Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 59| Part 12

ISSN: 2056-9890

December 2003 issue

Highlighted illustration

Cover illustration: Although this molecule could have twofold rotation symmetry, it actually crystallizes with four complete molecules in the asymmetric unit. Such a situation with Z' = 4 is unusual when the structure shows no obvious pseudosymmetry. See Lu, Liu, Zou, Xu, Wang, Chen & Huang [Acta Cryst. E59, o1960-o1961].

inorganic compounds

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Diammonium tetrathiocyanatocobaltate(II) tetrahydrate

S. Becker, H.-W. Lerner and M. Bolte

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Redetermination of Te₆[AsF₆]₄·2SO₂ at 125 K

J. Beck and F. Steden

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LiMnVO₄

M. Sugahara, A. Yoshiasa, T. Yamanaka and H. Takei

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α-Cs₂Cr₃O₁₀

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metal-organic compounds

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Bis{N′-[(E)-amino(imino)methyl]morpholinocarboximidamido}copper(II)

L. P. Lu and M. L. Zhu

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Hexakis(1H-imidazole-κN³)cobalt(II) dichloride tetrahydrate

H.-L. Zhu, S. Yang, X.-Y. Qiu, Z.-D. Xiong, Z.-L. You and D.-Q. Wang

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A new polymorph of [(S)-(−)-2-aminomethyl-1-ethylpyrrolidine-κ²N,N′](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate

M. D. Jones, F. A. Almeida Paz, J. E. Davies, B. F. G. Johnson and J. Klinowski

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Redetermination of bis(dimethylglyoximato-κ²N,N′)nickel(II)

D.-X. Li, D.-J. Xu and Y.-Z. Xu

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Bis(2,2′-diamino-4,4′-bi-1,3-thiazole-κ²N,N′)(phthalato-κ²O,O′)nickel(II) 3.5-hydrate

B.-X. Liu and D.-J. Xu

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(1,4,7,10,13-Pentamethyl-1,4,7,10,13-pentaazacyclopentadecane-κ⁵N)cobalt(II) perchlorate

F. Zhang, J.-R. Zhang, D.-L. Deng and R. Hage

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(η⁸-Cyclooctatetraene)(2,2′′,4,4′′,6,6′′-hexamethyl-m-terphenyl-κC^2′)(tetrahydrofuran-κO)thulium(III)

G. W. Rabe, M. Zhang-Preße, J. A. Golen and A. L. Rheingold

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catena-Poly[[(pyridine-κN)copper(II)]-μ-N-salicylideneglycinato-κ⁴O,N,O′:O′]

R. J. Butcher, G. M. Mockler and O. McKern

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Trichloro(2,6-di-2-pyridylpyridine-κ³N)indium(III)

R. J. Butcher, C. George, N. Muratore and A. P. Purdy

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A silver–iodine chain complex: catena-poly[anilinium [silver(I)-di-μ-iodo]], {[PhNH₃][AgI₂]}_n

N. W. Alcock, S. J. Archibald and D. H. Busch

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A new polymorph of μ-bis(diphenylphosphino)methane-κ²P:P′-bis[chlorogold(I)]

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1-(2-Bromobenzyl)pyridinium bis(maleodinitriledithiolato)nickelate(III)

X.-M. Ren, J.-L. Xie, Y.-Z. Li and Q.-J. Meng

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(Dimethyl sulfoxide-κS)bis[2′-(3-methylthiophen-2-ylmethylene)furan-2-carbohydrazido]zinc(II)

H. Ali, S. R. S. Omar, M. S. M. Yusof and B. M. Yamin

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Di-μ-trans-2-butenoato-κ³O,O,O′-di-μ-trans-2-butenoato-κ²O,O′-bis[(trans-2-butenoato-κ²O,O′)(1,10-phenanthroline-κ²N,N′)dysprosium(III)] dihydrate

R. Baggio, M. Perec and M. T. Garland

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Hexaaquabis(dicyanoguanidine)terbium(III) trichloride

W. Liao, C. Hu and R. Dronskowski

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Poly[diaquabis(3-pyridylpropionato)copper(II)]

L. A. Borkowski and C. L. Cahill

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Hexaaquanickel(II) dichromate bis(hexamethylenetetramine) monohydrate

P. Dagur, D. Chopra, A. S. Prakash, T. N. Guru Row and M. S. Hegde

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trans-Bis(2-aminoanilinium-κN²)bis(oxalato-κ²O,O′)copper(II)

T. D. Keene, M. B. Hursthouse and D. J. Price

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Bis(tetraethylammonium) μ-tetrathiomolybdato(VI)-bis[chlorocopper(I)]

