Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 58| Part 3

ISSN: 2056-9890

March 2002 issue

Highlighted illustration

Cover illustration: The difference in size complementarity between the radius of the cation and the 24-crown-8 cavity causes the macrocycle to adopt a folded, twisted conformation, encapsulating the ammonium cation. See Fallon, Lau & Langford [Acta Cryst. E58, o321-o323].

inorganic compounds

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The intermetallic compound BaAgBi

S. K. Kang and G. J. Miller

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Sodium zinc tris(dihydrogenphosphite) hydrate, NaZn(H₂PO₃)₃·H₂O

R. Ouarsal, A. A. Tahiri, B. El Bali, M. Lachkar and W. T. A. Harrison

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Lithium potassium tungstate monohydrate, LiKWO₄·H₂O

I. Radosavljevic Evans and J. A. K. Howard

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metal-organic compounds

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Further refinement of diaqua(1,7,11,17-tetraoxa-2,6,12,16-tetraazacycloeicosane-N,N′,N′′,N′′′)nickel(II) dichloride

V. A. Kuksa, S. M. S. V. Wardell, P. K. T. Lin and R. A. Howie

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Bis(8-hydroxyquinolinato)oxopropoxovanadium(V)

N. Okabe, Y. Muranishi and M. Odoko

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[NH₃(CH₂)₃NH₃][Ga(P₂O₇)(H₂PO₄)]: a new organically templated gallium phosphate-diphosphate

J. L. Kissick and A. M. Chippindale

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{[μ-N,N′-Bis(salicylidene)-1,3-propanediaminato-N,N′-dimethylformamide]zinc(II)}dichlorozinc(II)

L. Tatar, O. Atakol and D. Ülkü

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(N,N-Diethyldithiocarbamato)[tris(p-methoxyphenyl)phosphine]gold(I)

S. Y. Ho and E. R. T. Tiekink

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Heptacarbonyl(α-ethoxybenzylidene)di-μ-diethylphosphidodirhenium

U. Flörke and D. Petters

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Tris(pentafluorophenyl)[2-(diphenylphosphino)thiophenol-κP]gold(III) dichloromethane solvate

P. G. Jones, R. Terroba, E. Fernández and M. Laguna

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cyclo-Decakis(μ-2,2-diphenylacetato-O,O′)dodecakis(μ-methoxo)decairon(III)) mixed solvate

H. Kooijman, A. L. Spek, E. Bouwman, F. Miccichè, S. T. Warzeska and J. Reedijk

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Dichloro[2-chloro-6-(mercaptopyridin-2-yl)pyridine]copper(II)

A. J. Blake, M. W. George, P. Hubberstey, R. L. Garcia and C. Wilson

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catena-Poly[[tetrakis(μ-acetato-κO:κO′)dicopper(II)]-μ-2-aminopyrimidine-κ²N:N′] at 150 K

A. J. Blake, P. Hubberstey and C. L. Sampson

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A mixed copper(I)/copper(II) complex coordinated by a multidentate amidato ligand

G. Kickelbick and T. Gallauner

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Tetrakis(iodomethyl)stannane

R. A. Howie, J. M. S. Skakle and J. L. Wardell

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Dibromotetrakis(4-methylimidazole)copper(II) dihydrate

C. Näther, M. Wriedt and I. Jeß

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A cluster containing a pyrazole ligand: [Ru₃(μ-H)(μ-N₂C₃H₃)(CO)₁₀]

E. L. Diz, A. Neels, B. Therrien, H. Stoeckli-Evans and G. Süss-Fink

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[μ-N,N,N′,N′-Tetrakis(2-pyridylmethyl)-1,2-ethanediamine]bis[dichlorocopper(II)]

D.-C. Yoon, C.-E. Oh and U. Lee

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Octacarbonyl-μ-dicyclohexylphosphido-μ-N,N-diethyldithiocarbamato-dirhenium

H. Egold, U. Flörke and S. Klose

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Bis(aquamethyldiphenyltrifluoroacetatotin)–18-crown-6 (1/1)

M. M. Amini, M. Yousefi and S. W. Ng

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Tetrakis(μ-benzoato)bis[(N,N-diethylnicotinamide)zinc(II)]

H. Necefoglu, W. Clegg and A. J. Scott

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A linear trinuclear CaZn₂ complex with bridging benzoate ligands

H. Necefoglu, W. Clegg and A. J. Scott

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unsym-fac-(exo-OH)-[Co(dien)(dapo)(N₃)][ZnCl₄]

R. J. Browne, D. A. Buckingham, A. G. Blackman and C. R. Clark

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Dichlorobis(DL-alanine)zinc(II)

M. Subha Nandhini, R. V. Krishnakumar and S. Natarajan

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Bis(pyrazine-2-carboxamide)bis(trifluoromethanesulfonato)copper(II) monohydrate

