Polymorphism of K₂Co₂Mo₃O₁₂: variations in the packing schemes and changes in molybdenum coordination under high pressure

Within systematic studies on the K–Co–Mo–O system so-called high-temperature and high-pressure modifications of K₂Co₂Mo₃O₁₂ were found. The Birch–Murnaghan fits for the ambient-conditions modification α (Z = 4) and the high-pressure phase II (Z = 8) lead to V₀ = 1193.09 (4) ų, K = 30.8 (8) GPa, = 5.4 (4) and V₀ = 2170 (10) ų, K = 51 (2) GPa with fixed at 4.0, respectively. The high-pressure phase transition is denoted as pseudoreconstructive [Wiesmann et al. (1997). J. Solid State Chem. 132, 88–97], because some [MoO₄] tetrahedra turn into edge-sharing pairs of [MoO₅] pyramids or face-sharing pairs of [MoO₆] octahedra. The new phases are presented and compared with the α phase.

Computing details

For all compounds, data collection: CrysAlis CCD, Oxford Diffraction Ltd., Version 1.171.31.4 (release 06-08-2006 CrysAlis171 .NET) (compiled Aug 6 2006,16:44:45); cell refinement: CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.31.4 (release 06-08-2006 CrysAlis171 .NET) (compiled Aug 6 2006,16:44:45); data reduction: CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.31.4 (release 06-08-2006 CrysAlis171 .NET) (compiled Aug 6 2006,16:44:45). Program(s) used to solve structure: SHELXS97 (Sheldrick, 1990) for alpha; SHELXS97 (Sheldrick, 1997) for beta, (II). For all compounds, program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: Brandenburg et al. Diamond 3.0b; software used to prepare material for publication: SHELXL97 (Sheldrick, 1997).

Figures

(alpha)

Crystal data

Co2K2Mo3O12	F(000) = 1256
Mr = 675.88	Dx = 3.763 Mg m^−3
Monoclinic, P21/c	Mo Kα radiation, λ = 0.71073 Å
a = 7.0093 (1) Å	Cell parameters from 7011 reflections
b = 8.9624 (2) Å	θ = 2.5–30.1°
c = 19.9977 (4) Å	µ = 6.59 mm^−1
β = 108.247 (2)°	T = 293 K
V = 1193.09 (4) Å^3	Prism, blue
Z = 4	0.14 × 0.11 × 0.06 mm

Data collection

Oxford Diffraction Xcalibur (TM) Single Crystal X-ray Diffractometer with Sapphire CCD Detector.	2435 independent reflections
Radiation source: Enhance (Mo) X-ray Source	2152 reflections with I > 2σ(I)
Graphite monochromator	Rint = 0.017
Detector resolution: 8.4012 pixels mm^-1	θmax = 26.4°, θmin = 2.5°
Rotation method data acquisition using ω and phi scans.	h = −5→8
Absorption correction: analytical CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.31.4 (release 06-08-2006 CrysAlis171 .NET) (compiled Aug 6 2006,16:44:45) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)	k = −11→11
Tmin = 0.573, Tmax = 0.751	l = −24→24
8014 measured reflections

Refinement

Refinement on F^2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F^2 > 2σ(F^2)] = 0.028	w = 1/[σ^2(Fo^2) + (0.098P)^2] where P = (Fo^2 + 2Fc^2)/3
wR(F^2) = 0.137	(Δ/σ)max < 0.001
S = 1.24	Δρmax = 2.94 e Å^−3
2435 reflections	Δρmin = −1.61 e Å^−3
173 parameters	Extinction correction: SHELXL, Fc^*=kFc[1+0.001xFc^2λ^3/sin(2θ)]^-1/4
0 restraints	Extinction coefficient: 0.0075 (7)

Special details

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F² against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F², conventional R-factors R are based on F, with F set to zero for negative F². The threshold expression of F² > σ(F²) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F² are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq
Mo1	0.04914 (8)	0.34200 (6)	0.27004 (3)	0.0103 (2)
Mo2	0.80582 (8)	0.73501 (6)	0.40157 (3)	0.0090 (2)
Mo3	0.58498 (8)	0.33816 (6)	0.45880 (3)	0.0098 (2)
Co1	0.27783 (13)	0.65556 (9)	0.36482 (4)	0.0077 (3)
Co2	0.07178 (12)	0.41935 (9)	0.43901 (4)	0.0078 (3)
K1	0.1961 (3)	0.04268 (18)	0.40919 (9)	0.0245 (4)
K2	0.5042 (3)	0.0135 (3)	0.27230 (11)	0.0410 (6)
O1	0.2132 (8)	0.2065 (6)	0.2592 (3)	0.0256 (12)
O2	0.1740 (7)	0.5164 (5)	0.2797 (2)	0.0163 (10)
O3	−0.0096 (7)	0.3013 (6)	0.3486 (2)	0.0190 (11)
O4	−0.1777 (7)	0.3429 (5)	0.1962 (2)	0.0120 (10)
O6	0.5621 (7)	0.6710 (5)	0.3549 (3)	0.0137 (10)
O5	0.8305 (7)	0.9128 (5)	0.3723 (3)	0.0189 (11)
O7	0.8403 (7)	0.7553 (5)	0.4934 (2)	0.0152 (10)
O8	1.0029 (6)	0.6221 (5)	0.3884 (2)	0.0115 (9)
O9	0.5421 (8)	0.2074 (6)	0.3943 (3)	0.0258 (12)
O10	0.6224 (7)	0.2339 (5)	0.5369 (2)	0.0146 (10)
O11	0.8061 (7)	0.4433 (5)	0.4606 (2)	0.0136 (10)
O12	0.3644 (7)	0.4571 (5)	0.4350 (3)	0.0147 (10)

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
Mo1	0.0097 (3)	0.0122 (4)	0.0080 (3)	−0.00045 (19)	0.0012 (2)	−0.00164 (19)
Mo2	0.0076 (3)	0.0104 (3)	0.0087 (3)	0.0009 (2)	0.0021 (2)	0.00107 (19)
Mo3	0.0073 (3)	0.0114 (4)	0.0098 (3)	0.00017 (19)	0.0012 (2)	0.00075 (19)
Co1	0.0060 (4)	0.0091 (5)	0.0077 (5)	0.0003 (3)	0.0019 (3)	0.0001 (3)
Co2	0.0071 (4)	0.0098 (5)	0.0074 (4)	0.0018 (3)	0.0037 (3)	0.0016 (3)
K1	0.0274 (9)	0.0161 (8)	0.0309 (9)	−0.0021 (6)	0.0105 (7)	−0.0063 (6)
K2	0.0316 (10)	0.0644 (14)	0.0329 (11)	0.0273 (10)	0.0186 (8)	0.0238 (10)
O1	0.016 (3)	0.027 (3)	0.029 (3)	0.006 (2)	0.001 (2)	−0.010 (2)
O2	0.018 (2)	0.018 (2)	0.015 (2)	−0.006 (2)	0.008 (2)	−0.0063 (19)
O3	0.027 (3)	0.021 (2)	0.011 (2)	−0.010 (2)	0.010 (2)	−0.002 (2)
O4	0.011 (2)	0.011 (2)	0.012 (2)	−0.0001 (16)	−0.0001 (19)	−0.0025 (16)
O6	0.008 (2)	0.021 (3)	0.013 (2)	−0.0016 (18)	0.0045 (19)	−0.0017 (18)
O5	0.019 (3)	0.016 (3)	0.021 (3)	0.002 (2)	0.005 (2)	0.007 (2)
O7	0.020 (3)	0.014 (2)	0.013 (2)	0.0031 (19)	0.006 (2)	−0.0004 (18)
O8	0.010 (2)	0.014 (2)	0.012 (2)	0.0005 (18)	0.0050 (18)	0.0027 (18)
O9	0.027 (3)	0.025 (3)	0.022 (3)	−0.001 (2)	0.003 (2)	−0.010 (2)
O10	0.014 (2)	0.015 (2)	0.014 (2)	0.0004 (18)	0.003 (2)	0.0024 (18)
O11	0.013 (2)	0.017 (2)	0.012 (2)	−0.0018 (19)	0.0052 (19)	0.0006 (18)
O12	0.010 (2)	0.016 (2)	0.017 (2)	0.0019 (18)	0.0029 (19)	0.0073 (19)

Geometric parameters (Å, º)

