The structures of 1:1 and 1:2 adducts of phosphane­tricarbo­nitrile with 1,4-di­aza­bicyclo[2.2.2]octa­ne

Purdy, A.P.; Butcher, R.J.; Klug, C.A.

doi:10.1107/S2056989021011464

Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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Figure 6
(a) ³¹P MAS NMR spectrum for 1 obtained using a spinning speed of 5 kHz. The sideband pattern is corresponds to a chemical shift anisotropy (csa) with isotropic shift of −161 ppm, d_aniso = −67.7 ppm, and h = 0.34; (b) ¹³C MAS NMR spectrum for 1 obtained using a spinning speed of 12.5 kHz. Note that in both spectra, spinning sidebands are marked with asterisks (*).

CRYSTALLOGRAPHIC
COMMUNICATIONS

ISSN: 2056-9890

Volume 77| Part 12| December 2021| Pages 1190-1196

https://doi.org/10.1107/S2056989021011464

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