Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 59| Part 5

ISSN: 2056-9890

May 2003 issue

Highlighted illustration

Cover illustration: 2,2'-Bis(1-ethylbenzimidazol-2-yl)biphenyl adopts a twisted clamshell geometry, in which the imidazole fragments are almost eclipsed and are involved in extensive intramolecular [pi] - [pi] interactions. See Stibrany, Schugar & Potenza [Acta Cryst. E59, o693-o695].

inorganic compounds

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Dipotassium manganese(II) bis(dihydrogendiphosphate) dihydrate, K₂Mn(H₂P₂O₇)₂·2H₂O

A. Alaoui Tahiri, R. Ouarsal, M. Lachkar, P. Y. Zavalij and B. El Bali

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Potassium tetrachlorogallate

M. Gorlov, A. Fischer and L. Kloo

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Dipotassium bis[hexaaquacobalt(II)] decavanadate tetrahydrate

U. Lee, Y.-H. Jung and H.-C. Joo

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Sr₃MgPtO₆

M. D. Smith and H.-C. zur Loye

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Ag_1.49Mn_1.49^IIMn_1.51^III(AsO₄)₃

A. Brahim and H. Amor

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Reinvestigation of β-Li₃TaO₄

D. du Boulay, A. Sakaguchi, K. Suda and N. Ishizawa

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metal-organic compounds

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cis-Diaquabis(quinoline-2-carboxylato-κ²N,O)iron(II)–quinoline-2-carboxylic acid–water (2/1/2)

N. Okabe and Y. Muranishi

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Bis[dicarbonyl(η⁵-cyclopentadienyl)ferrio](N,N-diisobutyldithiocarbamato)tin(II)

B.-H. Chen, Y.-Z. Li, Y.-X. Ma, X.-L. Wu and P.-R. Li

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(trans-Cinnamaldehyde)tris(2,6-diphenylphenoxy)aluminium

W. Clegg, M. R. J. Elsegood, R. Snaith and A. E. H. Wheatley

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Orotato(1,10-phenanthroline)copper(II)

X. Li, R. Cao, W. Bi, D. Sun and M. Hong

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Triaqua(1,10-phenanthroline)sulfatocadmium(II)

X. Li, R. Cao, W. Bi, D. Sun and M. Hong

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Bis[μ-methylenebis(diphenylphosphine)-κ²P:P′]disilver(I) diperchlorate acetonitrile disolvate

Q. Wei, G. Yin and Z. Chen

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Bis[N-n-butyl-N-(3,5-di-tert-butyl-2-hydroxybenzyl)dithiocarbamato-κ²S,S′]zinc(II)

G. Reck and R. Becker

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Bis(tetrabutylammonium) decaiodotetramercurate(II), (Bu₄N)₂[Hg₄I₁₀]

P. Nockemann and G. Meyer

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Di-μ-chloro-bis({[bis(trimethylsilyl)amino]dichlorophosphoraniminato}trichlorotantalum(V))

E. Rivard, A. J. Lough and I. Manners

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Bis(cyanamidonitrato-κN)[tris(3,5-dimethylpyrazole)copper(II)

J. G. Díaz, J. Kožíšek and V. Langer

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Aquabis(quinoline-2-carboxylato-κ²N,O)zinc(II)

N. Okabe and Y. Muranishi

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trans-Diaquabis(isoquinoline-1-carboxylato-κ²N,O)zinc(II) dihydrate

N. Okabe and Y. Muranishi

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catena-Poly[[[tetraaqualanthanum(III)]-di-μ-isoniconitinato-κ²O:O′] nitrate]

L.-Z. Cai, M.-S. Wang, G.-W. Zhou, G.-C. Guo, J.-G. Mao and J.-S. Huang

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A cyano-bridged binuclear Cu–Fe complex based on nitroprusside

X. Peng, H.-Z. Kou, M. Xiong and R.-J. Wang

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Bis(cyclooctatetraenyl)thulium lithium tris(tetrahydrofuran)