Mo1—O1	1.732 (5)	K1—O5^vii	2.698 (5)
Mo1—O2	1.772 (5)	K1—O7^v	2.728 (5)
Mo1—O3	1.783 (5)	K1—O4^viii	2.738 (5)
Mo1—O4	1.799 (5)	K1—O3	2.797 (6)
Mo1—K1	3.7691 (18)	K1—O10^ix	2.840 (5)
Mo1—K2^i	3.8134 (19)	K1—O9	2.933 (6)
Mo1—K1^ii	3.8959 (18)	K1—O1	3.376 (6)
Mo1—K2^ii	4.008 (2)	K1—Co1^x	3.6704 (18)
Mo2—O5	1.725 (5)	K1—Mo2^vii	3.8534 (17)
Mo2—O6	1.766 (5)	K2—O1	2.624 (6)
Mo2—O7	1.786 (5)	K2—O5^x	2.679 (5)
Mo2—O8	1.797 (4)	K2—O2^xi	2.764 (5)
Mo2—K2^iii	3.736 (2)	K2—O6^xi	2.818 (5)
Mo2—K1^iv	3.8534 (17)	K2—O9	2.939 (6)
Mo2—K2^i	4.0024 (19)	K2—O4^viii	2.979 (5)
Mo3—O9	1.698 (5)	K2—Mo2^x	3.736 (2)
Mo3—O10	1.768 (5)	K2—Co1^xi	3.755 (2)
Mo3—O11	1.805 (5)	K2—Mo1^xi	3.8134 (19)
Mo3—O12	1.815 (4)	K2—Mo2^xi	4.0024 (19)
Mo3—K1	3.7059 (17)	K2—Mo1^viii	4.008 (2)
Co1—O2	2.051 (5)	O2—K2^i	2.764 (5)
Co1—O4^ii	2.065 (4)	O4—Co1^viii	2.065 (4)
Co1—O6	2.068 (5)	O4—K1^ii	2.738 (5)
Co1—O10^v	2.114 (5)	O4—K2^ii	2.979 (5)
Co1—O8^vi	2.144 (4)	O6—K2^i	2.818 (5)
Co1—O12	2.229 (5)	O5—K2^iii	2.679 (5)
Co1—K1^iii	3.6704 (18)	O5—K1^iv	2.698 (5)
Co1—K2^i	3.755 (2)	O7—Co2^v	2.033 (5)
Co2—O3	2.016 (5)	O7—K1^v	2.728 (5)
Co2—O7^v	2.033 (5)	O8—Co2^xii	2.062 (5)
Co2—O11^vi	2.050 (5)	O8—Co1^xii	2.144 (4)
Co2—O8^vi	2.062 (5)	O10—Co1^v	2.114 (5)
Co2—O12	2.105 (5)	O10—K1^ix	2.840 (5)
Co2—O11^v	2.281 (5)	O11—Co2^xii	2.050 (5)
Co2—K1	3.5828 (18)	O11—Co2^v	2.281 (5)
O1—Mo1—O2	107.9 (3)	O10^ix—K1—Co1^x	35.04 (10)
O1—Mo1—O3	108.2 (3)	O9—K1—Co1^x	104.75 (12)
O2—Mo1—O3	109.1 (2)	O1—K1—Co1^x	98.32 (10)
O1—Mo1—O4	110.6 (2)	Co2—K1—Co1^x	174.51 (6)
O2—Mo1—O4	111.4 (2)	O5^vii—K1—Mo3	159.62 (12)
O3—Mo1—O4	109.6 (2)	O7^v—K1—Mo3	63.90 (11)
O1—Mo1—K1	63.6 (2)	O4^viii—K1—Mo3	121.79 (11)
O2—Mo1—K1	122.39 (16)	O3—K1—Mo3	76.11 (11)
O3—Mo1—K1	44.66 (18)	O10^ix—K1—Mo3	108.52 (11)
O4—Mo1—K1	125.17 (14)	O9—K1—Mo3	26.52 (10)
O1—Mo1—K2^i	68.4 (2)	O1—K1—Mo3	72.49 (10)
O2—Mo1—K2^i	42.00 (16)	Co2—K1—Mo3	58.60 (3)
O3—Mo1—K2^i	135.28 (16)	Co1^x—K1—Mo3	125.65 (5)
O4—Mo1—K2^i	113.08 (15)	O5^vii—K1—Mo1	95.07 (11)
K1—Mo1—K2^i	113.41 (5)	O7^v—K1—Mo1	89.40 (11)
O1—Mo1—K1^ii	109.11 (19)	O4^viii—K1—Mo1	87.76 (10)
O2—Mo1—K1^ii	75.74 (16)	O3—K1—Mo1	26.61 (10)
O3—Mo1—K1^ii	138.45 (17)	O10^ix—K1—Mo1	152.58 (11)
O4—Mo1—K1^ii	38.84 (15)	O9—K1—Mo1	67.07 (11)
K1—Mo1—K1^ii	161.38 (4)	O1—K1—Mo1	27.35 (9)
K2^i—Mo1—K1^ii	76.47 (4)	Co2—K1—Mo1	55.10 (3)
O1—Mo1—K2^ii	151.52 (18)	Co1^x—K1—Mo1	121.44 (5)
O2—Mo1—K2^ii	95.57 (17)	Mo3—K1—Mo1	72.37 (3)
O3—Mo1—K2^ii	77.84 (17)	O5^vii—K1—Mo2^vii	22.92 (10)
O4—Mo1—K2^ii	43.69 (15)	O7^v—K1—Mo2^vii	106.22 (11)
K1—Mo1—K2^ii	116.85 (4)	O4^viii—K1—Mo2^vii	68.89 (10)
K2^i—Mo1—K2^ii	127.29 (7)	O3—K1—Mo2^vii	108.21 (11)
K1^ii—Mo1—K2^ii	60.63 (4)	O10^ix—K1—Mo2^vii	67.58 (10)
O5—Mo2—O6	107.7 (2)	O9—K1—Mo2^vii	162.84 (12)
O5—Mo2—O7	105.1 (2)	O1—K1—Mo2^vii	119.90 (10)
O6—Mo2—O7	111.9 (2)	Co2—K1—Mo2^vii	118.31 (5)
O5—Mo2—O8	107.9 (2)	Co1^x—K1—Mo2^vii	58.44 (3)
O6—Mo2—O8	113.6 (2)	Mo3—K1—Mo2^vii	167.29 (6)
O7—Mo2—O8	110.2 (2)	Mo1—K1—Mo2^vii	116.97 (5)
O5—Mo2—K2^iii	40.81 (16)	O1—K2—O5^x	138.76 (18)
O6—Mo2—K2^iii	66.89 (16)	O1—K2—O2^xi	131.05 (19)
O7—Mo2—K2^iii	120.57 (15)	O5^x—K2—O2^xi	71.17 (15)
O8—Mo2—K2^iii	124.72 (14)	O1—K2—O6^xi	71.12 (17)
O5—Mo2—K1^iv	37.53 (16)	O5^x—K2—O6^xi	134.69 (16)
O6—Mo2—K1^iv	144.16 (16)	O2^xi—K2—O6^xi	65.10 (14)
O7—Mo2—K1^iv	91.19 (16)	O1—K2—O9	63.81 (16)
O8—Mo2—K1^iv	80.81 (15)	O5^x—K2—O9	75.26 (16)
K2^iii—Mo2—K1^iv	77.89 (5)	O2^xi—K2—O9	115.77 (18)
O5—Mo2—K2^i	104.35 (17)	O6^xi—K2—O9	113.59 (17)
O6—Mo2—K2^i	37.62 (15)	O1—K2—O4^viii	74.63 (16)
O7—Mo2—K2^i	143.70 (16)	O5^x—K2—O4^viii	101.67 (15)
O8—Mo2—K2^i	80.02 (15)	O2^xi—K2—O4^viii	148.84 (16)
K2^iii—Mo2—K2^i	72.221 (13)	O6^xi—K2—O4^viii	121.83 (15)
K1^iv—Mo2—K2^i	125.09 (4)	O9—K2—O4^viii	90.21 (15)
O9—Mo3—O10	104.4 (3)	O1—K2—Mo2^x	139.75 (14)
O9—Mo3—O11	108.8 (2)	O5^x—K2—Mo2^x	24.88 (11)
O10—Mo3—O11	111.7 (2)	O2^xi—K2—Mo2^x	85.12 (11)
O9—Mo3—O12	105.8 (2)	O6^xi—K2—Mo2^x	148.97 (11)
O10—Mo3—O12	114.9 (2)	O9—K2—Mo2^x	86.33 (12)
O11—Mo3—O12	110.7 (2)	O4^viii—K2—Mo2^x	79.43 (10)
O9—Mo3—K1	50.44 (19)	O1—K2—Co1^xi	100.65 (15)
O10—Mo3—K1	75.65 (15)	O5^x—K2—Co1^xi	102.21 (12)
O11—Mo3—K1	158.99 (15)	O2^xi—K2—Co1^xi	32.37 (10)
O12—Mo3—K1	81.64 (15)	O6^xi—K2—Co1^xi	32.92 (10)
O2—Co1—O4^ii	92.15 (19)	O9—K2—Co1^xi	117.02 (14)
O2—Co1—O6	93.63 (19)	O4^viii—K2—Co1^xi	147.52 (12)
O4^ii—Co1—O6	92.77 (19)	Mo2^x—K2—Co1^xi	117.40 (5)
O2—Co1—O10^v	169.83 (19)	O1—K2—Mo1^xi	155.51 (15)
O4^ii—Co1—O10^v	96.92 (18)	O5^x—K2—Mo1^xi	57.41 (11)
O6—Co1—O10^v	90.53 (18)	O2^xi—K2—Mo1^xi	25.41 (10)
O2—Co1—O8^vi	89.30 (18)	O6^xi—K2—Mo1^xi	85.19 (10)
O4^ii—Co1—O8^vi	94.68 (18)	O9—K2—Mo1^xi	123.75 (13)
O6—Co1—O8^vi	171.88 (18)	O4^viii—K2—Mo1^xi	125.34 (11)
O10^v—Co1—O8^vi	85.39 (17)	Mo2^x—K2—Mo1^xi	63.78 (3)
O2—Co1—O12	89.60 (19)	Co1^xi—K2—Mo1^xi	54.86 (3)
O4^ii—Co1—O12	174.90 (19)	O1—K2—K1	56.96 (14)
O6—Co1—O12	91.89 (18)	O5^x—K2—K1	91.68 (12)
O10^v—Co1—O12	80.98 (17)	O2^xi—K2—K1	159.74 (13)
O8^vi—Co1—O12	80.55 (17)	O6^xi—K2—K1	127.94 (11)
O2—Co1—K1^iii	137.21 (15)	O9—K2—K1	47.12 (12)
