Crystal structure and Hirshfeld surface analysis of 1,2-bis­(2′,6′-diisoprop­oxy-[2,3′-bipyridin]-6-yl)benzene

Park, K.-M.; Moon, S.-H.; Kang, Y.

doi:10.1107/S2056989018013002

Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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Figure 5
Synthetic routes and reagents to obtain the title compound: (i) 1,2-dipinacolatobenzene(1.5 eq), Pd(PPh₃)₄ (6 mol%), 2 M K₃PO₄ (6 eq), THF, 363 K, 48 h; (ii) NaH (6 eq), ⁱPrOH (8 eq), DMF, 273 K, 10 h.

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 74| Part 10| October 2018| Pages 1475-1479

https://doi.org/10.1107/S2056989018013002

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