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Figure 4
Plots of θ-corrected X-ray diffraction results before (11 min) and after hydrothermal reaction. Homogenization significantly increases the intensity of the quartz 101 reflection, indicating some surface sensitivity of the in situ measurements. (See Fig. S3 for the full range)

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 53| Part 4| August 2020| Pages 1163-1166
https://doi.org/10.1107/S1600576720006019
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