O4^ii—Co1—K1^iii	47.50 (13)	O4^viii—K2—K1	43.29 (10)
O6—Co1—K1^iii	100.83 (13)	Mo2^x—K2—K1	83.09 (4)
O10^v—Co1—K1^iii	50.48 (13)	Co1^xi—K2—K1	155.52 (7)
O8^vi—Co1—K1^iii	81.96 (13)	Mo1^xi—K2—K1	146.81 (6)
O12—Co1—K1^iii	129.38 (13)	O1—K2—Mo2^xi	52.61 (13)
O2—Co1—K2^i	46.17 (14)	O5^x—K2—Mo2^xi	156.87 (13)
O4^ii—Co1—K2^i	89.12 (14)	O2^xi—K2—Mo2^xi	87.34 (11)
O6—Co1—K2^i	47.79 (14)	O6^xi—K2—Mo2^xi	22.49 (9)
O10^v—Co1—K2^i	138.22 (13)	O9—K2—Mo2^xi	108.15 (13)
O8^vi—Co1—K2^i	135.46 (13)	O4^viii—K2—Mo2^xi	101.19 (10)
O12—Co1—K2^i	95.54 (13)	Mo2^x—K2—Mo2^xi	165.47 (7)
K1^iii—Co1—K2^i	128.83 (5)	Co1^xi—K2—Mo2^xi	55.38 (3)
O3—Co2—O7^v	97.7 (2)	Mo1^xi—K2—Mo2^xi	105.50 (5)
O3—Co2—O11^vi	102.86 (19)	K1—K2—Mo2^xi	107.47 (5)
O7^v—Co2—O11^vi	92.72 (19)	O1—K2—Mo1^viii	63.98 (13)
O3—Co2—O8^vi	93.8 (2)	O5^x—K2—Mo1^viii	124.88 (12)
O7^v—Co2—O8^vi	168.55 (19)	O2^xi—K2—Mo1^viii	140.69 (13)
O11^vi—Co2—O8^vi	85.54 (17)	O6^xi—K2—Mo1^viii	97.25 (11)
O3—Co2—O12	93.2 (2)	O9—K2—Mo1^viii	103.42 (12)
O7^v—Co2—O12	93.02 (18)	O4^viii—K2—Mo1^viii	24.66 (9)
O11^vi—Co2—O12	162.06 (19)	Mo2^x—K2—Mo1^viii	100.97 (5)
O8^vi—Co2—O12	85.46 (18)	Co1^xi—K2—Mo1^viii	124.32 (6)
O3—Co2—O11^v	174.29 (19)	Mo1^xi—K2—Mo1^viii	127.29 (7)
O7^v—Co2—O11^v	83.01 (17)	K1—K2—Mo1^viii	58.29 (4)
O11^vi—Co2—O11^v	82.75 (18)	Mo2^xi—K2—Mo1^viii	77.32 (4)
O8^vi—Co2—O11^v	85.54 (18)	Mo1—O1—K2	167.3 (3)
O12—Co2—O11^v	81.10 (18)	Mo1—O1—K1	89.1 (2)
O3—Co2—K1	51.08 (16)	K2—O1—K1	82.37 (16)
O7^v—Co2—K1	49.17 (13)	Mo1—O2—Co1	131.4 (3)
O11^vi—Co2—K1	114.71 (13)	Mo1—O2—K2^i	112.6 (2)
O8^vi—Co2—K1	141.29 (13)	Co1—O2—K2^i	101.46 (18)
O12—Co2—K1	81.63 (13)	Mo1—O3—Co2	127.2 (3)
O11^v—Co2—K1	127.67 (12)	Mo1—O3—K1	108.7 (2)
O5^vii—K1—O7^v	100.88 (16)	Co2—O3—K1	94.81 (19)
O5^vii—K1—O4^viii	72.27 (15)	Mo1—O4—Co1^viii	122.0 (2)
O7^v—K1—O4^viii	172.30 (16)	Mo1—O4—K1^ii	116.8 (2)
O5^vii—K1—O3	85.55 (15)	Co1^viii—O4—K1^ii	98.70 (18)
O7^v—K1—O3	66.95 (15)	Mo1—O4—K2^ii	111.7 (2)
O4^viii—K1—O3	108.35 (15)	Co1^viii—O4—K2^ii	113.63 (19)
O5^vii—K1—O10^ix	90.08 (14)	K1^ii—O4—K2^ii	88.45 (14)
O7^v—K1—O10^ix	116.07 (15)	Mo2—O6—Co1	140.6 (3)
O4^viii—K1—O10^ix	68.21 (14)	Mo2—O6—K2^i	119.9 (2)
O3—K1—O10^ix	175.16 (15)	Co1—O6—K2^i	99.29 (18)
O5^vii—K1—O9	159.06 (16)	Mo2—O5—K2^iii	114.3 (2)
O7^v—K1—O9	90.19 (16)	Mo2—O5—K1^iv	119.6 (2)
O4^viii—K1—O9	95.28 (15)	K2^iii—O5—K1^iv	125.06 (19)
O3—K1—O9	82.51 (15)	Mo2—O7—Co2^v	121.3 (2)
O10^ix—K1—O9	101.03 (16)	Mo2—O7—K1^v	142.1 (2)
O5^vii—K1—O1	103.85 (15)	Co2^v—O7—K1^v	96.52 (18)
O7^v—K1—O1	112.50 (15)	Mo2—O8—Co2^xii	119.8 (2)
O4^viii—K1—O1	66.82 (13)	Mo2—O8—Co1^xii	137.6 (3)
O3—K1—O1	53.97 (14)	Co2^xii—O8—Co1^xii	98.22 (18)
O10^ix—K1—O1	125.48 (14)	Mo3—O9—K1	103.0 (2)
O9—K1—O1	55.27 (14)	Mo3—O9—K2	170.7 (3)
O5^vii—K1—Co2	101.10 (12)	K1—O9—K2	85.64 (16)
O7^v—K1—Co2	34.32 (10)	Mo3—O10—Co1^v	119.2 (2)
O4^viii—K1—Co2	142.10 (11)	Mo3—O10—K1^ix	136.2 (2)
O3—K1—Co2	34.11 (10)	Co1^v—O10—K1^ix	94.47 (17)
O10^ix—K1—Co2	149.62 (12)	Mo3—O11—Co2^xii	140.6 (3)
O9—K1—Co2	78.15 (12)	Mo3—O11—Co2^v	112.5 (2)
O1—K1—Co2	79.41 (10)	Co2^xii—O11—Co2^v	97.25 (18)
O5^vii—K1—Co1^x	74.50 (11)	Mo3—O12—Co2	131.0 (2)
O7^v—K1—Co1^x	148.90 (12)	Mo3—O12—Co1	132.5 (2)
O4^viii—K1—Co1^x	33.80 (10)	Co2—O12—Co1	94.35 (18)
O3—K1—Co1^x	140.98 (12)
O3—Co2—K1—O5^vii	−64.5 (2)	Co2—K1—K2—Mo1^viii	−114.95 (6)
O7^v—Co2—K1—O5^vii	93.1 (2)	Co1^x—K1—K2—Mo1^viii	59.10 (3)
O11^vi—Co2—K1—O5^vii	22.26 (18)	Mo3—K1—K2—Mo1^viii	−159.57 (4)
O8^vi—Co2—K1—O5^vii	−93.7 (2)	Mo1—K1—K2—Mo1^viii	−82.37 (3)
O12—Co2—K1—O5^vii	−165.52 (17)	Mo2^vii—K1—K2—Mo1^viii	27.58 (4)
O11^v—Co2—K1—O5^vii	122.61 (18)	O2—Mo1—O1—K2	70.2 (15)
O3—Co2—K1—O7^v	−157.6 (3)	O3—Mo1—O1—K2	−47.7 (16)
O11^vi—Co2—K1—O7^v	−70.8 (2)	O4—Mo1—O1—K2	−167.7 (15)
O8^vi—Co2—K1—O7^v	173.2 (3)	K1—Mo1—O1—K2	−47.7 (15)
O12—Co2—K1—O7^v	101.4 (2)	K2^i—Mo1—O1—K2	84.7 (15)
O11^v—Co2—K1—O7^v	29.5 (2)	K1^ii—Mo1—O1—K2	150.9 (15)
O3—Co2—K1—O4^viii	10.8 (3)	K2^ii—Mo1—O1—K2	−145.8 (12)
O7^v—Co2—K1—O4^viii	168.4 (3)	O2—Mo1—O1—K1	117.92 (19)
O11^vi—Co2—K1—O4^viii	97.6 (2)	O3—Mo1—O1—K1	0.0 (2)
O8^vi—Co2—K1—O4^viii	−18.3 (3)	O4—Mo1—O1—K1	−120.04 (18)
O12—Co2—K1—O4^viii	−90.2 (2)	K2^i—Mo1—O1—K1	132.42 (15)
O11^v—Co2—K1—O4^viii	−162.1 (2)	K1^ii—Mo1—O1—K1	−161.41 (5)
O7^v—Co2—K1—O3	157.6 (3)	K2^ii—Mo1—O1—K1	−98.1 (4)
O11^vi—Co2—K1—O3	86.8 (2)	O5^x—K2—O1—Mo1	1.8 (17)
O8^vi—Co2—K1—O3	−29.2 (3)	O2^xi—K2—O1—Mo1	−108.3 (15)
O12—Co2—K1—O3	−101.0 (2)	O6^xi—K2—O1—Mo1	−135.7 (15)
O11^v—Co2—K1—O3	−172.9 (2)	O9—K2—O1—Mo1	−6.0 (15)
O3—Co2—K1—O10^ix	−174.2 (3)	O4^viii—K2—O1—Mo1	92.0 (15)
O7^v—Co2—K1—O10^ix	−16.6 (3)	Mo2^x—K2—O1—Mo1	40.3 (17)
O11^vi—Co2—K1—O10^ix	−87.5 (3)	Co1^xi—K2—O1—Mo1	−121.0 (15)
O8^vi—Co2—K1—O10^ix	156.6 (3)	Mo1^xi—K2—O1—Mo1	−120.4 (14)
O12—Co2—K1—O10^ix	84.8 (3)	K1—K2—O1—Mo1	48.2 (15)
O11^v—Co2—K1—O10^ix	12.9 (3)	Mo2^xi—K2—O1—Mo1	−150.4 (16)
O3—Co2—K1—O9	94.1 (2)	Mo1^viii—K2—O1—Mo1	115.9 (16)
O7^v—Co2—K1—O9	−108.3 (2)	O5^x—K2—O1—K1	−46.5 (3)
O11^vi—Co2—K1—O9	−179.10 (18)	O2^xi—K2—O1—K1	−156.57 (19)
O8^vi—Co2—K1—O9	65.0 (2)	O6^xi—K2—O1—K1	176.03 (16)
