view article
Figure 17
Two powder diffraction patterns (unmasked) collected from the same phase in a DAC at a laboratory source (left) and at a synchrotron source (right). Comparing the primary 2D patterns makes it possible to see that the phase studied in the laboratory is in fact the same as that studied later at the synchrotron source (sample rings in the left photograph are shown by blue arrows). The pattern on the left is the same as was shown in Fig. 16[link]. Note that masking of the gasket rings (shown by red arrows) was no longer necessary for data collected at the synchrotron source, but masking of a few point reflections originating from diamond would still be needed. One can also see from the comparison that one of the gasket broad bold rings in fact overlaps with two rings from the sample that became accessible in a synchrotron experiment. Data courtesy of Dr N. Tumanov.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 58| Part 4| August 2025| Pages 1085-1105
https://doi.org/10.1107/S1600576725004728
Follow J. Appl. Cryst.
Sign up for e-alerts
E-alerts
Follow J. Appl. Cryst. on Twitter
Twitter
Follow us on facebook
Facebook
Sign up for RSS feeds
RSS