G. W. Rabe, M. Zhang-Preße, J. A. Golen and A. L. Rheingold

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One-dimensional chain structure of catena-poly[[[(1,10-phenanthroline)copper(II)]-μ-dicyanamido] perchlorate]

A.-Q. Wu, F.-K. Zheng, L.-Z. Cai, G.-C. Guo, J.-G. Mao and J.-S. Huang

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Aqua(azido)(dimethylglyoximato)(dimethylglyoxime)cobalt(III) monohydrate

Z.-Y. Dong, X.-W. Liu, X.-Q. Wang, R.-J. Wang and G.-Q. Shen

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Bis[aqua(4-chlorobenzoato)silver(I)](Ag—Ag)

H.-L. Zhu, A. Usman, H.-K. Fun and X.-J. Wang

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(Acetonitrile)(6,6′′-dimesityl-2,2′:6′,2′′-terpyridine)copper(I) hexafluorophosphate

A. Onoda, K. Kawakita, T. Okamura, H. Yamamoto and N. Ueyama

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Cp₂Ti(dddse): a well known precursor for Se-containing donors

S. Vincendeau, V. Collière and C. Faulmann

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Tris(8-quinolinolato-κ²N,O)chromium(III) ethanol solvate

D.-X. Li, D.-J. Xu and Y.-Z. Xu

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Bis[1,2-bis(diphenylphosphino)ethane]silver(I) bis(trifluoroacetato)triphenylstannate(IV)

C. F. Chee, K. M. Lo and S. W. Ng

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Dimethanoltetrakis[5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato]manganese(III) hexacyanooctaselenidorhenate(III) tridecahydrate

S.-M. Park, S. Kim, A. J. Lough, S.-J. Kim and Y. Kim

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Bis[2,2′-(2-aminoethylimino)di(ethylammonium)] hexasulfidodistannate(IV) dihydrate

C. Näther, S. Scherb and W. Bensch

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Decacarbonyl(μ₄-2-thiodithiobenzoato- κ⁴C,S,S′,S′′)bis(trimethyl phosphite)tetrafer

E. A. Laifa and N. Benali-Cherif

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Piperazinium hexaaquacobalt(II) disulfate

J.-X. Pan, G.-Y. Yang and Y.-Q. Sun

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Tribromo(tetrahydrofuran)aluminium(III)

S. Scholz, H.-W. Lerner and M. Bolte

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A distorted square-planar Pd^II complex with a shortened Pd—Cl bond induced by the bulky terpyridyl ligand 6,6′′-dimesityl-2,2′:6′,2′′-terpyridine

A. Onoda, K. Kawakita, T. Okamura, H. Yamamoto and N. Ueyama

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Hexaaquacobalt(II) bis(4-hydroxyisophthalate) tetrahydrate

X. Li, W. Bi, Y. Daqiang, Z. Youfu and R. Cao

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Tris(phenanthroline-κ²N,N′)cobalt(II) fumarate fumaric acid tetrahydrate

Y. Liu, D.-J. Xu and C.-H. Hung

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Tris(2,2′-bipyridine)nickel(II) diperchlorate

Y. Zhou, X. Li, Y. Xu, R. Cao and M. Hong

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Chloro(η⁶-p-cymene)(diethyldithiocarbamato-κ²S,S)ruthenium(II)

W.-R. Yao, Z.-H. Liu and Q.-F. Zhang

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organic compounds

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3-Acetyl-2-hydroxy-2-methylchromene

M. Yogavel, D. Velmurugan, K. Sekar, H. Schenk, J. Fraanje, R. Peschar, S. Srinivasan, PR. Athappan and Z. A. Rafi

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(R)-2,2′-Bis{[5-(2-phenylethynyl)thienyl]ethynyl}-1,1′-binaphthyl