O12—Co2—K1—O9	−6.88 (17)	O9—K2—O1—K1	−54.21 (15)
O11^v—Co2—K1—O9	−78.75 (18)	O4^viii—K2—O1—K1	43.80 (12)
O3—Co2—K1—O1	37.7 (2)	Mo2^x—K2—O1—K1	−7.9 (3)
O7^v—Co2—K1—O1	−164.70 (19)	Co1^xi—K2—O1—K1	−169.21 (9)
O11^vi—Co2—K1—O1	124.47 (17)	Mo1^xi—K2—O1—K1	−168.7 (3)
O8^vi—Co2—K1—O1	8.5 (2)	Mo2^xi—K2—O1—K1	161.41 (17)
O12—Co2—K1—O1	−63.30 (16)	Mo1^viii—K2—O1—K1	67.65 (9)
O11^v—Co2—K1—O1	−135.18 (17)	O5^vii—K1—O1—Mo1	73.8 (2)
O3—Co2—K1—Co1^x	−28.3 (6)	O7^v—K1—O1—Mo1	−34.4 (2)
O7^v—Co2—K1—Co1^x	129.3 (6)	O4^viii—K1—O1—Mo1	137.3 (2)
O11^vi—Co2—K1—Co1^x	58.5 (6)	O3—K1—O1—Mo1	−0.02 (16)
O8^vi—Co2—K1—Co1^x	−57.4 (7)	O10^ix—K1—O1—Mo1	174.06 (18)
O12—Co2—K1—Co1^x	−129.3 (6)	O9—K1—O1—Mo1	−108.0 (2)
O11^v—Co2—K1—Co1^x	158.8 (6)	Co2—K1—O1—Mo1	−25.12 (16)
O3—Co2—K1—Mo3	113.57 (18)	Co1^x—K1—O1—Mo1	149.82 (17)
O7^v—Co2—K1—Mo3	−88.85 (18)	Mo3—K1—O1—Mo1	−85.33 (18)
O11^vi—Co2—K1—Mo3	−159.67 (14)	Mo2^vii—K1—O1—Mo1	91.56 (19)
O8^vi—Co2—K1—Mo3	84.4 (2)	O5^vii—K1—O1—K2	−115.64 (17)
O12—Co2—K1—Mo3	12.55 (13)	O7^v—K1—O1—K2	136.14 (16)
O11^v—Co2—K1—Mo3	−59.33 (15)	O4^viii—K1—O1—K2	−52.18 (15)
O3—Co2—K1—Mo1	23.96 (18)	O3—K1—O1—K2	170.5 (2)
O7^v—Co2—K1—Mo1	−178.46 (18)	O10^ix—K1—O1—K2	−15.4 (2)
O11^vi—Co2—K1—Mo1	110.71 (14)	O9—K1—O1—K2	62.56 (17)
O8^vi—Co2—K1—Mo1	−5.2 (2)	Co2—K1—O1—K2	145.41 (14)
O12—Co2—K1—Mo1	−77.07 (14)	Co1^x—K1—O1—K2	−39.66 (13)
O11^v—Co2—K1—Mo1	−148.94 (15)	Mo3—K1—O1—K2	85.20 (12)
O3—Co2—K1—Mo2^vii	−80.66 (18)	Mo1—K1—O1—K2	170.5 (3)
O7^v—Co2—K1—Mo2^vii	76.92 (19)	Mo2^vii—K1—O1—K2	−97.92 (13)
O11^vi—Co2—K1—Mo2^vii	6.09 (15)	O1—Mo1—O2—Co1	−110.5 (4)
O8^vi—Co2—K1—Mo2^vii	−109.8 (2)	O3—Mo1—O2—Co1	6.8 (4)
O12—Co2—K1—Mo2^vii	178.31 (14)	O4—Mo1—O2—Co1	128.0 (3)
O11^v—Co2—K1—Mo2^vii	106.44 (15)	K1—Mo1—O2—Co1	−40.9 (4)
O9—Mo3—K1—O5^vii	−127.7 (4)	K2^i—Mo1—O2—Co1	−130.9 (5)
O10—Mo3—K1—O5^vii	109.3 (4)	K1^ii—Mo1—O2—Co1	143.6 (4)
O11—Mo3—K1—O5^vii	−137.2 (5)	K2^ii—Mo1—O2—Co1	85.9 (3)
O12—Mo3—K1—O5^vii	−9.1 (4)	O1—Mo1—O2—K2^i	20.3 (3)
O9—Mo3—K1—O7^v	−172.1 (3)	O3—Mo1—O2—K2^i	137.7 (2)
O10—Mo3—K1—O7^v	64.98 (19)	O4—Mo1—O2—K2^i	−101.2 (2)
O11—Mo3—K1—O7^v	178.5 (4)	K1—Mo1—O2—K2^i	89.9 (2)
O12—Mo3—K1—O7^v	−53.48 (19)	K1^ii—Mo1—O2—K2^i	−85.49 (18)
O9—Mo3—K1—O4^viii	2.0 (3)	K2^ii—Mo1—O2—K2^i	−143.27 (18)
O10—Mo3—K1—O4^viii	−121.0 (2)	O4^ii—Co1—O2—Mo1	−138.7 (4)
O11—Mo3—K1—O4^viii	−7.5 (4)	O6—Co1—O2—Mo1	128.4 (4)
O12—Mo3—K1—O4^viii	120.6 (2)	O10^v—Co1—O2—Mo1	14.4 (13)
O9—Mo3—K1—O3	−101.2 (3)	O8^vi—Co1—O2—Mo1	−44.1 (4)
O10—Mo3—K1—O3	135.84 (19)	O12—Co1—O2—Mo1	36.5 (4)
O11—Mo3—K1—O3	−110.7 (4)	K1^iii—Co1—O2—Mo1	−121.4 (3)
O12—Mo3—K1—O3	17.38 (19)	K2^i—Co1—O2—Mo1	134.6 (5)
O9—Mo3—K1—O10^ix	77.3 (3)	O4^ii—Co1—O2—K2^i	86.7 (2)
O10—Mo3—K1—O10^ix	−45.6 (2)	O6—Co1—O2—K2^i	−6.2 (2)
O11—Mo3—K1—O10^ix	67.9 (4)	O10^v—Co1—O2—K2^i	−120.2 (10)
O12—Mo3—K1—O10^ix	−164.08 (19)	O8^vi—Co1—O2—K2^i	−178.62 (19)
O10—Mo3—K1—O9	−122.9 (3)	O12—Co1—O2—K2^i	−98.07 (19)
O11—Mo3—K1—O9	−9.4 (5)	K1^iii—Co1—O2—K2^i	104.03 (19)
O12—Mo3—K1—O9	118.6 (3)	O1—Mo1—O3—Co2	111.6 (4)
O9—Mo3—K1—O1	−45.1 (3)	O2—Mo1—O3—Co2	−5.6 (4)
O10—Mo3—K1—O1	−168.04 (19)	O4—Mo1—O3—Co2	−127.8 (3)
O11—Mo3—K1—O1	−54.5 (4)	K1—Mo1—O3—Co2	111.6 (4)
O12—Mo3—K1—O1	73.50 (18)	K2^i—Mo1—O3—Co2	34.2 (5)
O9—Mo3—K1—Co2	−133.2 (2)	K1^ii—Mo1—O3—Co2	−95.4 (3)
O10—Mo3—K1—Co2	103.86 (16)	K2^ii—Mo1—O3—Co2	−97.3 (3)
O11—Mo3—K1—Co2	−142.6 (4)	O1—Mo1—O3—K1	0.0 (3)
O12—Mo3—K1—Co2	−14.60 (16)	O2—Mo1—O3—K1	−117.2 (2)
O9—Mo3—K1—Co1^x	42.6 (3)	O4—Mo1—O3—K1	120.6 (2)
O10—Mo3—K1—Co1^x	−80.31 (17)	K2^i—Mo1—O3—K1	−77.4 (3)
O11—Mo3—K1—Co1^x	33.2 (4)	K1^ii—Mo1—O3—K1	152.99 (11)
O12—Mo3—K1—Co1^x	161.23 (17)	K2^ii—Mo1—O3—K1	151.1 (2)
O9—Mo3—K1—Mo1	−73.8 (2)	O7^v—Co2—O3—Mo1	−134.8 (3)
O10—Mo3—K1—Mo1	163.24 (16)	O11^vi—Co2—O3—Mo1	130.6 (3)
O11—Mo3—K1—Mo1	−83.3 (4)	O8^vi—Co2—O3—Mo1	44.3 (4)
O12—Mo3—K1—Mo1	44.78 (16)	O12—Co2—O3—Mo1	−41.4 (4)
O9—Mo3—K1—Mo2^vii	147.2 (4)	O11^v—Co2—O3—Mo1	−38 (2)
O10—Mo3—K1—Mo2^vii	24.3 (3)	K1—Co2—O3—Mo1	−117.9 (4)
O11—Mo3—K1—Mo2^vii	137.8 (4)	O7^v—Co2—O3—K1	−16.92 (19)
O12—Mo3—K1—Mo2^vii	−94.2 (3)	O11^vi—Co2—O3—K1	−111.51 (17)
O1—Mo1—K1—O5^vii	−110.6 (2)	O8^vi—Co2—O3—K1	162.22 (16)
O2—Mo1—K1—O5^vii	154.2 (2)	O12—Co2—O3—K1	76.56 (17)
O3—Mo1—K1—O5^vii	69.4 (3)	O11^v—Co2—O3—K1	80 (2)
O4—Mo1—K1—O5^vii	−13.1 (2)	O5^vii—K1—O3—Mo1	−110.7 (2)
K2^i—Mo1—K1—O5^vii	−158.98 (12)	O7^v—K1—O3—Mo1	145.5 (3)
K1^ii—Mo1—K1—O5^vii	−39.87 (13)	O4^viii—K1—O3—Mo1	−41.0 (2)
K2^ii—Mo1—K1—O5^vii	37.47 (12)	O10^ix—K1—O3—Mo1	−85.1 (18)
O1—Mo1—K1—O7^v	148.5 (2)	O9—K1—O3—Mo1	52.1 (2)
O2—Mo1—K1—O7^v	53.3 (2)	O1—K1—O3—Mo1	0.02 (16)
O3—Mo1—K1—O7^v	−31.4 (2)	Co2—K1—O3—Mo1	132.0 (3)
O4—Mo1—K1—O7^v	−114.0 (2)	Co1^x—K1—O3—Mo1	−52.1 (3)
K2^i—Mo1—K1—O7^v	100.15 (11)	Mo3—K1—O3—Mo1	78.3 (2)
K1^ii—Mo1—K1—O7^v	−140.74 (12)	Mo2^vii—K1—O3—Mo1	−114.16 (19)
K2^ii—Mo1—K1—O7^v	−63.40 (11)	O5^vii—K1—O3—Co2	117.33 (19)
O1—Mo1—K1—O4^viii	−38.6 (2)	O7^v—K1—O3—Co2	13.51 (16)
O2—Mo1—K1—O4^viii	−133.8 (2)	O4^viii—K1—O3—Co2	−173.02 (17)
O3—Mo1—K1—O4^viii	141.4 (2)	O10^ix—K1—O3—Co2	142.9 (18)
O4—Mo1—K1—O4^viii	58.8 (3)	O9—K1—O3—Co2	−79.91 (18)
