Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 59| Part 10

ISSN: 2056-9890

October 2003 issue

Highlighted illustration

Cover illustration: The 1:1 flunixin-meglumine salt is a veterinary medicine. The two components are held together in layers in the crystal structure by hydrogen bonds as well as ionic interactions. See Cao, Sun & Pan [Acta Cryst. E59, o1471-o1473].

inorganic compounds

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Ammonium iron(III) molybdate

X. Wu, H. Zhang, C. Huang, X. Huang, Q. Sun and Z. Lin

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Cs₄Ge₂S₈

Y.-D. Wu, C. Näther and W. Bensch

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metal-organic compounds

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(4,4′-Dimethyl-2,2′-bipyridine)chloro-(2,2′:6′,2′′-terpyridine)-iridium(III) hexafluorophosphate

N. Yoshikawa, J. Sakamoto, N. Kanehisa, Y. Kai, T. Matsumura-Inoue, H. Takashima and K. Tsukahara

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trans-μ-(2,5-Dioctyl-1,4-phenylene)diethynyl-bis[phenylbis(triethylphosphine)platinum(II)]

M. S. Khan, M. K. Al-Suti, M. F. Mahon, L. Male and P. R. Raithby

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Cobalt diacetate tetrahydrate

A. N. Sobolev, E. B. Miminoshvili, K. E. Miminoshvili and T. N. Sakvarelidze

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(Diethyleneglycol dimethyl ether)tris(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)praseodymium(III)

J. Plakatouras, C. Kavounis and C. Cardin

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Tetraaqua-1,2,4,5-benzenetetracarboxylato(pyrazine)dicobalt(II) dihydrate

S.-Y. Yang, L.-S. Long, R.-B. Huang, L.-S. Zheng and S. W. Ng

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Dibenzoato-di(2-aminopyridine)nickel(II)

H.-L. Zhu, S.-C. Shao, J.-L. Ma, X.-Y. Qiu, L. Sun and S. Yang

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catena-Poly[di-μ₂-chloro(1,10-phenanthroline)cadmium(II)]

H.-B. Chen, Z.-H. Zhou, H.-L. Wan and S. W. Ng

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catena-Poly[μ-trifluoroacetato-O:O′-dimethyl-4-fluorophenyltin(IV)]

M. M. Amini, S. H. Abadi, M. Mirzaee, S.-Y. Yang and S. W. Ng

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catena-[μ₆-1,2,4,5-Benzenetetracarboxylato-tetraaqua-dinickel(II)] dihydrate

S.-Y. Yang, L.-S. Long, R.-B. Huang, L.-S. Zheng and S. W. Ng

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catena-(Bis(μ₂-1,3-bis(4-pyridyl)propane-N,N′)-diaqua-cobalt(II)) dinitrate 1,3-bis(4-pyridyl)propane monohydrate

K. J. Nordell, J. D. Hammond and M. D. Smith

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1-(4-Fluorobenzyl)pyridinium bis(maleonitriledithiolato)platinate(III)

X. Ren, J. Xie and Q. Meng

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Polymeric diaqua-8-hydroxyquinolinyl-5-sulfonatozinc(II)

H.-Y. Rao, J. Tao and S. W. Ng

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(2RS,5SR)-2,5-Diferrocenyl-1,6-dibenzoyl-3,4-dithiahexane

Q.-B. Song, Y.-Z. Li, Y.-M. Liang and Y.-X. Ma

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{2,6-Bis[(4R)-(+)-4-isopropyl-4,5-dihydro-1,3-oxazol-2-yl]pyridine-κ³N}dichlorozinc(II)

F. B. Panosyan, A. J. Lough and J. Chin

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Hexaaquacobalt(II) (μ₂-triethylenetetraminehexaacetato)diaquadicobalt(II) tetrahydrate

L.-J. Song, J. Zhang, Z.-R. Tang, W.-G. Wang and Z.-F. Ju

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Bis(diisopropylammonium) dimethyldioxalatostannate

T. Xu, S.-Y. Yang, Z.-X. Xie and S. W. Ng

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Bis(diisopropylammonium) diphenyldioxalatostannate(IV)

T. Xu, S.-Y. Yang, Z.-X. Xie and S. W. Ng

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Bis[1,1,3,3-tetramethyl-1,3-bis(dichloroacetato)distannoxane]

M. M. Amini, S. H. Abadi, M. Mirzaee, S.-Y. Yang and S. W. Ng

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Bis(N-(2-(2-hydroxyethylamino)ethyl)salicylideneimine)cobalt(III) chloride