S. Löhr, M. Yonemura, A. Orita, N. Imai, H. Akashi and J. Otera

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1-(Diphenylphosphino)-4-(diphenylphosphinoyl)butane

M. L. Williams, P. C. Healy, N. K. Loh, S. P. C. Dunstan and G. Smith

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O,O′-(R)-(1,1′-Dinaphthyl-2,2′-diyl) N-benzyl-N-(2-pyridyl)phosphoramidite

L. Liang, R. Guo and Z. Zhou

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3-Carbazoyl-5-methylpyridazin-6(1H)-one

X.-G. Cheng, Y.-Z. Li, X.-G. Fu, L. Cao and Z.-D. Hu

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1-Chloroacetyl-2,4-diphenyl-2,3-dihydro-1H-1,5-benzodiazepine

J. N. Low, J. Cobo, B. Insuasty, H. Insuasty, E. Díaz and H. Escobar

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3-(Anthracen-9-ylmethylene)-2,4-dimethyl-3H-benzo[1,5]diazepine

A. Megzari, B. El Bali, T. Janati, A. Kerbal, N. Benlarbi, T. Benhadda, M. Mimouni and M. Bolte

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2-{[(2-Hydroxyphenyl)methyl]methylamino}-1-phenylpropan-1-ol

F. Yuan, Y.-Z. Li, C.-J. Zhu, Y. Pan and L.-L. Xu

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Ethyl 2-phenyl-3-(pyridin-2-yl)acrylate

Y. Li, A. Usman, H.-K. Fun and J.-H. Xu

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N-(1,2-Diphenyl-2-oxoethylidene)benzenamine N-oxide

A. Usman, H.-K. Fun, H.-Y. Hu and J.-H. Xu

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5-(1,3-Benzodioxol-5-yl)-3-methyl-1,7-diphenyl-1,6,7,8-tetrahydropyrazolo[3,4-b][1,4]diazepine

J. N. Low, B. Insuasty, M. Mosquera and J. Cobo

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3-(6-Benzoyl-2-oxo-2,3-dihydro-2-benzothiazol-3-yl)propanoic acid

A. Aydın, T. Önkol, C. Arıcı, M. Akkurt, M. F. Şahín and D. Ülkü

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Tribromoacetic acid

P. G. Jones and V. Lozano

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3-Phenyl-4a,5-dihydro-1,2,4-triazolo[3,4-b][1,3]benzothiazine

P. G. Aravindan, V. Rajakannan, M. Yogavel, D. Velmurugan, A. Senthilvelan and I.-H. Suh

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[(2-Methoxyanilino)methylene]malononitrile

V. N. Nesterov, E. A. Viltchinskaia and S. V. Nesterova

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Benzyl N-[1-(thiophen-2-yl)ethylidene)]hydrazinecarbodithioate

M.-H.E. Chan, K. A. Crouse, M. T. H. Tarafder and B. M. Yamin

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Methyl 2,5-dihydroxybenzoate

C. L. Brown, J. F. Heagney, D. J. Young and P. C. Healy

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A second polymorph of 3,5-dibromopyridinium bromide

P. G. Jones and V. Lozano

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1-(12-Benzoyl-10-oxa-12-azatetracyclo[6.3.1.0^2,7.0^9,11]dodeca-2,4,6-trien-1-yl)ethan-1-one

S. Öztürk, M. Akkurt, E. Tepe, F. W. Heinemann, A. Altundaş and Y. Kara

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Dasypogalactone–methanol–water (1/2/1)

U. Flörke, W. P. Suwarso, R. L. Gani, K. Krohn and S. Wang

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N′-(4-Chlorobenzoyl)-N,N-diphenylthiourea

H. Arslan, U. Flörke and N. Külcü

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6,6,8-Triméthyl-6,7-dihydro-5H-tétrazolo[1,5-a]azepine

