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Figure 6
Pawley fits of XRPD data obtained with the laboratory X'Pert Pro diffractometer for the HI–m-cresol complex at ambient (capillary) and non-ambient conditions. In all plots, the black line represents the experimental data, the red line the calculated pattern and the blue line the difference profile, while the Bragg reflections corresponding to the rhombohedral space group R3 are represented by green vertical bars. The insets magnify the 2θ range from 5° to 11° corresponding to high-intensity Bragg peaks.

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CRYSTALLOGRAPHY
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