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Figure 3
(a) Normalized XRR curves with different collection times. ▵ denotes a triangle ω scan and ∼ a sine ω scan. Curves are shifted by 102 with respect to each other for visual clarity. The refnx fit of the reference XRR scan (solid line) is overlaid for reference. Constant exposure time was assumed for reference and 9.95 ms fast XRR scans. (b) Fitted parameters of the top gold layer for these scans. The median and estimated standard deviation from the MCMC chain are plotted. All scans are fitted after log10 transformation. The fastest scan at 213 µs scan time was additionally fitted untransformed (shown in green) as well as after Anscombe transformation (red); these are plotted with a shift to the left on the x axis for clarity.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 59| Part 4| August 2026|
https://doi.org/10.1107/S1600576726004449
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