Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 58| Part 10

ISSN: 2056-9890

October 2002 issue

Highlighted illustration

Cover illustration: Venlafaxine is an antidepressant drug. A second, monoclinic, polymorph of its hydrochloride has been characterized; its conformation differs from that of the previously reported orthorhombic form. See Sivalakshmidevi, Vyas, Mahender Rao & Om Reddy [Acta Cryst. E58, o1072-o1074].

inorganic compounds

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Calcium sodium iminodisulphonate trihydrate, a product of flue-gas desulfurization

F. Fogh, A. Hazell and S. E. Rasmussen

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Rb₂Al₂B₂O₇

J. L. Kissick and D. A. Keszler

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K₄(CrO₄)(NO₃)₂, the first chromate(VI)-nitrate

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Cobalt potassium dihydrogendiphosphate dihydrate, CoK₂(H₂P₂O₇)₂·2H₂O

A. Alaoui Tahiri, R. Ouarsal, M. Lachkar, B. El Bali and M. Bolte

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Decaammonium dodecatungstate nonahydrate, (NH₄)₁₀[H₂W₁₂O₄₂]·9H₂O: anionic `isomorphism'

G. J. Gainsford, S. V. Chong, B. Ingham and J. L. Tallon

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Titanium(IV) chloride at 150 K

A. Dawson, A. Parkin, S. Parsons, C. R. Pulham and A. L. C. Young

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metal-organic compounds

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cis-[1,3-Bis(diphenylphosphino)propane]dibromoplatinum(II)

J. L. Morgan, B. H. Robinson and J. Simpson

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Poly[diaqua(μ₄-squarato-O,O′,O′′,O′′′)iron(II)]

C. Näther, J. Greve and I. Jeß

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Bis[(1R,2R)-(−)-1,2-bis(trimethylsilylamino)cyclohexane(2−)-κ²N,N′]zirconium(IV)

J.-F. Li, L.-H. Weng, S.-P. Huang, H.-B. Tong and D.-S. Liu

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Metal-binding modes in sulfoxines: supramolecular network in (8-hydroxyquinoline-5-sulfonato-N¹,O⁸)sodium(I)

S. Baskar Raj, P. T. Muthiah, G. Bocelli and R. Olla

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Tris(O-methyldithiocarbonato)chromium(III)

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Bis(μ-N-(3-[3-indenyl]propyl-p-toluenesulfamido-N,O,O′)-dimethylamidodichorotitanium)

C. Lensink, G. J. Gainsford and M. J. R. Brandsma

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(NH₄)₂(NH₃(CH₂)₆NH₃)₄[H₂W₁₂O₄₂]·8H₂O: a novel ammonium 1,6-hexanediammonium dodecatungstate

G. J. Gainsford, N. Robinson and J. L. Tallon

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Tris[bis(diethylenetriamine)nickel(II)] bis[hexacyanoferrate(III)] decahydrate

I. Muga, P. Vitoria, J. M. Gutiérrez-Zorrilla, A. Luque and P. Román

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Trimethylphenylammonium trichloromercurate(II), (Me₃PhN)[HgCl₃]

P. Nockemann and G. Meyer

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Bis(tetraethylammonium) di-μ-bromo-bis[dibromomercurate(II)], (Et₄N)₂[Hg₂Br₆]

P. Nockemann and G. Meyer

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Bis(tetraethylammonium) octabromotrimercurate(II), (Et₄N)₂[Hg₃Br₈]

P. Nockemann and G. Meyer

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Bis(tetraethylammonium) decachloro- tetramercurate(II), (Et₄N)₂[Hg₄Cl₁₀]

P. Nockemann and G. Meyer

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Bis(O-methyldithiocarbonato)cadmium(II)

V. G. Young Jr and E. R. T. Tiekink

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A nanoporous three-dimensional metal coordination polymer {(NH₄)₂Zn[C₆H₂(COO)₄]·8H₂O}_n

Y.-Q. Sun, J. Zhang and G.-Y. Yang

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1,1,1-Tris(2-hydroxybenzylideneamino)methylpropane iron(III) chloroform solvate

J. Reglinski and M. Patykiewicz

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Bis(1,10-phenanthroline)diazidonickel(II)

Y.-Q. Cheng, A.-L. Liu, M.-L. Hu and S. W. Ng

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Hexaaquazinc(II) dihydrogen-1,2,4,5-benzenetetracarboxylate

Y.-Q. Sun, J. Zhang and G.-Y. Yang

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Bisquinolinium tetrachlorocuprate dihydrate