M. Hosaini Sadr, H. Razmi, N. R. Brooks and W. Clegg

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A new one-dimensional coordination polymer: {[Cu(C₁₀H₉NO₅S)(H₂O)]·H₂O}_n

J.-L. Zeng, Y.-M. Jiang and K.-B. Yu

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Bis(μ-pentafluorobenzenethiolato-κ²S:S)-trans-bis{(pentafluorobenzenethiolato-κS)[(pentafluorophenyl)diphenylphosphine-κP]palladium(II)}

L. Villanueva, S. Bernès and H. Torrens

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catena-Poly[[triaquacobalt(II)]-μ-2,3-pyridinedicarboxylato-κ²O²:O³]

X.-M. Zhang, R.-Q. Fang, H.-S. Wu and S. W. Ng

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1,5-Di-tert-butyl-3,3,7,7,10,10-hexaphenyl-2,4,6,8,9,11-hexaoxa-3,7,10-trisila-1,5-digermabicyclo[3.3.3]undecane

M. Akkurt, S. Öztürk, T. R. Kök, F. W. Heinemann, S. Franken and H. Puff

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Bis[μ-3-phosphonopropionato(2–)]bis[aqua(1,10-phenanthroline)copper(II)]

X.-M. Zhang, R.-Q. Fang, H.-S. Wu and S. W. Ng

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Bis(benzylammonium) hydrogenarsenate monohydrate

C. Lee and W. T. A. Harrison

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Hydrogen-bonded supramolecular motifs in aqua(8-hydroxyquinoline-5-sulfonato-κ²N,O)potassium(I)

S. Francis, P. T. Muthiah, G. Bocelli and A. Cantoni

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Polymeric diaqua(μ-8-hydroxy-7-iodoquinoline-5-sulfonato-κ⁴N,O,O′,O′′)copper(II) tetrahydrate

S. Francis, P. T. Muthiah, G. Bocelli and A. Cantoni

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Interplay of hydrogen bonding and coordination modes in diaquabis(8-hydroxy-7-iodoquinoline-5-sulfonato)calcium(II) monohydrate

S. Francis, P. T. Muthiah, U. Rychlewska and B. Warżajtis

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Supramolecular organization via varied coordination modes in triaqua(μ-8-hydroxy-7-iodoquinoline-5-sulfonato)barium(II) monohydrate

P. T. Muthiah, S. Francis, G. Bocelli and A. Cantoni

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The binuclear copper(II) complex μ-chloro-μ-methoxy-bis[chloro(di-2-pyridylamine)copper(II)]

X.-R. Zeng, S.-M. Peng and G.-H. Lee

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Di-μ-aspirinato-copper(II): a redetermination

F. Garcia, M. A. Méndez-Rojas, E. González-Vergara, S. Bernès and M. A. Quiroz

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N-Ferrocenoyl-labelled glutamate diethyl ester

H.-B. Kraatz, T. C. Sutherland and F. E. Appoh

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Aqua{1-[(2-oxidophenyl)iminomethyl]naphthalen-2-olato}pyridinecopper(II)

X.-L. Zhang, C.-X. Ren, X.-M. Chen and S. W. Ng

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Di-μ-pivalato-bis[cis-diammineplatinum(II)] bis(perchlorate) pivalic acid solvate

K. Sakai, E. Ishigami, K. Yokokawa, T. Kajiwara and T. Ito

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(1-Methylimidazole)(N-salicylidene-rac-glutamato)copper(II)

V. Langer, E. Scholtzová, D. Gyepesová, M. Kohútová and A. Valent

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(18-Crown-6)-bis(tetrahydrofuran)potassium iodide

S. T. Liddle and W. Clegg

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syn-Tetracarbonyldi-μ-phenylthiolato-bis[(triphenylphosphine)ruthenium(I)]

K.-B. Shiu, F.-L. Liao and S.-L. Wang

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trans-Diaquatetrakis(imidazole)nickel(II) dichloride

K.-B. Shiu, C.-H. Yen, F.-L. Liao and S.-L. Wang

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trans-Bis(3-aminopyridine)diaquabis(4-cyanobenzoato)cobalt(II) dihydrate

H.-Y. He and L.-G. Zhu

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catena-Poly[bis(4-pyridylthioacetato)zinc(II)]

X.-M. Zhang, R.-Q. Fang, H.-S. Wu and S. W. Ng

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Di-μ-acetylacetonato-bis[diacetylacetonato(tert-butylamine)nickel(II)]