O. Kristiansson

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organic compounds

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Dimethyl 1,3-dichloro-8-phenyl-5-phenylsulfanylisoquinoline-6,7-dicarboxylate

H.-K. Fun, A. Usman, I. A. Razak, S. Chantrapromma, T. K. Sarkar, S. Basak and N. Panda

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Tetramethylguanidinium chloride

A. K. Fischer and P. G. Jones

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Ethyl 4-oxo-2,6-diphenylpiperidine-3-carboxylate

L. Vijayalakshmi and T. R. Radhakrishnan

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A monoclinic polymorph of 3-amino-4′-(N,N-diethylamino)-5-methylbiphenyl-2,4-dicarbonitrile

A. Subbiah Pandi, D. Velmurugan, S. Shanmuga Sundara Raj, H.-K. Fun and V. Raghukumar

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Methyl (2′R,3′R)-6-deoxy-3,4-O-(2′,3′-dimethoxybutane-2′,3′-diyl)-2-O-toluene-p-sulfonyl-α-L-mannopyranoside

J. C. Barnes, J. S. Brimacombe, L. M. C. Connolly and A. P. Dix

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Methyl (2′R,3′R)-2-azido-2,6-dideoxy-3,4-O-(2′,3′-dimethoxybutane-2′,3′-diyl)-α-L-glucopyranoside

J. C. Barnes, J. S. Brimacombe, L. M. C. Connolly and A. P. Dix

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(2-Methoxyphenyl)phenylphosphine oxide

W. Wieczorek, R. Kruszynski, J. J. Skoweranda and K. M. Pietrusiewicz

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(1R,2S)-3-Methyl-2-(p-methylphenylsulfonylamino)-1-phenylbutan-1-ol

X. Li, X. Jia and Z. Zhou

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3-Pyridylmethylphosphonic acid monohydrate

L. Chęcińska, M. Małecka, K. Aranowska and J. Ochocki

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(E)-2-Styryl-[1,3,6,2]dioxazaborolane

A. N. Thadani, R. A. Batey, A. J. Lough and D. V. Smil

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A tetra-tert-butylcalix[4]arene-12-crown-4 N,N-dimethylformamide inclusion complex

J. C. Bryan and T. G. Levitskaia

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1,3,5-Tris(phenylthiomethyl)-2,4,6-trimethylbenzene

J.-R. Li, Z. Yan, M. Du, Y.-B. Xie, R.-H. Zhang and X.-H. Bu

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Propyl gallate dihydrate

N. Okabe and H. Kyoyama

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( $\pm$ )-2,5-Dioxoperhydrocycloocta[b]furan-3-carboxylic acid

B. W. Greatrex, M. C. Kimber, D. K. Taylor and G. D. Fallon

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1-Acetamido-1-(1-naphthyl)ethylene

X. Jia, X. Li, Z. Zhou, R. Guo, Y. Chen and X. Yao

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[(2R,5S)-2,5-Bis(4-nitrophenyl)perhydrofuro[2,3-b]furan-3-yl]triisopropylsilane

M. E. Light and M. B. Hursthouse

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1-Ethyl-4-hydroxy-2-oxo-1,2-dihydroquinoline-3-carboxylic acid

S. V. Shishkina, O. V. Shishkin, I. V. Ukrainets, A. N. Dakkah and L. V. Sidorenko

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(3S,2R)-3-Hydroxy-2-hydroxymethyl-7,9-diazaspiro[4.5]decane-6,8,10-trione

M.-T. Averbuch-Pouchot, A. Durif, A. Renard, M. Kotera and J. Lhomme

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2,3,5-Trichloro-6-(2-diethylaminovinyl)-1,4-benzoquinone

A. Krivokapic and H. L. Anderson

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1-Benzoyl-2(S)-tert-butyl-4-methoxy-6(S)-carbomethoxy-1,2,5,6-tetrahydro-1,3-pyrimidine: a useful precursor of α-alkylated aspartic acids

J. Giraldés, M. L. McLaughlin and F. R. Fronczek

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4-Bromophenyl 2,6-dibromophenyl ether

J. Eriksson, L. Eriksson and J. Hu

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3-(Dicyanomethylene)-1,5-diphenylpenta-1,4-diyne

P. G. Jones, H. Hopf and M. Kreutzer

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2,2,2-Tris(cyclohexyloxy)-4,5-(2′,2′'-biphenylo)-1,3,2-dioxaphospholene

P. G. Jones, A. J. Kirby and M. Pilkington

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(S)-2,2′-Bis[bis(3,5-dimethylphenyl)phosphinoyl]-5,5′,6,6′,7,7′,8,8′-octahydro-1,1′-binaphthyl

R. Guo, J. Wu, W. Kowk, J. Chen, M. C. K. Choi and Z. Zhou

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Bis(L-glutamic acid) sulfate hemihydrate