D. E. Lynch and I. McClenaghan

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Tetrakis(2-methylimidazolo)bis(trifluoromethylsulfonato)copper(II)

S.-J. Liu, R.-J. Wang and C.-C. Su

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[RuCl{2,6-bis(3,4-dihydro-2H-pyrrol-5-yl)pyridine}(PPh₃)₂]BF₄ dichloromethane solvate

A. Cabort, B. Therrien, K. Bernauer and G. Süss-Fink

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fac-Tricarbonylchloro(1,10-phenanthroline)rhenium(I)

S. F. Haddad, J. A. Marshall, G. A. Crosby and B. Twamley

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An oxygen-bridged bis(sila[1]ferrocenophane), [Fe(η-C₅H₄)₂Si(Me)]₂O

A. Berenbaum, A. J. Lough and I. Manners

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[2,6-Bis(3,4-dihydro-2H-pyrrol-5-yl)pyridine]trichlororhodium(III) dibenzene solvate

A. Cabort, B. Therrien, K. Bernauer and G. Süss-Fink

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Diazidotetraimidazolenickel(II)

Q.-Z. Zhang, C.-D. Wu, W.-B. Yang, Y.-Q. Yu, S.-M. Chen, X.-P. Zhan and C.-Z. Lu

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Diaquadihydroxohexakis(tri-tert-butoxysilanethiolato)octalithium(I)–toluene (1/2)

K. Baranowska, J. Chojnacki, W. Wojnowski and I. Krossing

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Nonacarbonyl-μ-hydrido-(μ³,η²-triisopropylsilylethynyl)triruthenium

E. Delgado, B. Donnadieu, E. Hernandez, M. P. Martin and F. Zamora

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Bis[1-(2,4-dichlorobenzoylhydrazonomethyl)ferrocene(1–)]nickel(II)

G.-S. Huang, Y.-Z. Li, Y.-X. Ma, Q.-B. Song and Y.-M. Liang

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trans-Bis(2-amino-5-methyl-1,3,4-thiadiazole-κN)bis(3,5-dicarboxybenzoato-κO)copper(II) dihydrate

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cis-Bis(amidinothioureato-κ²N,N′)nickel(II)

M. K. Kabir, K. Yamada, K. Adachi, M. Kondo and S. Kawata

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Nicotinium tetrachlorocuprate(II)

S.-N. Choi, Y.-M. Lee, H.-W. Lee, S. K. Kang and Y.-I. Kim

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Trichloro(tetrahydrofuran)gallium(III)

S. Scholz, H.-W. Lerner and M. Bolte

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trans-Bis(isothiocyanato)tetrapyridineruthenium(II) dichloromethane disolvate

J. Chen, L. Han and Z. Chen

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(μ-Benzenethiolato)bis[(bipyridine)tricarbonylrhodium(I)] perchlorate dichloromethane hemisolvate

Y. Chen, L. Zhang and Z. Chen

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The lamellar architecture of 1,6-hexamethylenediammonium tetrachlorocobaltate(II)

A. H. Mahmoudkhani and V. Langer

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Tris(1,10-phenanthroline)copper(II) tricyanomethanide

I. Potočňák, M. Pohlová, C. Wagner and L. Jäger

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Bis(μ-N-n-propyl-N-trimethylsilylbenzamidinato)bis[(diethyl ether-O)lithium]

C. L. Boyd, B. R. Tyrrell and P. Mountford

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Hexaaquacobalt(II) tetrapotassium diethylenediaminetetraacetato(4–)cobaltate(III) β-octamolybdate hexahydrate

U. Lee, H.-C. Joo and M.-A. Cho

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The two-dimensional coordination polymer tetraaquamesaconatobarium(II), [Ba(C₅H₄O₄)(OH₂)₄]_n

A. Briceño, J. M. Delgado and G. Díaz de Delgado

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Bis[μ-bis(4-nitrophenyl) phosphato-κ²O:O]bis[(4,4′-dimethyl-2,2′-bipyridine)nitratocopper(II)]

J. R. Deschamps, C. M. Hartshorn and E. L. Chang

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organic compounds

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endo-4-Phenyl-7-n-propyl-2-oxa-6-thia-3-azabicyclo[3.2.0^1,4]hept-3-ene 6,6-dioxide

G. J. Gainsford and A. D. Woolhouse

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5,5′-Dimethyl-2,2′-dithiodi-1,3,4-thiadiazole