M. Dakir, A. Auhmani, M. Akssira, A. Benharref and M. Pierrot

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(R,R)-(−)-trans-1,4-Dioxaspiro[4,5]decane-2,3-diylbis(diphenylmethanol) N-allyl-N-propyl-3-oxo-1-cyclohexenecarboxamide (2/1 inclusion compound)

S. Ohba and H. Miyamoto

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Diprotonated adeninium diperchlorate hydrate at 120 K

L. Bendjeddou, A. Cherouana, S. Dahaoui, N. Benali-Cherif and C. Lecomte

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Bis(4-maleimidophenyl)methane

A. Usman, H.-K. Fun, H.-L. Zhu and G. Ke

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Anthracene-9-carbaldehyde hydrazone

J. Urban, J. Ludvík, J. Fábry and I. Císařová

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(Z)-Azulene-1-carboxaldehyde oxime

M. Kedziorek, K. Hafner and H. J. Lindner

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3,3,6,6-Tetramethyl-9-(4-pyridyl)-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione monohydrate

P. G. Aravindan, M. Yogavel, D. Velmurugan, P. Murugan, S. Shanmuga Sundara Raj and H.-K. Fun

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N,N-Dimethyl-N'-phenylformamidinium perchlorate

M. Yogavel, P. G. Aravindan, D. Velmurugan, P. T. Perumal, S. Shanmuga Sundara Raj and H.-K. Fun

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4,4,4-Trifluoro-trans-2-butenoic acid

A. T. Hulme and D. J. Watkin

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[6a,16b]-cis-7,7-Dimethyl-6,6a,7,16b-tetrahydrochromeno[4′,3′:3,4]pyrano[3,2-c]-α-naphthocoumarin

R. Krishna, S. Selvanayagam, M. Yogavel, D. Velmurugan and S. Manikandan

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4,11-Bis(4-chlorophenyl)-3,10-bis(2,6-dichlorophenyl)-1,8-dioxa-2,9-diazadispiro[4.1.4.2]trideca-2,9-dien-6-one–chloroform–methanol (1/1/0.75)

X.-F. Li, Y.-Q. Feng and H. Xiao-Fen

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2-[2-(5-Ethoxy-4-methoxy-2-nitrophenyl)vinyl]-1H-indole

R. Sankaranarayanan, M. Yogavel, D. Velmurugan, P. C. Srinivasan, S. Shanmuga Sundara Raj and H.-K. Fun

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4-(4-Chlorophenyl)-3-(2,6-dichlorophenyl)-1,7-dioxa-2-azaspiro[4.4]non-2-en-6-one

X.-F. Li, Y.-Q. Feng and M. Xu

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3-Benzyl-7,7-dimethyl-9-phenyl-1-thia-3-aza-7-azoniaspiro[4.4]nonane-2,4-dione iodide

X.-F. Li, Y.-Q. Feng, X.-D. You and M. Xu

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{[N-Benzyl-N-(2-pyridyl)amino]methylene}diphenylphosphine oxide

D.-J. Cui, X.-S. Zeng, X.-B. Leng, F.-B. Xu and Z.-Z. Zhang

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3-Indolylformaldehyde isonicotinoylhydrazone methanol solvate

X.-S. Tai, X.-H. Yin, M.-Y. Tan and Y.-Z. Li

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N,N′-Disuccinimidyl carbonate

M. Simon, C. Csunderlik, P. G. Jones, I. Neda and A. Tarta-Micle

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N,N′-Carbonyldisuccinimide

M. Simon, C. Csunderlik, P. G. Jones, I. Neda and A. Tarta-Micle

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A second polymorph of bis(o-nitrophenyl) carbonate

M. Simon, C. Csunderlik, P. G. Jones, I. Neda and A. K. Fischer

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Bis(p-nitrophenyl) carbonate–benzene (3/1)

M. Simon, C. Csunderlik, P. G. Jones, I. Neda and A. K. Fischer

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2,2′-Bis(1-ethylbenzimidazol-2-yl)biphenyl