B. Sridhar, N. Srinivasan and R. K. Rajaram

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2,7-Dimethylocta-2,3,5,6-tetraene

P. G. Jones, P. Bubenitschek, H. Hopf and R. Stamm

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DL-Valinium trichloroacetate at 123 K

K. Rajagopal, R. V. Krishnakumar, M. Subha Nandhini, A. Mostad and S. Natarajan

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N-Phenyl-2-nitrobenzamide, an acridone alkaloid precursor

R. J. Jackson, M. Parvez, S. S. Nizami and R. Y. Khan

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Cirsimaritin

N.H.-H. Chou, M. Parvez, M. S. Ali, S. Ahmed and W. Ahmed

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2-(N-Phenylacetamido)-6H-1,3-thiazin-6-one

M. Evain, C. Landreau, D. Deniaud, A. Reliquet and J. C. Meslin

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4-Methyl-N-(prop-2-ynyl)-N-(1H-pyrrol-2-ylmethyl)benzenesulfonamide

J. W. Bats, J. P. Weyrauch and A. S. K. Hashmi

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N-(2-Aminoethyl)dithiocarbamic acid

B. M. Yamin, M. A. Kadir, M. Z. M. Zin, A. Usman, I. A. Razak and H.-K. Fun

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3-Bromo-β-lapachone

C. A. De Simone, V. R. S. Malta, M. A. Pereira, J. R. S. Bispo, A. V. Pinto and M. C. F. R. Pinto

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( $\pm$ )-2-Oxo-4-(2-oxo-2-phenylethyl)-5-phenyltetrahydrofuran-3-carboxylic acid

B. W. Greatrex, M. C. Kimber, D. K. Taylor and G. D. Fallon

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4,13-Diacetyl-[2.2]paracyclophane

P. G. Jones, H. Hopf and J. Hillmer

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1-Phenyl-2-phenylsulfinylcyclobutan-1-ol

W. A. Loughlin, C. C. Rowen, Z. D. Berg and P. C. Healy

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(2-Bromophenyl)diphenylphosphine

M. L. Williams, C. L. Noack, R. J. Saverin and P. C. Healy

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(1S,2R)-N-[(E)-4-Methoxycinnamoyl]-10,2-camphorsultam

F. Garzino, A. Méou, P. Brun and G. Pèpe

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(2R,3R)-2-(4-Methoxyphenyl)-3-{1-[(3aS)-(3aα,6α,7aα)-hexahydro-8,8-dimethyl-3H-3a,6-methano-2,2-dioxo-2,1-benzoisothiazolyl]carbonyl}-4-isopropoxycarbonyl-5-methyl-2,2-dihydrofuran

F. Garzino, A. Méou, P. Brun and G. Pèpe

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2′,3′-Diphenyl-4′-p-tolylspiro[isothiachroman-3,5′-isoxazolidin]-4(2H)-one

B. Bennani, B. Filalibaba, A. El-Fazazi, G. A. Houari, N. Bilit, A. Kerbal, B. El-Bali and M. Bolte

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5,7,7,8,10-Pentabromo-7,8-dihydrobenzocyclooctene

I. Çelik, A. Tutar, M. Akkurt, Y. Özcan and O. Çakmak

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N-(3-Chlorophenyl)-2-hydroxy-1-naphthaldimine at 200 K

G. Pavlović, J. M. Sosa, D. Vikić-Topić and I. Leban

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Ammonium 2,5,8,11,21,24,27-octaoxatricyclo[26.4.0.0^12,17]dotriaconta-1(32),12(17),13,15,28,30-hexaene hexafluorophosphate

G. D. Fallon, V.-L. Lau and S. J. Langford

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Matricarin

M. Parvez, V. U. Ahmad, U. Farooq, A. R. Jassbi and H. S. Raziullah

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2,5-Lutidine

A. D. Bond and J. E. Davies

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3,4-Lutidine

A. D. Bond and J. E. Davies

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α-Methylstyrene

A. D. Bond and J. E. Davies

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Diisopropyl 2-(2-benzoyl-1-phenylethyl)malonate

A. Jeyabharathi, M. N. Ponnuswamy, S. Narasimhan and S. Velmathi

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A vinylic α-carbamoyloxyborane with a carbenoid-type bonding arrangement

P. Kocieński, M. Marsch, K. Harms and G. Boche

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4,4′-Methylenediantipyrine monohydrate

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o-Methylselenobenzoyl cyanide

L. Dupont, M. Messali and L. Christiaens

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A phenyl-end-capped tetramer of aniline

M. Evain, S. Quillard, B. Corraze, W. Wang and A. G. MacDiarmid

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N-(5-Phenylseleno)pentylphthalimide

W.-X. Zhang, H.-T. Yu, D.-R. Bai and J.-B. Meng

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2,4-Dibromophenyl 2,6-dibromophenyl ether

J. Eriksson, L. Eriksson and J. Hu

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Kudos

Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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