H.-L. Zhu, Y.-S. Lin, F.-J. Meng, Y. Zou and D.-Q. Wang

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(1,4,7,11,14,17-Hexathia-9,9,19,19-tetrahydroxymethylcycloicosane)silver(I) nitrate

M. Fainerman-Melnikova, L. F. Lindoy, J. C. McMurtrie and W. N. Setzer

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trans-Diaquabis(isoquinoline-1-carboxylato-κ²N,O)iron(II) dihydrate

Y. Muranishi and N. Okabe

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Bis(2,2′-diamino-4,4′-bi-1,3-thiazole-N,N′)(dichloro)cobalt(II) dihydrate

J.-G. Liu, D.-J. Xu and Y.-Z. Xu

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Bis(2,2-bipyridine N,N′-dioxide-κ²O,O′)bis(dicyanamido-κN¹)copper(II)

G. A. van Albada, I. Mutikainen, U. Turpeinen and J. Reedijk

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Tris(O-methyl dithiocarbonato)cobalt(III)

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Bis[3-(4-methylcoumarinyl-7-oxy)-μ-methoxy-1,1,3,3-tetramethyldistannoxane]

Y. Zhang, L. E. Khoo, T. Y. Tou and S. W. Ng

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trans-Bis(isoquinoline-3-carboxylato-κ²N,O)bis(methanol-κO)iron(II)

N. Okabe and Y. Muranishi

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A nickel(II) fumarate complex with o-phenanthroline

J.-F. Ma, J. Yang and J.-F. Liu

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Diaquabis(nitrato-κO)bis(4,7-dihydro-1,2,4-triazolo[1,5-a]pyrimidin-7-one-κN³)copper(II)

M. Abul-Haj, M. Quirós and J. M. Salas

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catena-Poly[[silver(I)-μ-1,2-diaminoethane] hexafluoroarsenate]

H.-L. Zhu, Z.-Y. Sun, N.-N. Rong, B. Zhang, M. Zhang and Y. Li

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Tetraaqua(1,10-phenanthroline-N,N′)manganese(II) dinitrate

W. Wang, C. Ma, F. Chen, C. Chen and Q. Liu

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μ-Hydroxo-bis[(4,4′-dimethyl-2,2′-bipyridine)tricarbonylrhenium(I)] perrhenate acetone hemisolvate

D. H. Gibson, M. S. Mashuta and X. Yin

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Dicarbonyl(η⁵-cyclopentadienyl)iodoiron(II)

M. Zeller, E. Lazich and A. D. Hunter

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Dichloro{methyl 4-[(1,4,7,10-tetraazacyclododec-1-yl)methyl]benzoate}cobalt(III) methylsulfate

J. R. Deschamps, D. A. Knight, E. R. Goldman, J. B. Delehanty and E. L. Chang

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μ₄-Oxo-hexa-μ₂-chloro-tetrakis[(benzimidazole-κN)copper(II)] ethanol disolvate: a reformulation

Y.-Q. Zhang, D.-J. Xu and J.-R. Su

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On the number of uncoordinated water molecules in the open-framework coordination compound, bis(1,2,4,5-benzenetetracarboxylato)dihydroxytetraaquapentacobalt(II) x-hydrate, and the crystal structure of the isomorphous decahydrated zinc(II) analog

S.-Y. Yang, L.-S. Long, R.-B. Huang, L.-S. Zheng and S. W. Ng

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Hexaaquanickel(II) dichloride bis(hexamethylenetetramine) tetrahydrate

H.-L. Zhu, Z.-L. You, Y. Qu, W.-S. Liu, M.-Y. Tan and J.-L. Ma

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Triaqua(4-hydroxypyridine-2,6-dicarboxylato-κ³N,O,O′)zinc(II)–acetonitrile–water(1/0.25/1)

G.-W. Zhou, G.-C. Guo, B. Liu, M.-S. Wang, L.-Z. Cai, G.-H. Guo and J.-S. Huang

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Trichloro(diethyl ether-κO)aluminium(III) from a twinned crystal

L. Hubener, H.-W. Lerner and M. Bolte

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Dicarbonyl(η⁵-methylcyclopentadienyl){η²-[tricarbonyl(η⁶-styrene)chromium(0)]}manganese(I)

B. Crocock, C. Long, M. Lyons and R. A. Howie

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Hexakis(dimethyl sulfoxide-κO)aluminium(III) trichloride

D. Boström, M. Clausén and M. Sandström

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(1,2-Benzenediolato-κ²O,O′)(1,10-phenanthroline-κ²N,N′)palladium(II) dihydrate