X.-H. He, Y.-Z. Yao, X. Luo, L. Zhang and Q. Wu

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Pentacarbonyl[diphenyl(perfluorovinyl)phosphine]molybdenum(0)

R. G. Peters, J. D. Palcic and R. G. Baughman

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catena-Poly[benzylmethylammonium [[diaquadichloromanganate(II)]-μ-chloro]]

T. Maris and R. Zouari

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organic compounds

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2,7,12-Tris(2-bromoethoxy)-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononaene

S.-Q. Wang, G. Zeng, X.-F. Zheng and K. Zhao

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Absolute configuration of 3α-feruloyltaraxerol dichloromethane solvate

S. Chantrapromma, H.-K. Fun, I. A. Razak, S. Laphookhieo and C. Karalai

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Conformation of (–)-membrenone-C

R. A. Sampson, M. V. Perkins and M. R. Taylor

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Imidazolium hydrogen tartronate

T. Fukunaga and H. Ishida

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N,N′-Bis(2-hydroxycyclohexyl)-trans-cyclohexane-1,2-diamine: a structure reanalysed at low temperature

A. S. de Sousa and M. A. Fernandes

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1,2,3,4-Tetrahydro-4′-furfuryl-1′-methylnaphthalene-2-spiro-3′-pyrrolidine-2′-spiro-1′′-acenaphthene-1,2′′-dione

M. M. Govind, S. Selvanayagam, D. Velmurugan, K. Ravikumar, R. Rathna Durga and R. Raghunathan

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5′′-Benzylidene-1′-methyl-4′-phenylindole-3-spiro-2′-pyrrolidine-3′-spiro-3′′-piperidine-2(3H),4′′-dione

M. M. Govind, S. Selvanayagam, D. Velmurugan, K. Ravikumar, G. Sridhar and R. Raghunathan

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Ethyl 5-cyano-1H-pyrrole-2-carboxylate

Y.-H. Zhang, Z. Yin, X.-F. Li, J. He and J.-P. Cheng

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1-Acetyl-4′,5′a-diphenyl-2′,2′a,5′,5′a-tetrahydrospiro[1H-indole-3,2′-oxeto[5,4-b]oxazol]-2(3H)-one

X.-M. Li, L. Wang, J.-H. Xu, S.-S. Zhang and H.-K. Fun

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Benzil 4-nitrophenylhydrazone

S. Shan, H.-G. Yu, W.-X. Hu and D.-J. Xu

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An ethanol solvate of Beclomethasone dipropionate

P. J. Kuehl, M. D. Carducci and P. B. Myrdal

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N,N′-Bis(2-pyridylmethyl)pyromellitic diimide

X. Lü, L. Zhang, C. Chen, C. Su, B. Kang and S. W. Ng

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The N—O bond as an element of chirality: (P)-4-(p-chlorophenyl)-3-{2-[4-(p-toluenesulfonyl)piperazino]ethoxy}thiazole-2(3H)-thione

J. Hartung, K. Špehar, I. Svoboda and H. Fuess

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[3,5-Bis(trifluoromethyl)phenyl]{(E)-2-[(E)-3,5-bis(trifluoromethyl)phenylimino]-1-methylpropylidene}amine

H. L. Aberdeen, R. E. Allan and J. D. Crane

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Hydrogen-bonding in 4-(hydroxymethyl)imidazolium picrate

M. Du and X.-J. Zhao

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1,3-Dibenzoyl-5,8-dimethoxy-2-phenyl-5,8-dihydroindolizine

H.-K. Fun, Y. Li, J.-H. Xu, X.-M. Li and S.-S. Zhang

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1-(3-Bromo-1-phenylsulfonyl-1H-indol-2-ylmethyl)pyrrolidine-2,5-dione

T. Ravishankar, K. Chinnakali, N. Arumugam, P. C. Srinivasan, A. Usman and H.-K. Fun

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Ethyl 2-(acetylamino)-2-(9-hydroxy-10-oxo-9,10-dihydro-9-phenanthrenyl)acetate

X.-M. Li, L. Wang, J.-H. Xu, S.-S. Zhang and H.-K. Fun

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Pyridine-2-carbaldehyde thiosemicarbazone 1.75-hydrate

Z. M. Jin, L. Shen, L. He, H. Guo and H. T. Wang

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L-Argininium bis(trifluoroacetate)

M. R. Silva, J. A. Paixão and A. M. Beja

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9-(p-Methylpheny)-9-fluorenol

P. D. Robinson, A. W. McLean and C. Y. Meyers

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7,8-Didehydro-4,5-epoxy-17-methylmorphinan-6-yl naphthalene-1-carboxylate