J.-L. Song, W.-B. Zhou, H.-Y. Zeng and Z.-C. Dong

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2-Hydroxy-3-(p-nitrobenzenesulfonylamino)propylammonium p-nitrobenzenesulfonate

K. W. Y. Chan and W. T. Wong

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4-Methyl-2-(8-quinolyl)phthalazin-1-one

D. E. Lynch and I. McClenaghan

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3,5-Bis(3-chlorophenyl)-4-formyl-2,6-dimethylcyclohexan-1-one

T. R. Sarangarajan, K. Panchanatheswaran, K. Thanikachalam and R. Jeyaraman

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1-Acetyl-1,2-dihydro-2-oxotrispiro[indole-3,2′-oxetane-3′,1′′; 4′,1′′′-dicyclopropane]

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

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A redetermination of 4′-hydroxyacetophenone

A. J. Kresge, A. J. Lough and Y. Zhu

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2-Benzoyl-3-(1,2-dioxo-2-phenylethyl)-3-phenyl-2-(pyridin-2-yl)oxirane

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Li, Y. Zhang and J.-H. Xu

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2-(2,4-Dichlorophenyl)-5-fluoro-6-morpholin-4-yl-1H-benzimidazole monohydrate

S. Özbey, F. B. Kaynak, C. Kuş and H. Göker

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9-(Thio-2′-methyl-4′-nitrophenyl) acridine

A. Mrozek, J. Karolak-Wojciechowska, P. Amiel and J. Barbe

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trans-[8]Paracyclophan-4-ene-3,6-dione

P. G. Jones, K.-L. Noble, P. Bubenitschek and H. Hopf

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8-Hydrazinoquinoline dihydrochloride hydrate

D. E. Lynch and I. McClenaghan

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A monoclinic polymorph of venlafaxine hydrochloride

A. Sivalakshmidevi, K. Vyas, S. Mahender Rao and G. Om Reddy

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1-Methoxymethyl-5-ethyl-6-(1-naphthylmethyl)uracil

G. Meng, L. H. Weng and F. E. Chen

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(1R,2R)-(−)-1,2-Dibenzamidino-cyclohexane

J.-F. Li, L.-H. Weng, S.-P. Huang, H.-B. Tong and D.-S. Liu

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The 1:1 complex of 4-chloro-3-nitrobenzoic acid and pyridazine

H. Ishida, T. Fukunaga and S. Kashino

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The 1:1 complex of 2-chloro-4-nitrobenzoic acid and 1,2,3-benzotriazole

H. Ishida, T. Fukunaga and S. Kashino

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Benzimidazolium 2-chloro-4-nitrobenzoate

H. Ishida, T. Fukunaga and S. Kashino

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Ethylenediammonium 4-nitroanthranilate dihydrate

G. Smith, U. D. Wermuth and J. M. White

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(E)-Ethyl 3-acetamido-2-hexenoate

X. Chen, R. Guo and Z. Zhou

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2-[5,5-Dimethyl-3-(2-p-tolyl-vinyl)-cyclohex-2-enylidene]-malononitrile

T. Kolev, D. Yancheva, M. Schürmann, D.-C. Kleb, H. Preut and M. Spiteller

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A diphenylboron chelate of an N-alkyl-2,2-diarylglycolohydroxamic acid

W. Kliegel, U. Schumacher, B. O. Patrick, S. J. Rettig and J. Trotter

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Propanone 2-chloro-4,6-dinitrophenylhydrazone

Y. Kawai, M. Hayashi and N. Tokitoh

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Imidazolium trihydrogen-1,2,4,5-benzenetetracarboxylate

Y.-Q. Sun, J. Zhang and G.-Y. Yang

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DL-Phenylalaninium nitrate

B. Sridhar, N. Srinivasan and R. K. Rajaram

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An unexpected TTFAQ donor–fluorene acceptor reaction resulting in a novel salt: 2,6-dihexyloxy-9,10-bis(4,5-dimethyl-1,3-dithiol-2-ylium)-anthracene bis(2,5,7-trinitro-4-bromo-9-cyanofluorenide) dioxane trisolvate

A. S. Batsanov, M. R. Bryce, S. B. Lyubchik and I. F. Perepichka

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2-(2-Nitrophenyl)-4,5-benz-1,3-oxazin-6-one

B. N. Yadav, S. Prasad and S. M. Prasad

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3,5-Dimethyl-2H-pyrazol-1-ium diphenylphosphate

