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Figure 1
The single-crystal X-ray structure of DyIIINa(3-OHben)4[12-MCMn(III)N(shi)-4](H2O)4·10DMA, 1, (a) top view with only the metal atoms and shi3− ligands labeled for clarity and (b) side view with only the metal atoms and axial ligands labeled for clarity. The displacement ellipsoids are drawn at the 50% probability level. For clarity, hydrogen atoms, solvent mol­ecules, and disorder have been omitted. Color scheme: purple – DyIII, green – MnIII, yellow – Na+, red – oxygen, blue – nitro­gen, and gray – carbon. All figures were generated with the program Mercury (Macrae et al., 2020BB15). [Symmetry codes: (i) +x, −y + [{3\over 2}], +z; (ii) −x + [{3\over 2}], −y + [{3\over 2}], +z; (iii) −x + [{3\over 2}], +y, +z.]

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