(+)-(1R,5S,6R)-1-[3-(9,9-Dimethyl-4,4-dioxo-4λ6-thiatricyclo[6.1.1.02,6]dec-2-en-5-yl)-2-tert-butyldimethylsilyloxy-4,6-dimethoxyphenyl]-3-methylbutan-1-one methyl tert-butyl ether solvate at 133K

Bats, J.W.; Berger, B.; Gerlach, M.; Reggelin, M.

doi:10.1107/S0108270199099837

(+)-(1R,5S,6R)-1-[3-(9,9-Dimethyl-4,4-dioxo-4⁶-thiatricyclo[6.1.1.0^2,6]dec-2-en-5-yl)-2-tert-butyldimethylsilyloxy-4,6-dimethoxyphenyl]-3-methylbutan-1-one methyl tert-butyl ethersolvate at 133K

J. W. Bats, B. Berger, M. Gerlach and M. Reggelin

The absolute configuration of the title compound has been determined. The structure contains two independent molecules with very similar conformations. Torsion angles about corresponding bonds differ by less than 10°. The solvent molecule is not involved in short intermolecular contacts.

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(+)-(1R,5S,6R)-1-[3-(9,9-Dimethyl-4,4-dioxo-4⁶-thiatricyclo[6.1.1.0^2,6]dec-2-en-5-yl)-2-tert-butyldimethylsilyloxy-4,6-dimethoxyphenyl]-3-methylbutan-1-one methyl tert-butyl ethersolvate at 133K

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	Crystallographic Information File (CIF) Contains datablocks default, qa0081
	Structure factor file (CIF format) Contains datablock mg618

(+)-(1R,5S,6R)-1-[3-(9,9-Dimethyl-4,4-dioxo-46-thiatricyclo[6.1.1.02,6]dec-2-en-5-yl)-2-tert-butyldimethylsilyloxy-4,6-dimethoxyphenyl]-3-methylbutan-1-one methyl tert-butyl ethersolvate at 133K

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(+)-(1R,5S,6R)-1-[3-(9,9-Dimethyl-4,4-dioxo-4⁶-thiatricyclo[6.1.1.0^2,6]dec-2-en-5-yl)-2-tert-butyldimethylsilyloxy-4,6-dimethoxyphenyl]-3-methylbutan-1-one methyl tert-butyl ethersolvate at 133K