K2^i—Mo1—K1—O4^viii	−87.01 (11)	O1—K1—O3—Co2	−132.0 (2)
K1^ii—Mo1—K1—O4^viii	32.10 (12)	Co1^x—K1—O3—Co2	175.88 (9)
K2^ii—Mo1—K1—O4^viii	109.44 (11)	Mo3—K1—O3—Co2	−53.70 (14)
O1—Mo1—K1—O3	180.0 (3)	Mo1—K1—O3—Co2	−132.0 (3)
O2—Mo1—K1—O3	84.8 (3)	Mo2^vii—K1—O3—Co2	113.86 (14)
O4—Mo1—K1—O3	−82.6 (3)	O1—Mo1—O4—Co1^viii	25.8 (4)
K2^i—Mo1—K1—O3	131.6 (2)	O2—Mo1—O4—Co1^viii	145.8 (3)
K1^ii—Mo1—K1—O3	−109.3 (2)	O3—Mo1—O4—Co1^viii	−93.4 (3)
K2^ii—Mo1—K1—O3	−32.0 (2)	K1—Mo1—O4—Co1^viii	−45.7 (3)
O1—Mo1—K1—O10^ix	−10.6 (3)	K2^i—Mo1—O4—Co1^viii	100.3 (3)
O2—Mo1—K1—O10^ix	−105.8 (3)	K1^ii—Mo1—O4—Co1^viii	121.1 (4)
O3—Mo1—K1—O10^ix	169.5 (3)	K2^ii—Mo1—O4—Co1^viii	−139.2 (4)
O4—Mo1—K1—O10^ix	86.9 (3)	O1—Mo1—O4—K1^ii	−95.2 (3)
K2^i—Mo1—K1—O10^ix	−59.0 (2)	O2—Mo1—O4—K1^ii	24.7 (3)
K1^ii—Mo1—K1—O10^ix	60.2 (2)	O3—Mo1—O4—K1^ii	145.5 (2)
K2^ii—Mo1—K1—O10^ix	137.5 (2)	K1—Mo1—O4—K1^ii	−166.76 (9)
O1—Mo1—K1—O9	58.1 (2)	K2^i—Mo1—O4—K1^ii	−20.8 (2)
O2—Mo1—K1—O9	−37.1 (2)	K2^ii—Mo1—O4—K1^ii	99.7 (2)
O3—Mo1—K1—O9	−121.9 (3)	O1—Mo1—O4—K2^ii	165.1 (2)
O4—Mo1—K1—O9	155.5 (2)	O2—Mo1—O4—K2^ii	−75.0 (2)
K2^i—Mo1—K1—O9	9.68 (12)	O3—Mo1—O4—K2^ii	45.8 (3)
K1^ii—Mo1—K1—O9	128.80 (13)	K1—Mo1—O4—K2^ii	93.56 (17)
K2^ii—Mo1—K1—O9	−153.86 (12)	K2^i—Mo1—O4—K2^ii	−120.49 (16)
O2—Mo1—K1—O1	−95.2 (3)	K1^ii—Mo1—O4—K2^ii	−99.7 (2)
O3—Mo1—K1—O1	−180.0 (3)	O5—Mo2—O6—Co1	−95.8 (4)
O4—Mo1—K1—O1	97.5 (3)	O7—Mo2—O6—Co1	19.1 (5)
K2^i—Mo1—K1—O1	−48.4 (2)	O8—Mo2—O6—Co1	144.7 (4)
K1^ii—Mo1—K1—O1	70.7 (2)	K2^iii—Mo2—O6—Co1	−96.0 (4)
K2^ii—Mo1—K1—O1	148.1 (2)	K1^iv—Mo2—O6—Co1	−107.4 (4)
O1—Mo1—K1—Co2	149.4 (2)	K2^i—Mo2—O6—Co1	173.5 (6)
O2—Mo1—K1—Co2	54.20 (19)	O5—Mo2—O6—K2^i	90.7 (3)
O3—Mo1—K1—Co2	−30.6 (2)	O7—Mo2—O6—K2^i	−154.3 (2)
O4—Mo1—K1—Co2	−113.13 (18)	O8—Mo2—O6—K2^i	−28.7 (3)
K2^i—Mo1—K1—Co2	101.01 (4)	K2^iii—Mo2—O6—K2^i	90.6 (2)
K1^ii—Mo1—K1—Co2	−139.87 (7)	K1^iv—Mo2—O6—K2^i	79.2 (3)
K2^ii—Mo1—K1—Co2	−62.53 (4)	O2—Co1—O6—Mo2	−168.2 (4)
O1—Mo1—K1—Co1^x	−35.7 (2)	O4^ii—Co1—O6—Mo2	99.4 (4)
O2—Mo1—K1—Co1^x	−130.88 (19)	O10^v—Co1—O6—Mo2	2.5 (4)
O3—Mo1—K1—Co1^x	144.4 (2)	O8^vi—Co1—O6—Mo2	−57.2 (15)
O4—Mo1—K1—Co1^x	61.79 (19)	O12—Co1—O6—Mo2	−78.5 (4)
K2^i—Mo1—K1—Co1^x	−84.07 (6)	K1^iii—Co1—O6—Mo2	52.2 (4)
K1^ii—Mo1—K1—Co1^x	35.05 (8)	K2^i—Co1—O6—Mo2	−174.3 (5)
K2^ii—Mo1—K1—Co1^x	112.39 (6)	O2—Co1—O6—K2^i	6.0 (2)
O1—Mo1—K1—Mo3	85.8 (2)	O4^ii—Co1—O6—K2^i	−86.30 (18)
O2—Mo1—K1—Mo3	−9.38 (19)	O10^v—Co1—O6—K2^i	176.75 (17)
O3—Mo1—K1—Mo3	−94.1 (2)	O8^vi—Co1—O6—K2^i	117.1 (13)
O4—Mo1—K1—Mo3	−176.71 (18)	O12—Co1—O6—K2^i	95.76 (18)
K2^i—Mo1—K1—Mo3	37.43 (4)	K1^iii—Co1—O6—K2^i	−133.50 (12)
K1^ii—Mo1—K1—Mo3	156.55 (6)	O6—Mo2—O5—K2^iii	−0.2 (3)
K2^ii—Mo1—K1—Mo3	−126.12 (4)	O7—Mo2—O5—K2^iii	−119.6 (2)
O1—Mo1—K1—Mo2^vii	−103.5 (2)	O8—Mo2—O5—K2^iii	122.8 (2)
O2—Mo1—K1—Mo2^vii	161.28 (19)	K1^iv—Mo2—O5—K2^iii	168.7 (4)
O3—Mo1—K1—Mo2^vii	76.5 (2)	K2^i—Mo2—O5—K2^iii	38.9 (2)
O4—Mo1—K1—Mo2^vii	−6.05 (19)	O6—Mo2—O5—K1^iv	−168.9 (2)
K2^i—Mo1—K1—Mo2^vii	−151.91 (5)	O7—Mo2—O5—K1^iv	71.6 (3)
K1^ii—Mo1—K1—Mo2^vii	−32.79 (8)	O8—Mo2—O5—K1^iv	−45.9 (3)
K2^ii—Mo1—K1—Mo2^vii	44.55 (6)	K2^iii—Mo2—O5—K1^iv	−168.7 (4)
O5^vii—K1—K2—O1	79.5 (2)	K2^i—Mo2—O5—K1^iv	−129.9 (2)
O7^v—K1—K2—O1	−68.2 (2)	O5—Mo2—O7—Co2^v	−157.1 (3)
O4^viii—K1—K2—O1	103.3 (2)	O6—Mo2—O7—Co2^v	86.3 (3)
O3—K1—K2—O1	−7.68 (19)	O8—Mo2—O7—Co2^v	−41.2 (3)
O10^ix—K1—K2—O1	167.47 (18)	K2^iii—Mo2—O7—Co2^v	161.58 (18)
O9—K1—K2—O1	−83.4 (2)	K1^iv—Mo2—O7—Co2^v	−121.8 (3)
Co2—K1—K2—O1	−37.26 (16)	K2^i—Mo2—O7—Co2^v	59.7 (4)
Co1^x—K1—K2—O1	136.79 (16)	O5—Mo2—O7—K1^v	25.9 (4)
Mo3—K1—K2—O1	−81.89 (15)	O6—Mo2—O7—K1^v	−90.7 (4)
Mo1—K1—K2—O1	−4.69 (15)	O8—Mo2—O7—K1^v	141.9 (4)
Mo2^vii—K1—K2—O1	105.26 (16)	K2^iii—Mo2—O7—K1^v	−15.4 (5)
O5^vii—K1—K2—O5^x	−129.1 (2)	K1^iv—Mo2—O7—K1^v	61.2 (4)
O7^v—K1—K2—O5^x	83.2 (2)	K2^i—Mo2—O7—K1^v	−117.2 (3)
O4^viii—K1—K2—O5^x	−105.31 (18)	O5—Mo2—O8—Co2^xii	164.3 (2)
O3—K1—K2—O5^x	143.75 (16)	O6—Mo2—O8—Co2^xii	−76.4 (3)
O10^ix—K1—K2—O5^x	−41.10 (16)	O7—Mo2—O8—Co2^xii	50.1 (3)
O9—K1—K2—O5^x	68.01 (19)	K2^iii—Mo2—O8—Co2^xii	−153.78 (15)
O1—K1—K2—O5^x	151.4 (2)	K1^iv—Mo2—O8—Co2^xii	138.0 (2)
Co2—K1—K2—O5^x	114.17 (12)	K2^i—Mo2—O8—Co2^xii	−93.7 (2)
Co1^x—K1—K2—O5^x	−71.78 (12)	O5—Mo2—O8—Co1^xii	13.6 (4)
Mo3—K1—K2—O5^x	69.55 (12)	O6—Mo2—O8—Co1^xii	132.9 (3)
Mo1—K1—K2—O5^x	146.75 (13)	O7—Mo2—O8—Co1^xii	−100.6 (4)
Mo2^vii—K1—K2—O5^x	−103.30 (13)	K2^iii—Mo2—O8—Co1^xii	55.5 (4)
O5^vii—K1—K2—O2^xi	−160.5 (4)	K1^iv—Mo2—O8—Co1^xii	−12.7 (3)
O7^v—K1—K2—O2^xi	51.8 (4)	K2^i—Mo2—O8—Co1^xii	115.6 (3)
O4^viii—K1—K2—O2^xi	−136.7 (4)	O10—Mo3—O9—K1	57.1 (2)
O3—K1—K2—O2^xi	112.3 (4)	O11—Mo3—O9—K1	176.44 (18)
O10^ix—K1—K2—O2^xi	−72.5 (4)	O12—Mo3—O9—K1	−64.5 (3)
O9—K1—K2—O2^xi	36.6 (4)	O10—Mo3—O9—K2	−143.9 (18)
O1—K1—K2—O2^xi	120.0 (4)	O11—Mo3—O9—K2	−24.5 (19)
Co2—K1—K2—O2^xi	82.8 (4)	O12—Mo3—O9—K2	94.5 (18)
Co1^x—K1—K2—O2^xi	−103.2 (4)	K1—Mo3—O9—K2	159 (2)
Mo3—K1—K2—O2^xi	38.1 (4)	O5^vii—K1—O9—Mo3	129.6 (4)
Mo1—K1—K2—O2^xi	115.3 (4)	O7^v—K1—O9—Mo3	7.1 (2)
Mo2^vii—K1—K2—O2^xi	−134.7 (4)	O4^viii—K1—O9—Mo3	−178.3 (2)
