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Figure 11
Evolution of the normalized unit-cell parameters a/ai, c/ci and volume V/Vi as a function of RH for the six dehydration and rehydration cycles of the HI–m-nitrophenol complex. The normalization was calculated relative to the initial unit-cell parameter values at 95% RH for the dehydration and rehydration process of each cycle. The plots highlight the hysteresis in unit-cell parameter variation, with distinct differences observed between dehydration and rehydration phases, indicating the structural response of the crystals to environmental changes. |
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