N. Okabe, Y. Muranishi and T. Aziyama

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Dichlorobis(tetrahydrofuran)(N,N′-di-tert-butylethane-1,2-diamine)vanadium(II)

A. C. Niedwieski, G. J. Leigh, T. Hasegawa and F. S. Nunes

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Tris(μ-1,6-diaminohexane)diterephthalatotetrasilver(I) dihydrate

H.-L. Zhu, Z.-G. Wang, Y.-S. Lin, Y. Zou, L.-L. Tang and S.-C. Shao

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catena-Poly[[diaquabis(1H-benzimidazole-κN³)cobalt(II)]-μ-succinato-κO]

Y.-H. Xue, Y. Liu and D.-J. Xu

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A two-dimensional coordination polymer, μ-1,3-benzenedicarboxylato-μ-ethylenediaminezinc(II) trihydrate

Y.-Q. Jiang, Z.-X. Xie and S. W. Ng

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[N,N′-Ethylenebis(salicylideneiminato)]nickel(II) dimethylformamide solvate

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Bis(1,4,7-trithiacyclononane-κ³S,S′,S′′)iron(II) bis(perchlorate)

T. W. Green, J. A. Krause Bauer and W. B. Connick

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cis-Bis(3,5-di-tert-butyl-2-hydroxybenzoato-κ²O,O′)bis(ethanol)zinc(II)

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trans-Bis(benzylamine)dichloropalladium(II)

C. Sui-Seng and D. Zargarian

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organic compounds

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2′-Deoxy-2′,2′-difluorocytidine monohydrochloride (Gemcitabine hydrochloride)

A. Sivalakshmidevi, K. Vyas, G. Om Reddy, S. D. V. N. Sivaram, P. V. Swamy, R. Puranik and P. Sairam

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4′-(p-Methoxyphenyl)-1′-methyl-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-1′′-cyclopentane-2(3H),2′′-dione

M. M. Govind, S. Selvanayagam, D. Velmurugan, K. Ravikumar, G. Sridhar and R. Raghunathan

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Tetrathiafulvalenium 4-oxo-2,2,6,6-tetramethylpiperidin-1-sulfate

H. Akutsu, J. Yamada and S. Nakatsuji

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2,6-Diaminopyridinium bromide monohydrate

S. F. Haddad and R. H. Al-Far

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3,3,6,6-Tetramethyl-9-(3,4-methylenedioxylphenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione

Y. Li, X. Wang, D. Shi, B. Du and S. Tu

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(S,S)-1,2-Bis(1-methylbenzimidazol-2-yl)-1′,2′-bis(methoxy)ethane

R. T. Stibrany, H. J. Schugar and J. A. Potenza

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3,3′-(1,4-Naphthalenedimethylene)bis(1-ethylimidazolium) diiodide methanol solvate

R.-Y. Zou, F.-B. Xu, Q.-S. Li and Z.-Z. Zhang

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2,5-Dihydro-2,5-dimethyl-3,6-diphenylpyrrolo[3,4-c]pyrrole-1,4-(diylidene)bis(cyanamide) chloroform disolvate

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Guanidinium 8-hydroxy-7-iodoquinoline-5-sulfonate monohydrate

G. Smith, U. D. Wermuth and P. C. Healy

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Spiro-[2-3′]oxindole-spiro-[3-3′′]oxindole-4[p-methylbenzyl]pyrrolidizine

P. R. Seshadri, S. Selvanayagam, D. Velmurugan, K. Ravikumar, A. R. Sureshbabu and R. Raghunathan

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N,N-(2-benzothiazole)(2-pyridylmethyl)amine

Z.-F. Chen, Y.-Z. Tang, S.-M. Shi, X.-W. Wang, H. Liang and K.-B. Yu

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(Z)-2-Thiophen-3-ylmethylene-1-aza-bicyclo[2.2.2]octan-3-one

V. N. Sonar, S. Parkin and P. A. Crooks

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1-Methyl-spiro[2.3′]oxindole-spiro[3.2′′]5′′,6′′-dihydroimidazo[2′′,1′′-b]thiazol-3′′-one-4-(2-benzo[1,3]dioxol-5-yl)pyrrolidine

X.-F. Li, Y.-Q. Feng, B. Gao and H.-L. Chen

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1-(2,4-Dihydroxy-3,5-dimethylphenyl)-ethanone (Clavatol)

S.-Y. Li, J.-F. Wang, Z.-H. Zheng, Q.-Y. Xu, Y.-J. Huang, Y.-F. Zhao and W.-J. Su

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The complex of flunixin and meglumine