O5^vii—K1—K2—O6^xi	74.7 (2)	O3—K1—O9—Mo3	73.8 (2)
O7^v—K1—K2—O6^xi	−73.0 (2)	O10^ix—K1—O9—Mo3	−109.5 (2)
O4^viii—K1—K2—O6^xi	98.5 (2)	O1—K1—O9—Mo3	124.7 (3)
O3—K1—K2—O6^xi	−12.44 (19)	Co2—K1—O9—Mo3	39.5 (2)
O10^ix—K1—K2—O6^xi	162.70 (18)	Co1^x—K1—O9—Mo3	−145.3 (2)
O9—K1—K2—O6^xi	−88.2 (2)	Mo1—K1—O9—Mo3	96.4 (2)
O1—K1—K2—O6^xi	−4.76 (19)	Mo2^vii—K1—O9—Mo3	−156.2 (3)
Co2—K1—K2—O6^xi	−42.02 (17)	O5^vii—K1—O9—K2	−47.1 (5)
Co1^x—K1—K2—O6^xi	132.03 (16)	O7^v—K1—O9—K2	−169.57 (15)
Mo3—K1—K2—O6^xi	−86.65 (16)	O4^viii—K1—O9—K2	5.00 (16)
Mo1—K1—K2—O6^xi	−9.45 (15)	O3—K1—O9—K2	−102.86 (16)
Mo2^vii—K1—K2—O6^xi	100.50 (16)	O10^ix—K1—O9—K2	73.79 (16)
O5^vii—K1—K2—O9	162.9 (2)	O1—K1—O9—K2	−51.97 (14)
O7^v—K1—K2—O9	15.2 (2)	Co2—K1—O9—K2	−137.21 (13)
O4^viii—K1—K2—O9	−173.3 (2)	Co1^x—K1—O9—K2	38.01 (14)
O3—K1—K2—O9	75.75 (19)	Mo3—K1—O9—K2	−176.7 (3)
O10^ix—K1—K2—O9	−109.10 (19)	Mo1—K1—O9—K2	−80.30 (11)
O1—K1—K2—O9	83.4 (2)	Mo2^vii—K1—O9—K2	27.1 (5)
Co2—K1—K2—O9	46.17 (16)	O1—K2—O9—Mo3	−91.4 (18)
Co1^x—K1—K2—O9	−139.78 (16)	O5^x—K2—O9—Mo3	93.9 (18)
Mo3—K1—K2—O9	1.54 (15)	O2^xi—K2—O9—Mo3	33.7 (19)
Mo1—K1—K2—O9	78.74 (16)	O6^xi—K2—O9—Mo3	−38.9 (19)
Mo2^vii—K1—K2—O9	−171.31 (17)	O4^viii—K2—O9—Mo3	−164.1 (18)
O5^vii—K1—K2—O4^viii	−23.79 (18)	Mo2^x—K2—O9—Mo3	116.5 (18)
O7^v—K1—K2—O4^viii	−171.5 (2)	Co1^xi—K2—O9—Mo3	−2.5 (19)
O3—K1—K2—O4^viii	−110.94 (16)	Mo1^xi—K2—O9—Mo3	61.6 (19)
O10^ix—K1—K2—O4^viii	64.21 (16)	K1—K2—O9—Mo3	−159.5 (19)
O9—K1—K2—O4^viii	173.3 (2)	Mo2^xi—K2—O9—Mo3	−62.3 (18)
O1—K1—K2—O4^viii	−103.3 (2)	Mo1^viii—K2—O9—Mo3	−143.1 (18)
Co2—K1—K2—O4^viii	−140.52 (14)	O1—K2—O9—K1	68.14 (18)
Co1^x—K1—K2—O4^viii	33.53 (13)	O5^x—K2—O9—K1	−106.59 (17)
Mo3—K1—K2—O4^viii	174.86 (14)	O2^xi—K2—O9—K1	−166.75 (14)
Mo1—K1—K2—O4^viii	−107.94 (13)	O6^xi—K2—O9—K1	120.67 (15)
Mo2^vii—K1—K2—O4^viii	2.01 (13)	O4^viii—K2—O9—K1	−4.58 (14)
O5^vii—K1—K2—Mo2^x	−105.69 (13)	Mo2^x—K2—O9—K1	−83.97 (11)
O7^v—K1—K2—Mo2^x	106.63 (17)	Co1^xi—K2—O9—K1	157.01 (9)
O4^viii—K1—K2—Mo2^x	−81.91 (13)	Mo1^xi—K2—O9—K1	−138.86 (10)
O3—K1—K2—Mo2^x	167.16 (11)	Mo2^xi—K2—O9—K1	97.28 (12)
O10^ix—K1—K2—Mo2^x	−17.70 (10)	Mo1^viii—K2—O9—K1	16.44 (14)
O9—K1—K2—Mo2^x	91.41 (16)	O9—Mo3—O10—Co1^v	171.5 (3)
O1—K1—K2—Mo2^x	174.84 (16)	O11—Mo3—O10—Co1^v	54.1 (3)
Co2—K1—K2—Mo2^x	137.58 (5)	O12—Mo3—O10—Co1^v	−73.1 (3)
Co1^x—K1—K2—Mo2^x	−48.37 (4)	K1—Mo3—O10—Co1^v	−146.6 (3)
Mo3—K1—K2—Mo2^x	92.95 (4)	O9—Mo3—O10—K1^ix	36.1 (4)
Mo1—K1—K2—Mo2^x	170.15 (6)	O11—Mo3—O10—K1^ix	−81.2 (3)
Mo2^vii—K1—K2—Mo2^x	−79.90 (6)	O12—Mo3—O10—K1^ix	151.6 (3)
O5^vii—K1—K2—Co1^xi	105.8 (2)	K1—Mo3—O10—K1^ix	78.1 (3)
O7^v—K1—K2—Co1^xi	−41.9 (3)	O9—Mo3—O11—Co2^xii	−29.4 (5)
O4^viii—K1—K2—Co1^xi	129.6 (2)	O10—Mo3—O11—Co2^xii	85.3 (4)
O3—K1—K2—Co1^xi	18.7 (2)	O12—Mo3—O11—Co2^xii	−145.3 (4)
O10^ix—K1—K2—Co1^xi	−166.19 (19)	K1—Mo3—O11—Co2^xii	−21.7 (7)
O9—K1—K2—Co1^xi	−57.1 (2)	O9—Mo3—O11—Co2^v	−165.3 (2)
O1—K1—K2—Co1^xi	26.3 (2)	O10—Mo3—O11—Co2^v	−50.6 (3)
Co2—K1—K2—Co1^xi	−10.9 (2)	O12—Mo3—O11—Co2^v	78.8 (3)
Co1^x—K1—K2—Co1^xi	163.13 (18)	K1—Mo3—O11—Co2^v	−157.6 (2)
Mo3—K1—K2—Co1^xi	−55.54 (18)	O9—Mo3—O12—Co2	73.7 (4)
Mo1—K1—K2—Co1^xi	21.66 (17)	O10—Mo3—O12—Co2	−40.9 (4)
Mo2^vii—K1—K2—Co1^xi	131.61 (16)	O11—Mo3—O12—Co2	−168.6 (3)
O5^vii—K1—K2—Mo1^xi	−109.09 (18)	K1—Mo3—O12—Co2	29.0 (3)
O7^v—K1—K2—Mo1^xi	103.2 (2)	O9—Mo3—O12—Co1	−85.1 (4)
O4^viii—K1—K2—Mo1^xi	−85.31 (19)	O10—Mo3—O12—Co1	160.3 (3)
O3—K1—K2—Mo1^xi	163.75 (16)	O11—Mo3—O12—Co1	32.6 (4)
O10^ix—K1—K2—Mo1^xi	−21.10 (17)	K1—Mo3—O12—Co1	−129.9 (3)
O9—K1—K2—Mo1^xi	88.0 (2)	O3—Co2—O12—Mo3	−80.0 (4)
O1—K1—K2—Mo1^xi	171.4 (2)	O7^v—Co2—O12—Mo3	17.9 (4)
Co2—K1—K2—Mo1^xi	134.17 (13)	O11^vi—Co2—O12—Mo3	126.4 (5)
Co1^x—K1—K2—Mo1^xi	−51.78 (13)	O8^vi—Co2—O12—Mo3	−173.5 (4)
Mo3—K1—K2—Mo1^xi	89.55 (14)	O11^v—Co2—O12—Mo3	100.3 (3)
Mo1—K1—K2—Mo1^xi	166.75 (15)	K1—Co2—O12—Mo3	−30.1 (3)
Mo2^vii—K1—K2—Mo1^xi	−83.30 (15)	O3—Co2—O12—Co1	84.5 (2)
O5^vii—K1—K2—Mo2^xi	64.07 (14)	O7^v—Co2—O12—Co1	−177.60 (18)
O7^v—K1—K2—Mo2^xi	−83.61 (17)	O11^vi—Co2—O12—Co1	−69.1 (6)
O4^viii—K1—K2—Mo2^xi	87.86 (14)	O8^vi—Co2—O12—Co1	−8.98 (18)
O3—K1—K2—Mo2^xi	−23.08 (12)	O11^v—Co2—O12—Co1	−95.16 (18)
O10^ix—K1—K2—Mo2^xi	152.07 (11)	K1—Co2—O12—Co1	134.43 (16)
O9—K1—K2—Mo2^xi	−98.83 (16)	O2—Co1—O12—Mo3	83.5 (4)
O1—K1—K2—Mo2^xi	−15.40 (14)	O4^ii—Co1—O12—Mo3	−166.4 (19)
Co2—K1—K2—Mo2^xi	−52.66 (8)	O6—Co1—O12—Mo3	−10.1 (4)
Co1^x—K1—K2—Mo2^xi	121.39 (7)	O10^v—Co1—O12—Mo3	−100.3 (4)
Mo3—K1—K2—Mo2^xi	−97.28 (6)	O8^vi—Co1—O12—Mo3	172.9 (4)
Mo1—K1—K2—Mo2^xi	−20.08 (5)	K1^iii—Co1—O12—Mo3	−115.8 (3)
Mo2^vii—K1—K2—Mo2^xi	89.87 (7)	K2^i—Co1—O12—Mo3	37.7 (3)
O5^vii—K1—K2—Mo1^viii	1.78 (12)	O2—Co1—O12—Co2	−80.6 (2)
O7^v—K1—K2—Mo1^viii	−145.90 (17)	O4^ii—Co1—O12—Co2	29 (2)
O4^viii—K1—K2—Mo1^viii	25.57 (13)	O6—Co1—O12—Co2	−174.26 (19)
O3—K1—K2—Mo1^viii	−85.37 (11)	O10^v—Co1—O12—Co2	95.5 (2)
O10^ix—K1—K2—Mo1^viii	89.78 (10)	O8^vi—Co1—O12—Co2	8.72 (18)
O9—K1—K2—Mo1^viii	−161.12 (16)	K1^iii—Co1—O12—Co2	80.1 (2)
O1—K1—K2—Mo1^viii	−77.69 (15)	K2^i—Co1—O12—Co2	−126.50 (14)