N. Gathergood, P. J. Scammells and G. D. Fallon

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{2-[(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylimino)methyl]phenoxy}acetic acid nitrate

Z.-L. You, H.-L. Zhu, W.-S. Liu and M.-Y. Tan

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{4-[(1-Naphthyl)vinyl]phenyl}di-p-tolylamine

X.-D. Cao, D.-Z. Liu, X.-Q. Zhou and S.-F. Sun

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tert-Butyl (2R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-iodopropionate

W. Clegg and L. Horsburgh

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Glycoluril diamide dihydrate

J. C. Fettinger, C. A. Burnett and L. Isaacs

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4b,4c,9b,9c-Tetrahydro-4b,4c,9b,9c-tetrachlorocyclobuta[1,2-a:3,4-a′]diindene-5,10-dione

S.-S. Zhang, M. Zhang, J.-H. Xu, X.-M. Li and H.-K. Fun

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2-tert-Butyl-4-methyl-6-(phenyldiazenyl)phenol

H. Kocaokutgen, M. S. Soylu, P. Lönnecke and S. Özkınalı

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21α-Fluoro-7-nor-12,13,15,16-tetrahydrovouacapane-17β,21α-lactone

S. Guilardi, J. A. L. C. Resende, M. T. P. Gambardella, A. J. Demuner, L. C. A. Barbosa and D. Piló-Veloso

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4,5-Dicyano-1,2-bis(2-dimethylaminoethylsulfanyl)benzene

U. Çoruh, R. Ustabaş, İ. Yılmaz and M. Yavuz

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(1,3-Dithiol-2-ylidene)propanedinitrile

M. Tomura and Y. Yamashita

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4′-Bromomethylbiphenyl-2-carbonitrile

Q.-B. Song, Y.-Z. Li, C.-Z. Qi, T.-H. Shen and H.-B. Wang

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tert-Butyl (2S)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-(3′,4′-dimethoxyphenyl)propionate chloroform sesquisolvate

W. Clegg and M. R. J. Elsegood

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5-Benzoyl-1-n-butyl-4-phenylpyrimidin-2(1H)-one

S. Türktekin, M. Akkurt, İ. Yıldırım, Ö. Özgen, E. Kendi and Y. Akçamur

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N-Hydroxysuccinimide

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A 1:1 diastereoisomeric complex of trans-2-{[(R)-(+)-1-phenylethylamino]carbonyl}cyclohexanecarboxylic acid

K. Takahashi, T. Okamura, H. Yamamoto and N. Ueyama

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(2,4-Dinitrophenyl)(1-nitrohexyl)diazene

D.-S. Yang, Y.-Z. Li and L.-M. Wu

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Methyl (RS)-[1-hydroxy-1-(3-nitrophenyl)-3-oxo-1,3-dihydroisoindol-2-yl]acetate

J. B. Baell, P. J. Duggan, G. D. Fallon and Y. P. Lok

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Bis(4-phenylpiperazin-1-yl)methane

Y.-X. Lu, C.-M. Liu, Z.-G. Zou, W. Xu, J.-M. Wang, M.-Q. Chen and Y.-M. Huang

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8-Chloro-5-(4-methylpiperazin-1-yl)-11H-pyrido[2,3-b][1,5]benzoxazepine

L. Dupont and J.-F. Liégeois

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Diethyl (2′R,4R,4′R)-2-(4′-ethoxycarbonyl-2′-thiazolidinyl)-6-methyl-4-(2′'-thienyl)-1,4-dihydropyridine-3,5-dicarboxylate

V. Vrábel, J. Kožíšek and Š. Marchalín

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2-(3-Ethyl-2,3,4,5-tetrahydro-4-oxo-2-thioxo-4-thiazolidin-5-ylidene)-1,2-dihydroacenaphthylen-1-one

T. V. Sundar, V. Parthasarathi, S. García-Granda, A. Jain and R. T. Pardasani

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(S)-2-(Methoxydiphenylmethyl)-1-(thiophen-3-ylmethyl)pyrrolidine

E. Martin, A. L. Winfrey, J. B. Human, C. Z. Carlin, D. S. Jones and C. A. Ogle

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(+)-Pinoresinol–dioxane (1/1)

R. Stomberg, W. Ibrahim, V. Langer and K. Lundquist

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3-[4-(2-Chlorophenyl)piperazinomethyl]-5-methyl-1-benzoxazolin-2(3H)-one

Y. Koysal, Ş. Işık, M. Köksal, H. Erdoğan and N. Gökhan

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(S)-(–)-1-Phenylethylaminium 3,5-dinitrosalicylate