X.-J. Cao, C.-R. Sun and Y.-J. Pan

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2-Amino-4-(2-chlorophenyl)-3-ethoxycarbonyl-4H-benzo[f]chromene

Q. Zhuang, D. Shi and X. Wang

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(+)-(1S,2S,4S,4aR,5R,6S,9S,10S)-4-Benzyloxy-9,10-(carbonyldioxy)-1-methoxymethoxy-4a,6,8,8-tetramethyl-7-methylenedodecahydro-6,9-ethanobenzocyclooctene-5-ol

S. Ohba, A. Chinen, Y. Matsumoto and N. Chida

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2-(1-Benzyl-1H-indol-3-ylmethylene)-1-azabicyclo[2.2.2]octan-3-one

V. N. Sonar, S. Parkin and P. A. Crooks

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4-(2-Indanoxy)phthalonitrile

Ş. Işık, Y. Köysal, N. Akdemir, K. Cihan and E. Ağar

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A new refinement of the orthorhombic polymorph of acetamide

J. W. Bats, M. C. Haberecht and M. Wagner

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4(R)-(N-Benzoylamino)-5(R)-methyltetrahydrofuran-2-one: an L-β-threonine analogue

M. Doi and A. Asano

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1,3-Dibenzylthymine

J.-C. Ding, M.-C. Liu, H.-P. Xiao and M.-L. Hu

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4,8-Bis[(4-butylphenyl)amino]-1,5-naphthalenedione

J. Mizuguchi and H. Shiozaki

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2,6-Bis(butylamino)-4,8-dihydroxy-1,5-naphthalenedione

J. Mizuguchi and H. Shiozaki

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4-Bromo-2-(2-pyridylmethyliminomethyl)phenol

Y. Zhang, L. E. Khoo and S. W. Ng

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(–)-(1S,2S)-N,N′-Bis(salicylidene)-1,2-diphenyl-1,2-ethanediamine

I. V. Korendovych and E. V. Rybak-Akimova

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Ethyl 2-amino-4-(4-fluorophenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-benzo[b]pyran-3-carboxylate

D. Shi, S. Zhang, X. Wang and Q. Zhuang

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Redetermination of skimmianine: a new inhibitor against the Leishmania APRT enzyme

H. B. Napolitano, M. Silva, J. Ellena, W. C. Rocha, P. C. Vieira, O. H. Thiemann and G. Oliva

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Redetermination and comparative structural study of isopimpinellin: a new inhibitor against the Leishmania APRT enzyme

H. B. Napolitano, M. Silva, J. Ellena, W. C. Rocha, P. C. Vieira, O. H. Thiemann and G. Oliva

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3-Isopropylamino-7-nitro-1,4,2-benzodithiazine 1,1-dioxide

L. Dupont, F. Somers, P. D. Tullio and B. Pirotte

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1,3-Dimethoxy-5-(triphenylmethylthio)benzene

C. M. L. Vande Velde, H. J. Geise and F. Blockhuys

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tert-Butyl 6-O-benzyl-2,2-dichloro-2,5-dideoxy-4-O-methyl-α-D-ribo-oct-3-pyranulosonate

G. J. Gainsford and P. C. Tyler

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3,7,8-Trihydroxy-3-methyl-10-oxo-4,10-dihydro-1H,3H-pyrano[4,3-b]chromene-9-carboxylic acid (fulvic acid) methanol 0.75-solvate

J.-F. Wang, M.-J. Fang, H.-Q. Huang, G.-L. Li, W.-J. Su and Y.-F. Zhao

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Swietenine

K. A. Solomon, R. Malathi, S. S. Rajan, S. Narasimhan and M. Nethaji

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Allyl 4-hydroxybenzoate

A. M. Herrera, S. Bernès and D. López

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1-β-Hydroxycorticosterone hemihydrate

R. S. V. S. Gadepalli, J. M. Rimoldi and F. R. Fronczek

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3,5-Diphenyl-4-(3,4,5-trimethoxybenzylideneamino)-4H-1,2,4-triazole

Ş. Atalay, M. Yavuz, O. Bekircan, A. Ağar and S. Şaşmaz

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3,5-Di-tert-butyl-2-hydroxybenzoic acid

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N-(3-Chloro-4-methoxyphenyl)-N′-hydroxy-2-oxo-2-phenylacetamidine

S. Soylu, M. Taş, Ö. Andaç, H. Batı, N. Çalışkan and O. Büyükgüngör

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3-Phenyl-5-p-tolyl-4-(3,4,5-trimethoxybenzylamino)-4H-1,2,4-triazole

