Figure 3
The structure of H2[OO]tBu (50% probability ellipsoids) is shown with the co-crystallized dichloromethane solvent molecule. The dichloromethane carbon atom was found to be disordered about an inversion center; only one orientation is shown, which is not the one belonging to the asymmetric unit. Hydroxyl H atoms are disordered over two positions, both positions are shown above. |