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Figure 4
Comparison of synthesized precession images of the 0kl plane collected at 100 K and 200 K showing the additional weak reflections along k. The corresponding unit-cell packing diagrams viewed along [100] are shown below for the 100 K structure (right) and the 200 K structure (left). For comparison, the 100 K cell is shown doubled along the b axis to illustrate that the disorder is retained, as observed in the smaller unit cell. Yellow spheres in the 200 K packing diagram indicate inversion centers. The disordered Et4N+ cations are positioned on these inversion centers and are therefore not visible in the packing view. Teal = Mo atoms; red = O atoms; lavender = N atoms; white = H atoms. |

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