Symmetry codes: (i) −x+1, y+1/2, −z+1/2; (ii) −x, y+1/2, −z+1/2; (iii) x, y+1, z; (iv) x+1, y+1, z; (v) −x+1, −y+1, −z+1; (vi) x−1, y, z; (vii) x−1, y−1, z; (viii) −x, y−1/2, −z+1/2; (ix) −x+1, −y, −z+1; (x) x, y−1, z; (xi) −x+1, y−1/2, −z+1/2; (xii) x+1, y, z.

(beta)

Crystal data

Co2K2Mo3O12	F(000) = 2512
Mr = 675.88	Dx = 3.754 Mg m^−3
Monoclinic, C2/c	Mo Kα radiation, λ = 0.71073 Å
a = 7.0418 (3) Å	Cell parameters from 4486 reflections
b = 19.3329 (7) Å	θ = 2.3–29.2°
c = 17.7267 (7) Å	µ = 6.53 mm^−1
β = 97.608 (4)°	T = 298 K
V = 2392.04 (16) Å^3	Needle, blue
Z = 8	0.12 × 0.04 × 0.03 mm

Data collection

Oxford Diffraction Xcalibur (TM) Single Crystal X-ray Diffractometer with Sapphire CCD Detector.	3025 independent reflections
Radiation source: Enhance (Mo) X-ray Source	1739 reflections with I > 2σ(I)
Graphite monochromator	Rint = 0.071
Detector resolution: 8.4012 pixels mm^-1	θmax = 29.2°, θmin = 2.3°
Rotation method data acquisition using ω and phi scans.	h = −9→9
Absorption correction: analytical CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.31.4 (release 06-08-2006 CrysAlis171 .NET) (compiled Aug 6 2006,16:44:45) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)	k = −25→26
Tmin = 0.509, Tmax = 0.871	l = −23→24
15336 measured reflections

Refinement

Refinement on F^2	0 restraints
Least-squares matrix: full	Primary atom site location: structure-invariant direct methods
R[F^2 > 2σ(F^2)] = 0.038	Secondary atom site location: difference Fourier map
wR(F^2) = 0.121	w = 1/[σ^2(Fo^2) + (0.0529P)^2] where P = (Fo^2 + 2Fc^2)/3
S = 1.05	(Δ/σ)max < 0.001
3025 reflections	Δρmax = 1.76 e Å^−3
178 parameters	Δρmin = −1.78 e Å^−3

Special details

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F² against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F², conventional R-factors R are based on F, with F set to zero for negative F². The threshold expression of F² > σ(F²) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F² are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq	Occ. (<1)
Mo1	0.44455 (12)	0.54543 (4)	0.36986 (5)	0.0130 (2)
Mo2	−0.12869 (12)	0.63426 (5)	0.59743 (5)	0.0146 (2)
Mo3	0.09676 (12)	0.72629 (4)	0.41307 (5)	0.0132 (2)
Co1	0.34851 (18)	0.60621 (7)	0.54411 (7)	0.0138 (3)
Co2	0.60605 (18)	0.69965 (7)	0.44820 (7)	0.0139 (3)
K1	0.5000	0.39013 (19)	0.2500	0.0359 (10)
K2	−0.0624 (4)	0.53650 (13)	0.35597 (17)	0.0360 (7)
K3	0.6121 (9)	0.6985 (3)	0.2478 (3)	0.048 (2)	0.532 (9)
O1	0.2949 (10)	0.5470 (4)	0.2850 (4)	0.0207 (16)
O2	0.3062 (10)	0.5473 (3)	0.4456 (4)	0.0189 (16)
O3	0.5938 (10)	0.6206 (3)	0.3720 (4)	0.0195 (16)
O4	0.5915 (9)	0.4704 (3)	0.3759 (4)	0.0154 (16)
O5	−0.1570 (11)	0.5871 (4)	0.6769 (4)	0.0280 (18)
O6	0.0602 (9)	0.5976 (4)	0.5559 (4)	0.0214 (17)
O7	−0.0766 (9)	0.7209 (4)	0.6286 (4)	0.0185 (16)
O8	−0.3549 (9)	0.6278 (3)	0.5362 (4)	0.0151 (15)
O9	0.0419 (12)	0.6736 (4)	0.3378 (4)	0.034 (2)
O10	0.1213 (9)	0.8099 (3)	0.3751 (4)	0.0177 (16)
O11	−0.0987 (9)	0.7202 (3)	0.4664 (4)	0.0145 (15)
O12	0.3185 (9)	0.6925 (3)	0.4651 (4)	0.0153 (15)

