ium-4-carboxylate

N. Grant, M. F. Ward, M. Jaspars and W. T. A. Harrison

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1,2-Bis(diphenylarsino)ethane

N. J. Hill, W. Levason, G. Reid and M. Webster

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2-Fluoro-6-iodobenzonitrile

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Anion–anion dimerization in tetrabutylammonium hydrogensulfate

M. E. Light, P. A. Gale and M. B. Hursthouse

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Piperidinium p-nitrobenzoate

Y. Moritani, A. Takeda and S. Kashino

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2,2-exo-3,5,6-Pentabromobicycloheptane

T. Hökelek, İ. Çelik, A. Tutar and O. Çakmak

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1:1 Complex of 2,4-dinitrophenol and 4-methoxypyridine N-oxide hydrate

R. Moreno-Fuquen, F. Cano, M. Martinez-Ripoll, A. Montaño and J. Zukerman-Schpector

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3,4-Dihydroxyphenylacetic acid

N. Okabe and H. Kyoyama

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Bis(N-methyl-N-phenylthiocarbamoyl) disulfide

H.-K. Fun, S. Chantrapromma, I. A. Razak, F.-L. Bei, F.-F. Jian, X.-J. Yang, L. Lu and X. Wang

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N-(3-Pyridyl)urea

S. George and A. Nangia

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4-(4-Ethoxyphenylamino)-2-oxo-1,2-dihydroquinoline

V. B. Rybakov, V. V. Chernyshev, I. V. Ukrainets, P. A. Bezugly, L. V. Sidorenko and N. Skaif

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(+)-N-{4-[(1S,2S)-2-(Dimethylamino)-1-(1H-imidazol-1-yl)propyl]phenyl}-2-benzothiazolamine

O. M. Peeters, N. M. Blaton and C. J. De Ranter

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Pentafluorophenyl 3-chloro-3-phenylpropanoate

B. Chan, E. W. Tan and A. G. Blackman

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Anion–anion one-dimensional chain formation within cationic channels in tetrabutylammonium dihydrogenphosphate dichloromethane solvate

M. E. Light, S. Camiolo, P. A. Gale and M. B. Hursthouse

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2-[(2-Chlorophenyl)iminomethyl]-4,6-dimethylquinoline

S. Öztürk, M. Akkurt, M. Aygün and F. Aydogan

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9-p-Toluidinoanthracene

S. Lahlou, A. Kerbal, T. Janati, S. A. Lyazidi, N. Bitit, B. El-Bali and M. Bolte

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2,2′-Dihydroxychalcone

S. Kashino, M. Tanaka and T. D. Todorov

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2,6-Diamino-3,5-dinitropyrazine

R. D. Gilardi and R. J. Butcher

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1,3-Diphenyl-1-o-tolyl-3,4-dimethylindan

R. Spagna, G. L. Cascarano, F. Ciminale, G. M. Farinola and L. Lopez

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Imidazolium 2-chloro-4-nitrobenzoate

H. Ishida, B. Rahman and S. Kashino

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Bis(DL-methioninium) sulfate

N. Srinivasan, B. Sridhar and R. K. Rajaram

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N,N′-Di-2-naphthylpyridine-2,6-dicarboxamide

J.-Y. Qi, Z.-Y. Zhou and A. S. C. Chan

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Glycinium maleate

K. Rajagopal, R. V. Krishnakumar, A. Mostad and S. Natarajan

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Bis(D-phenylglycinium) sulfate monohydrate

N. Srinivasan, B. Sridhar and R. K. Rajaram

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2,6-Diamino-3,5-dinitro-1,4-pyrazine dimethyl sulfoxide solvate

R. D. Gilardi and R. J. Butcher

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2-{3-[2-(1H-Indol-3-yl)vinyl]-5,5-dimethylcyclohex-2-enylidene}malononitrile

T. Kolev, Z. Glavcheva, D. Yancheva, M. Schürmann, D.-C. Kleb, H. Preut and P. Bleckmann

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4,5,7,8-Tetrahydro-2-(2-propenyl)-6H-[1,3,6,2]dioxazaborocine

A. N. Thadani, R. A. Batey and A. J. Lough

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Gallic acid monohydrate

N. Okabe, H. Kyoyama and M. Suzuki

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1-Methylethyl 2-[(1-bromo-2-naphthyl)oxy]ethanoate

J. M. S. Skakle and S. M. S. V. Wardell

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DL-Threoninium oxalate

M. S. Nandhini, R. V. Krishnakumar, R. Malathi, S. S. Rajan and S. Natarajan

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Bis(DL-phenylalaninium) sulfate monohydrate

N. Srinivasan, B. Sridhar and R. K. Rajaram

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1-[2-(Dicarboxymethyl)-3-oxocyclopent-4-en-1-yl]pyrrolidin-1-ium bromide hydrate

J. Kožíšek, P. Šafář and V. Langer

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N-(1-Benzenesulfonyl-4-acetylpyrrol-3-yl)acetamide

D. A. Grossie, D. Ketcha, J. P. Brooke, S. A. Jones and J. G. Grieb

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5,17-Di-tert-butyl-25,27-dihydroxycalix[4]arene

J. C. Bryan, R. A. Sachleben and A. Urvoas

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3-Pyridylmethyl urea dihydrate

W. T. A. Harrison

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An isoindoline EPR label: 5-acetamido-1,1,3,3-tetramethylisoindolin-2-yloxyl

G. Smith, S. E. Bottle, D. A. Reid and R. C. Bott

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Racemic 6-exo-hydroxybicyclo[2.2.1]heptane-2-exo-carboxylic acid

G. Smith, R. C. Bott, I. D. Jenkins and U. D. Wermuth

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1,2,3,4-Tetrachloro-11,11-dimethoxy-1,4,5,6,9,10-hexahydro-endo-1,4-exo-6,9-dimethanonaphthalene

A. J. Blake, A. Dietel, W.-S. Li and N. R. Thomas

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1,5-Dichloro-3,6,6-triphenyl-3-azabicyclo[3.2.0]heptane-2,4-dione

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, B.-G. Zhao and J.-H. Xu

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2-p-Toluoylquinoxaline

K. Chowdhury, R. Mukhopadhyay, M. Mukherjee, C. K. Broder and N. G. Kundu

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Diisopropyl hydrazocarboxylate

T. Gelbrich, J. D. Kilburn and M. B. Hursthouse

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Cyclo(alanine-4-hydroxyproline)

S. F. Pavkovic, J. A. Zerkowski and Q. Zeng

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2-(1-Naphthyl)cyclohexyl 3-furancarboxylate

M. Parvez, I. R. Hunt and B. A. Keay

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2-Phenylcyclohexyl 3-furancarboxylate

M. Parvez, I. R. Hunt and B. A. Keay

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2-(1-Naphthyl)cyclohexyl 2-methylfuran-3-carboxylate

M. Parvez, I. R. Hunt and B. A. Keay

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Racemic 7-oxabicyclo[2.2.1]heptane-5-exo-iodo-6-endo-hydroxy-2-endo-carboxylic acid-γ-lactone

G. Smith, R. C. Bott, I. D. Jenkins and U. D. Wermuth

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2-[(5-Méthylisoxazol-3-yl)méthyl]benzimidazole

K. H. Attar, B. E. Azaoui, M. Benchidmi, E. M. Essassi and M. Pierrot

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NTA–1,10-phenanthroline–water (1/1/1)

N. Shan, A. D. Bond and W. Jones

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N^S,N^O-Diphenyl(thiooxamide)

V. B. Rybakov, E. V. Babaev and Y. V. Dlinnykh

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Kudos

Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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