Ş. Işık, B. C. Olcay, A. Ağar and S. Şaşmaz

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2,6-Bis(4-methylphenyl)-3-phenylpiperidin-4-one

M. S. Nandhini, M. Srinivasan, R. V. Krishnakumar, A. Mostad, S. Perumal, S. Selvaraj and S. Natarajan

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(1RS,3RS)-2-Methoxymethyl-1,3-dithiolane 1,3-dioxide

Ö. Özcan, Z. Gültekin, W. Frey and T. Hökelek

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2,4,6-Trimethyl-1,3,5-tris(phenoxymethyl)benzene

D. J. Bray, L. F. Lindoy and J. C. McMurtrie

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2,4-Di(butylureido)-6-methyl-s-triazine

H. Kooijman, A. L. Spek, F. H. Beijer, R. P. Sijbesma and E. W. Meijer

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Ethyl 4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)benzoate

Vasu, K. A. Nirmala, D. Chopra and M. Vishwas

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(1R,5R,6S,7R)-6,7-Dihydroxy-6-hydroxymethyl-2-oxabicyclo[3.2.0]heptan-3-one

K. Blann, D. B. G. Williams, A. Roodt and A. Muller

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Ethyl (O–B)-5-(difluoroboryloxy)tricyclo[4.3.1.1^3,8]undecane-4-carboxylate

G. Argay, A. Kálmán, G. Bernáth and Zs. Cs. Gyarmati

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29H,31H-Tetrabenzo[b,g,l,q]porphin

S. Aramaki and J. Mizuguchi

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2′-Benzoyl-1′,2,2′,3,4′,5′,6′,6a′-octahydro-1H-indan-2-spiro-3′-(3′H-pyrrolizine)-1′-spiro-3′′-1H-indoline-1,2′′,3-trione

P. R. Seshadri, S. Selvanayagam, D. Velmurugan, K. Ravikumar, A. R. Sureshbabu and R. Raghunathan

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3-Amino-1-(4-fluorophenyl)-3a,3b,6,7-tetrahydrobenz[4,5]indene-2-carbonitrile

D. Shi, L. Rong, J. Wang, X. Wang and H. Hu

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C—Halogen⋯π interactions in 4-chloro-2-(9-ethylcarbazol-3-yl)-1,2-dihydroquinoline-1-carbaldehyde

P. G. Aravindan, S. Selvanayagam, D. Velmurugan, K. Ravikumar, R. Nagarajan and P. T. Perumal

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6,22-Dioxaparazylenyl 2,10,18,26-tetrathia-33,35 diazapentacyclo[27.3.1.1^4,8.1^12,16.1^20,24]hexatriconta-4,6,8(36),12,14,16(35),20,22,24(34),28,30,32-dodecaene

S. Bhaskaran, S. Selvanayagam, V. Rajakannan, D. Velmurugan, S. Narasingarao, M. Dhanasekaran, P. Rajakumar and M.-J. Kim

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Isopropyl 2-methyl-4-(3-nitrophenyl)-5,7-dioxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,4-b]pyridine-3-carboxylate

V. Vrábel, Š. Marchalín and J. Kožišek

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2-Benzoyl-3-cyclohexyl-4-(p-methoxyphenyl)-5-phenylpyrrolidine-3-spiro-3′-chroman-4′-one

G. Usha, S. Selvanayagam, M. Yogavel, D. Velmurugan, A. Amalraj, R. Raghunathan, S. Shanmuga Sundara Raj and H.-K. Fun

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3-(5,7-Dimethoxy-2,2-dimethyl-2H-benzo[b]pyran-6-yl)propionic acid: a potential inhibitor against Leishmania

M. Silva, H. B. Napolitano, J. Ellena, W. C. Rocha, P. C. Vieira, G. Oliva and O. H. Thiemann

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Methyl {2-[4-ethyl-1-(tolylsulfonyl)-2,3-dihydropyrrol-3-yl]ethyl}benzoate

Y.-M. Hu, Y.-Z. Li, J. Zhou, H.-W. Hu and Y. Pan

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N—H⋯O=C hydrogen bonding and O⋯O=C repulsive interactions in tert-butoxycarbonyl-L-leucyl-L-alanine ethyl ester (Boc-L-Leu-L-Ala-OEt)

H. Oku, K. Yamada and R. Katakai

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4-Ammonio-1-hydroxy-2,2,6,6-tetramethylpiperidin-1-ium dichloride monohydrate

T. Q. Hu, B. O. Patrick, D. A. Osmond and B. R. James

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2-tert-Butyl-4-methyl-6-(1-piperidiniomethyl)phenol bromide

M. Du and X.-J. Zhao

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