Figure 14
The independent components of compound (XIV) showing the atom-labelling scheme and the disorder in one of the anions. The major disorder component is drawn using full lines and the minor disorder component is drawn using broken lines. Displacement ellipsoids are drawn at the 30% probability level. The atoms marked `a' or `b' are at the symmetry positions (2 − x, 1 − y, 2 − z) and (−x, −y, 2 − z), respectively. The H atoms bonded to atoms O32, O34 and O42 have occupancies 0.286 (9), 0.214 (9) and 0.5, respectively, as do their inversion-related equivalents. |