G. Smith, U. D. Wermuth and J. M. White

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Bis(4,4′-bipyridinium) bis(8-hydroxyquinoline-5-sulfonate) bipyridine pentahydrate

S. Baskar Raj, P. T. Muthiah, G. Bocelli and A. Cantoni

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A redetermination of 4-chloro-3-nitrobenzoic acid

H. Ishida and T. Fukunaga

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1-tert-Butyl 2-methyl 4-(R)-hydroxypyrrolidine-1,2-(2S)-dicarboxylate

W. Clegg, H. J. C. Deboves and M. R. J. Elsegood

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8-Methyl-6-(4-methylpiperazin-1-yl)-11H-pyrido[2,3-b][1,4]benzodiazepine

M.-R. Spirlet, A. Graulich and J.-F. Liégeois

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C₆₀ thiophene disolvate

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Methyl 5-carboxyl-1-methylpyrazole-3-carboxylate monohydrate

C. Yin, F. Huo, F. Gao, G. Xue and P. Yang

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1-{(2E)-2-[(Aminocarbonothioyl)hydrazono]-2-(3-mesityl-3-methylcyclobutyl)ethyl}pyrrolidine-2,5-dione

T. Karakurt, M. Dinçer, I. Yılmaz and A. Čukurovalı

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8-Methoxy-4-(4-methoxyphenyl)isochroman-3-ol

M. Palusiak, S. J. Grabowski, J. A. Epsztajn and J. A. Kowalska

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8-(4-Methoxyphenyl)-3,5-bis[(E)-1-(4-methoxyphenyl)methylidene]-1,2,3,5,6,7-hexahydrodicyclopenta[b,e]pyridine

J. D. Crane and J. Crompton

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2,4,6-Triisopropylbenzenesulfonamide from single-crystal data

J. C. Clark, M. L. McLaughlin and F. R. Fronczek

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2-(N,N-Diacetamido)-3a,4,9,9a-tetrahydro-4,9-[1′,2′]benzeno-1H-benzo[f]isoindole-1,3(2H)-dione

I. Wolska and E. Hejchman

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(Z)-2-(2,4-Dimethoxybenzylidene)-1-azabicyclo[2.2.2]octan-3-ol

V. N. Sonar, S. Parkin and P. A. Crooks

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Methyl 4-bromo-1,3-dimethylpyrazole-5-carboxylate

F. Huo, C. Yin, W. Guo, C. Xia and P. Yang

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Hydrogen-bonding patterns in 4,4′-bipyridinium bis(3-carboxy-4-hydroxybenzenesulfonate) dihydrate

P. T. Muthiah, M. Hemamalini, G. Bocelli and A. Cantoni

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4-[2-(1-Naphthyl)vinyl]-N,N-diphenylaniline

X.-D. Cao, D.-Z. Liu and X.-Q. Zhou

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3-(2,4-Dichlorophenyl)-3-hydroxy-1-phenylpropan-1-one

Z. Yu, B. Zhao, Z. Tian and X. Gu

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Sperminium bis(tri-tert-butoxysilanethiolate)–2-propanol (1/2)

K. Baranowska, J. Chojnacki, W. Wojnowski and B. Becker

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1-Methyl-4′-(3-nitrophenyl)-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-2′′-indan-2,1′′,3′′-trione

P. R. Seshadri, S. Selvanayagam, D. Velmurugan, K. Ravikumar, A. R. Sureshbabu and R. Raghunathan

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A monoclinic polymorph of 2,3,2′,3′-tetrakis(2-pyridyl)-6,6′-biquinoxalinyl

A. Neels and H. Stoeckli-Evans

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An orthorhombic polymorph of 2,3,2′,3′-tetrakis(2-pyridyl)-6,6′-biquinoxalinyl

A. Neels and H. Stoeckli-Evans

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3,3-Bis(difluoroaminomethyl)oxetane, a promising new energetic material

R. Gilardi, R. N. Evans and G. E. Manser

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addenda and errata

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Ethyl 1-acetyl-2′-methyl-2-oxo-4′,5′-dihydro-1H-indoline-3-spiro-5′-oxazole-4′-carboxylate. Erratum

H.-K. Fun, L. Wang, J.-H. Xu, X.-M. Li and S.-S. Zhang

Erratum to Acta Cryst. (2003), E59, o1827–o1829.

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20-Dimethylamino-3α-methylamino-5α-pregnane. Erratum

M. I. Choudhary, K. P. Devkota, S. Anjum, A. A. Rahman, H.-K. Fun and Atta-ur-Rahman

Erratum to Acta Cryst. (2003), E59, o1682–o1684.

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Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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