R. T. Stibrany, H. J. Schugar and J. A. Potenza

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10-[2-(4-Acetylpiperzin-1-yl)ethyl]-9-(4-chlorophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-2H,5H-acridine-1,8-dione

P. R. Seshadri, M. Yogavel, T. J. Rajan, D. Velmurugan, S. Shanmuga Sundara Raj and H.-K. Fun

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Fenofibrate

R. F. Henry, G. Z. Zhang, Y. Gao and I. S. Buckner

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6,7-Dimethyl-3,4,4a,7,8,8a-hexahydroisochromen-1-one

N. Kayal and V. McKee

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3-[2-(2,4-Dichlorophenyl)vinyl]-2-methyl-1-phenylsulfonyl-1H-indole

V. K. Ganesh, M. Yogavel, D. Velmurugan, S. Shanmuga Sundara Raj, H.-K. Fun, S. Kannadasan and P. C. Srinivasan

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(1R,2S)-1-(6-Methoxy-2-naphthyl)-3-methyl-2-(p-methylphenylsulfonylamino)-butan-1-ol

X. Li, X. Jia and Z. Zhou

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1,14-Dibromotetradecane

K. Uno and N. Nakamura

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1′'-Benzyl-5′′-benzylidene-1′-methyl-4′-phenyl-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-3′′-piperidine-2(3H),3′′-dione

X.-F. Li, Y.-Q. Feng, X.-F. Hu and M. Xu

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1,1-Dichloro-3-méthylthio-1a-phényl-1,1a,2,9-tétrahydroaziridino[2,1-d][1,5]benzodiazépine

S. El Hazazi, S. Baouid, A. Hasnaoui and M. Pierrot

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4,11-Bis(4-chlorophenyl)-3,10-bis(2,6-dichlorophenyl)-1,8-dioxa-2,9-diazadispiro[4.1.4.4]pentadeca-2,9-dien-6-one

X.-F. Li, Y.-Q. Feng, H. Xiao-Fen and X. Mian

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4-Acetamido-2-methoxy-5-[3-(phenylsulfanyl)indole-2-carbonyl]benzoic acid

V. Rajakannan, S. Selvanayagam, M. Yogavel, L. Govindasamy, D. Velmurugan, S. Shanmuga Sundara Raj, H.-K. Fun and P. C. Srinivasan

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4′,5a′-Diphenyl-10-oxospiro[phenanthrene[9,2′]oxeto[5,4-b]oxazole]

L. Wang, A. Usman, H.-K. Fun, Y. Zhang and J.-H. Xu

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2-Cyano-N-(2-hydroxyphenyl)acetamide

J. A. L. C. Resende, S. Santos Jr, J. Ellena and S. Guilardi

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Zwitterionic 2-(methylamino)ethanesulfonic acid

J. A. Kalaitzis, P. de. Almeida Leone, R. J. Quinn and P. C. Healy

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Tetrahydro-2,6,6-trimethyl-1,4-pyran-2,5-dicarboxylic acid (cineolic acid)

J. C. Barnes and T. J. R. Weakley

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Ethylenediammonium bis(2-carboxylato-3,4,5,6-tetrahydro-2,6,6-trimethyl-2H-pyran-5-carboxylic acid) dihydrate [ethylenediammonium bis(hydrogen cineolate) dihydrate]

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1,7-Dihydro-1,4,7,10-tetraazacyclododecanephosphine oxide iodide

B. Twamley, O. D. Gupta and J. M. Shreeve

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Methyl (3SR,4RS)-3-benzyl-4-hydroxy-2-oxopyrrolidine-3-carboxylate

A. S. Hamzah, Z. Shaameri, I. A. Adziz and B. M. Yamin

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Ethyl N-(2-butyl-1,3-dioxo-2,3-dihydro-1H-isoindol-5-yl)carbamate

D.-X. Shi, Y.-Q. Feng and X.-F. Li

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Kudos

Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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Editorial Advisory Board

S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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