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The following articles are a selection of those recently accepted for publication in Acta Crystallographica Section E: Crystallographic Communications.
See also Forthcoming articles in all IUCr journals.
research communications (GO)Crystal structure and in vitro anti-proliferative activity of 2-[(4-acetylphenyl)carbamoyl]phenyl acetate
2-[(4-Acetylphenyl)carbamoyl]phenyl acetate, a derivative of aspirin, has been structurally characterized revealing a structure based on intermolecular N—H⋯O hydrogen bonds and π–π interactions.
research communications (GM)Synthesis, crystal structure, stereochemical and Hirshfeld surface analysis of trans-diaquabis(1-phenylpropane-1,2-diamine-κ2N,N′)nickel(II) dichloride dihydrate
The cation of the title compound exhibits point group symmetry ![[\overline{1}]](./)
, with the central NiII atom in a trans [N4O2] coordination environment.
research communications (GM)research communications (GM)Crystal structure of bis{3-(3,4-dimethoxyphenyl)-5-[6-(pyrazol-1-yl)pyridin-2-yl]-1,2,4-triazol-3-ato}iron(II)–methanol–dichloroform (1/2/2)
The title compound, a charge-neutral bis{5-(3,4-dimethoxyphenyl)-1,2,4-triazol-3-ato)-6-(pyrazol-1-yl)pyridine} iron(II) dimethanol dichloroform solvate, is a high-spin complex with a distorted pseudooctahedral coordination environment of the metal ion. Due to the tapered shape and polar nature, the molecules stack in one-dimensional columns that are bound by weak hydrogen bonds into layers, which, in turn, are arranged in a three-dimensional network without interlayer interactions below van der Waals radii.
research communications (GO)research communications (GO)Synthesis and crystal structure of 2-(anthracen-9-yl)-1-(tert-butyldimethylsilyl)-3,6-dihydro-1λ4,2λ4-azaborinine
A modification of a B—Cl 1,2–azaborinine precursor with anthracenyl lithium generates an air-stable analog of cyclohexadiene. In the crystal packing, van der Waals interactions are dominant.
research communications (GM)Crystal structure of dibenzylammonium hydrogen (4-aminophenyl)arsonate monohydrate
The title salt consists of three components, comprising one dibenzylammonium cation, [(C6H5CH2)2NH2]+, one hydrogen (4-aminophenyl)arsonate anion, [H2NC6H4As(OH)O2]−, and one molecule of water. In the crystal, these components are organized in infinite zigzag chains via intermolecular hydrogen bonds. Weak interactions between the chains lead to a three-dimensional network.
research communications (GO)research communications (GM)Crystal structure and Hirshfeld surface analysis of cyclo-tetrabromido-1κ2Br,3κ2Br-tetrakis(μ2-2-{[(pyridin-2-yl)methyl]amino}ethane-1-thiolato-κ3N,S:S)tetramercury(II)
A macrometallacyclic mercury(II) complex [((HgL2)(HgBr2))2], where HL = 2-{[(pyridin-2-yl)methyl]amino}ethane-1-thiol, was synthesized and characterized by single-crystal X-ray diffraction and Hirshfeld analysis.
research communications (GM)Synthesis, crystal structure and reactivity of bis(μ-2-methylpyridine N-oxide-κ2O:O)bis[dibromido(2-methylpyridine N-oxide-κO)cobalt(II)] butanol monosolvate
The crystal structure of the title compound consists of dinuclear complexes, in which the CoII cations are fivefold coordinated and linked by centrosymmetric pairs of μ-1,1(O,O)-bridging 2-methylpyridine N-oxide coligands.
