Figure 3
(a) A photograph showing a 96-well (8 × 12) TPFS plate placed in an in-house-designed three-dimensional printed adaptor conforming to the SBS format of microtitre plates. The adaptor is in two pieces held together by magnets. (b) The plate holder, ready for data collection, mounted on the in situ horizontal goniometer of beamline I24 at Diamond Light Source. The vertical goniometer is visible at the bottom of the picture (upward arrow) having been retracted from the sample position. (c) A photograph of an isolated well held in a prototype tweezer pin and mounted on the vertical goniometer of beamline I24 at 294 K with the cryoshutter closed; the view is along the beam axis away from the detector. |