M. Małecka, A. Rybarczyk-Pirek, S. J. Grabowski, K. Malinowska and J. Ochocki

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1-(2-Hydroxy-4,6-dimethoxy-3-methylphenyl)-3-(4-methoxyphenyl)-2-methyl-1,3-propanedione

R. Stomberg, V. Langer and M. Hauteville

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erythro-2-Piperidinyl-1,2-diphenylethanol

N. Ocak, C. Kazak, S. Öztürk, C. Zerrin, N. Arsu, H.-K. Fun and A. Erdönmez

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A chiral oxazolidin-2-one-derived Reissert compound

M. Evain, M. Pauvert, S. Collet and A. Guingant

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A chiral 3,4-dihydro-2H-thiopyran compound

M. Evain, S. Collet and A. Guingant

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Triethylammonium 8-acetyl-3-methyl-9-phenyl-7-oxo-2-azaspiro[4.5]dec-2-ene-4-nitronate

M. F. A. Adamo, S. Chimichi, D. Donati and P. Sarti-Fantoni

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Dihydronium 3-nitrobenzenesulfonate

C. George, J. R. Deschamps and A. P. Purdy

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The 1:1 adduct of 1,3,5-trinitrobenzene with 1,2,3,4-tetrahydroquinoline

G. Smith, U. D. Wermuth and J. M. White

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3-Pentafluorothiopropionic acid

A. F. T. Yokochi, R. Winter and G. Gard

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3-(1-Methyl-5-nitroimidazol-2-yl)-1-(methylsulfonyl)imidazolidin-2-one

L. Damodharan, V. Pattabhi and K. Nagarajan

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2-Amino-6-nitrobenzo-1,3-thiazole hydrate

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κ²N¹³,N^13′-Hydro-rac-2,2′-bis[2-(1-propylbenzimidazol-2yl)]biphenyl trifluoromethanesulfonate, the salt of a novel proton sponge

R. T. Stibrany, H. J. Schugar and J. A. Potenza

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1,4,5,8-Tetramethoxyanthracene

J. W. Springer, T. A. Moore, A. L. Moore, D. Gust and T. L. Groy

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4-Bromophenyl 2,3,4,5,6-pentabromophenyl ether

L. Eriksson and J. Hu

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2-Phenylpyrrolo[2,3-h]quinoline dihydrate

D. E. Lynch and I. McClenaghan

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erythro-2-Morpholino-1,2-diphenylethanol

N. Karadayı, C. Kazak, S. Öztürk, M. Aydın, N. Arsu, H.-K. Fun and O. Büyükgüngör

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(Z)-4-(4-{4-[(Z)-1-Methyl-3-oxobut-1-enylamino]phenoxy}phenylamino)pent-3-en-2-one

Y.-H. Feng, X.-H. Yin, L. Chen, M.-Y.. Tan and K.-B. Yu

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Ethyl (E)-3-acetamido-2-butenoate

X. Chen, R. Guo and Z. Zhou

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Methyl (E)-3-acetamido-2-butenoate

X. Chen, R. Guo and Z. Zhou

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Cyclopropyl m-nitrophenyl ketone

V. M. Kolb, M. G. Donahue, E. A. Putnam, C. Y. Meyers and P. D. Robinson

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N,N′-Bis(2-pyridylethyl)oxamide

A.-W. Xu, H.-X. Zhang, H.-Y. Tan and B.-S. Kang

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2-Propyl mesityl sulfone

C. Y. Meyers, W. Roper, F. Klavetter, T. Horii, P. B. Sandrock and P. D. Robinson

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(+)-(3S,4R)-Norcisapride hydrogen (2R,3R)-tartrate monohydrate

O. M. Peeters and N. M. Blaton

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2-{3-[2-(2,4-Dimethoxyphenyl)vinyl]-5,5-dimethylcyclohex-2-enylidene}malononitrile

T. Kolev, M. Schürmann, D.-C. Kleb, H. Preut and M. Spiteller

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2,2′-Sulfonylbis(2-benzoyl-3-phenyloxirane)

R. V. Krishnakumar, M. S. Nandhini, S. Renuga, S. Natarajan, S. Selvaraj and S. Perumal

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L-Citrullinium perchlorate

B. Sridhar, N. Srinivasan, B. Dalhus and R. K. Rajaram

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(E)-3,5,4′-Trimethoxystilbene

Q. Yin, Y.-M. Shi, H.-M. Liu, C.-B. Li and W.-Q. Zhang

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Kudos

Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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