The crystal structures of {LnCu5}3+ (Ln = Gd, Dy and Ho) 15-metallacrown-5 complexes and a reevaluation of the isotypic EuIII analogue

Pavlishchuk, A.; Naumova, D.; Zeller, M.; Calderon Cazorla, S.; Addison, A.W.

doi:10.1107/S205698901900999X

Acta Crystallographica Section E
Acta Crystallographica
Section ECRYSTALLOGRAPHIC COMMUNICATIONS

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Figure 5
Difference electron density in 2 around the water molecules O11w, O24w and O25w (using the SHELXLE GUI for SHELXL; Hübschle et al., 2011

). Difference electron densities were calculated with water H atoms removed from the final structural model. H-atom positions, refined as described in the Refinement section, are shown. The difference electron-density mesh setting used is 0.28 e Å⁻³.

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 75| Part 8| August 2019| Pages 1215-1223

https://doi.org/10.1107/S205698901900999X

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