Crystal engineering with short-chained amphiphiles: deca­sodium octa-n-butane­sulfonate di-μ-chlorido-bis­[di­chlorido­palladate(II)] tetra­hydrate, a layered inorganic–organic hybrid material

Thoelen, F.; Frank, W.

doi:10.1107/S2056989019004201

Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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Figure 2
Coordination environments of sodium cations. For clarity, n-butylgroups of the n-butanesulfonate anions are not shown. [Symmetry codes: (i) x, $[{1\over 2}]$ − y, $[{1\over 2}]$ + z; (ii) 1 − x, 1 − y, 1 − z; (iii) x, 1 + y, z; (iv) x, −1 + y, z; (v) 1 − x, − $[{1\over 2}]$ + y, $[{1\over 2}]$ − z; (vi) 1 − x, $[{1\over 2}]$ + y, $[{1\over 2}]$ − z]. The Na—O distances [Na1—O = 2.284 (3)–2.540 (3) Å; Na2—O = 2.283 (3)–2.700 (3) Å; Na3—O = 2.212 (2)–2.649 (3) Å; Na4—O = 2.308 (5)–2.479 (3) Å; Na5—O = 2.391 (3)–3.000 (4) Å] are within the reported range for short-chained sodium alkanesulfonates (Wei & Hingerty, 1981

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 75| Part 5| May 2019| Pages 557-561

https://doi.org/10.1107/S2056989019004201

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