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
Mo1	0.0126 (5)	0.0095 (4)	0.0165 (4)	−0.0004 (4)	0.0007 (4)	0.0004 (4)
Mo2	0.0123 (5)	0.0118 (5)	0.0191 (4)	0.0006 (4)	0.0002 (4)	0.0023 (4)
Mo3	0.0127 (5)	0.0101 (5)	0.0167 (4)	0.0003 (4)	0.0011 (4)	0.0014 (4)
Co1	0.0131 (7)	0.0105 (7)	0.0178 (7)	−0.0002 (6)	0.0022 (6)	0.0017 (6)
Co2	0.0123 (7)	0.0110 (7)	0.0183 (7)	−0.0007 (6)	0.0023 (6)	0.0000 (6)
K1	0.058 (3)	0.031 (2)	0.0187 (17)	0.000	0.0042 (18)	0.000
K2	0.0162 (13)	0.0261 (15)	0.0646 (19)	−0.0006 (11)	0.0012 (13)	0.0067 (14)
K3	0.084 (5)	0.034 (4)	0.023 (3)	0.004 (3)	0.004 (3)	−0.003 (2)
O1	0.019 (4)	0.023 (4)	0.018 (4)	0.001 (3)	−0.003 (3)	0.005 (3)
O2	0.018 (4)	0.009 (4)	0.030 (4)	−0.007 (3)	0.005 (3)	−0.004 (3)
O3	0.022 (4)	0.014 (4)	0.022 (4)	−0.012 (3)	0.003 (3)	−0.001 (3)
O4	0.014 (4)	0.017 (4)	0.016 (3)	0.001 (3)	0.007 (3)	−0.001 (3)
O5	0.034 (5)	0.018 (4)	0.030 (4)	−0.003 (4)	−0.004 (4)	0.004 (3)
O6	0.013 (4)	0.019 (4)	0.034 (4)	−0.006 (3)	0.007 (3)	−0.002 (3)
O7	0.019 (4)	0.017 (4)	0.020 (4)	−0.009 (3)	0.002 (3)	−0.003 (3)
O8	0.008 (3)	0.015 (4)	0.023 (4)	−0.001 (3)	0.004 (3)	0.005 (3)
O9	0.047 (5)	0.024 (5)	0.028 (4)	−0.005 (4)	−0.006 (4)	0.000 (4)
O10	0.021 (4)	0.014 (4)	0.018 (3)	−0.003 (3)	0.001 (3)	0.001 (3)
O11	0.009 (3)	0.012 (4)	0.022 (3)	0.001 (3)	−0.003 (3)	0.000 (3)
O12	0.012 (4)	0.013 (4)	0.023 (4)	0.003 (3)	0.012 (3)	0.004 (3)

Geometric parameters (Å, º)

Mo1—O1	1.718 (7)	K1—Mo1^ii	3.729 (3)
Mo1—O2	1.761 (7)	K1—Mo2^iii	4.0306 (10)
Mo1—O4	1.776 (7)	K1—Mo2^viii	4.0306 (10)
Mo1—O3	1.791 (6)	K2—O9	2.781 (8)
Mo1—K2^i	3.517 (3)	K2—O1^x	2.808 (7)
Mo1—K2	3.550 (3)	K2—O4^xi	2.815 (7)
Mo1—K3^ii	3.612 (5)	K2—O2	2.866 (8)
Mo1—K1	3.729 (3)	K2—O5^iii	2.946 (8)
Mo1—K3	3.937 (6)	K2—O3^xi	2.961 (8)
Mo2—O5	1.712 (7)	K2—O1	2.965 (7)
Mo2—O6	1.753 (7)	K2—O6^iii	3.026 (7)
Mo2—O7	1.786 (7)	K2—Mo1^xi	3.517 (3)
Mo2—O8	1.810 (6)	K2—Mo2^iii	3.619 (3)
Mo2—K2^iii	3.619 (3)	K3—K3^ii	1.590 (13)
Mo2—K1^iii	4.0306 (10)	K3—O3	2.684 (8)
Mo3—O9	1.683 (7)	K3—O7^v	2.727 (8)
Mo3—O10	1.768 (7)	K3—O7^xii	2.814 (9)
Mo3—O11	1.774 (7)	K3—O3^ii	2.840 (9)
Mo3—O12	1.826 (7)	K3—O9^ii	3.074 (10)
Mo3—K3^ii	3.766 (6)	K3—O1^ii	3.074 (9)
Mo3—K2	3.930 (3)	K3—O9^i	3.264 (10)
Co1—O4^iv	2.056 (7)	K3—Co2^ii	3.609 (5)
Co1—O2	2.073 (7)	K3—Mo1^ii	3.612 (5)
Co1—O6	2.075 (7)	K3—Mo3^ii	3.766 (6)
Co1—O8^i	2.153 (6)	O1—K2^x	2.808 (7)
Co1—O10^v	2.155 (7)	O1—K3^ii	3.074 (9)
Co1—O12	2.170 (6)	O3—K3^ii	2.840 (9)
Co1—K1^iv	3.6651 (13)	O3—K2^i	2.961 (8)
Co1—K2^iii	3.969 (3)	O4—Co1^iv	2.056 (7)
Co2—O3	2.033 (7)	O4—K2^i	2.815 (7)
Co2—O7^v	2.046 (7)	O5—K1^iii	2.921 (8)
Co2—O8^i	2.080 (6)	O5—K2^iii	2.946 (8)
Co2—O12	2.091 (6)	O6—K2^iii	3.026 (7)
Co2—O11^i	2.099 (6)	O7—Co2^v	2.046 (7)
Co2—O11^v	2.172 (7)	O7—K3^v	2.727 (8)
Co2—K3	3.558 (5)	O7—K3^xiii	2.814 (9)
Co2—K3^ii	3.609 (5)	O8—Co2^xi	2.080 (6)
K1—O4	2.725 (7)	O8—Co1^xi	2.153 (6)
K1—O4^ii	2.725 (7)	O9—K3^ii	3.074 (10)
K1—O10^vi	2.748 (7)	O9—K3^xi	3.264 (10)
K1—O10^vii	2.748 (7)	O10—Co1^v	2.155 (7)
K1—O5^iii	2.921 (8)	O10—K1^xiv	2.748 (7)
K1—O5^viii	2.921 (8)	O11—Co2^xi	2.099 (6)
K1—Co1^iv	3.6651 (13)	O11—Co2^v	2.172 (6)
K1—Co1^ix	3.6651 (13)
O1—Mo1—O2	109.3 (3)	O9—K2—O1^x	87.7 (2)
O1—Mo1—O4	110.6 (3)	O9—K2—O4^xi	133.9 (2)
O2—Mo1—O4	110.3 (3)	O1^x—K2—O4^xi	74.4 (2)
O1—Mo1—O3	107.1 (3)	O9—K2—O2	76.2 (2)
O2—Mo1—O3	110.5 (3)	O1^x—K2—O2	150.1 (2)
O4—Mo1—O3	109.0 (3)	O4^xi—K2—O2	134.4 (2)
O1—Mo1—K2^i	115.9 (2)	O9—K2—O5^iii	126.7 (2)
O2—Mo1—K2^i	134.9 (2)	O1^x—K2—O5^iii	98.1 (2)
O4—Mo1—K2^i	52.5 (2)	O4^xi—K2—O5^iii	98.2 (2)
O3—Mo1—K2^i	57.3 (2)	O2—K2—O5^iii	73.1 (2)
O1—Mo1—K2	56.3 (2)	O9—K2—O3^xi	73.7 (2)
O2—Mo1—K2	53.2 (2)	O1^x—K2—O3^xi	70.0 (2)
O4—Mo1—K2	122.5 (2)	O4^xi—K2—O3^xi	60.32 (19)
O3—Mo1—K2	128.5 (2)	O2—K2—O3^xi	126.8 (2)
K2^i—Mo1—K2	170.29 (10)	O5^iii—K2—O3^xi	157.1 (2)
O1—Mo1—K3^ii	58.2 (2)	O9—K2—O1	68.5 (2)
O2—Mo1—K3^ii	113.2 (2)	O1^x—K2—O1	92.6 (2)
O4—Mo1—K3^ii	136.2 (2)	O4^xi—K2—O1	151.8 (2)
O3—Mo1—K3^ii	50.7 (2)	O2—K2—O1	58.20 (19)
K2^i—Mo1—K3^ii	91.96 (11)	O5^iii—K2—O1	58.3 (2)
K2—Mo1—K3^ii	88.09 (11)	O3^xi—K2—O1	138.9 (2)
O1—Mo1—K1	67.3 (2)	O9—K2—O6^iii	153.3 (2)
O2—Mo1—K1	124.1 (2)	O1^x—K2—O6^iii	118.9 (2)
O4—Mo1—K1	43.3 (2)	O4^xi—K2—O6^iii	59.45 (19)
O3—Mo1—K1	124.1 (2)	O2—K2—O6^iii	80.43 (19)
K2^i—Mo1—K1	75.03 (5)	O5^iii—K2—O6^iii	56.0 (2)
K2—Mo1—K1	95.83 (5)	O3^xi—K2—O6^iii	111.7 (2)
K3^ii—Mo1—K1	110.02 (9)	O1—K2—O6^iii	109.3 (2)
O1—Mo1—K3	72.5 (2)	O9—K2—Mo1^xi	103.86 (19)
O2—Mo1—K3	129.8 (2)	O1^x—K2—Mo1^xi	66.06 (15)
O4—Mo1—K3	115.6 (2)	O4^xi—K2—Mo1^xi	30.05 (14)
O3—Mo1—K3	35.3 (2)	O2—K2—Mo1^xi	141.96 (18)
K2^i—Mo1—K3	68.17 (10)	O5^iii—K2—Mo1^xi	127.02 (17)
K2—Mo1—K3	111.72 (10)	O3^xi—K2—Mo1^xi	30.59 (13)
K3^ii—Mo1—K3	23.82 (19)	O1—K2—Mo1^xi	158.03 (16)
K1—Mo1—K3	103.33 (8)	O6^iii—K2—Mo1^xi	86.76 (14)
O5—Mo2—O6	107.9 (4)	O9—K2—Mo1	71.53 (18)
O5—Mo2—O7	106.6 (3)	O1^x—K2—Mo1	121.38 (17)
O6—Mo2—O7	111.9 (3)	O4^xi—K2—Mo1	153.23 (16)
O5—Mo2—O8	105.5 (3)	O2—K2—Mo1	29.47 (14)
O6—Mo2—O8	112.1 (3)	O5^iii—K2—Mo1	60.28 (15)
O7—Mo2—O8	112.3 (3)	O3^xi—K2—Mo1	142.56 (15)
O5—Mo2—K2^iii	53.6 (3)	O1—K2—Mo1	28.84 (13)
O6—Mo2—K2^iii	56.4 (2)	O6^iii—K2—Mo1	93.99 (14)
O7—Mo2—K2^iii	136.9 (2)	Mo1^xi—K2—Mo1	170.29 (10)
O8—Mo2—K2^iii	110.2 (2)	O9—K2—Mo2^iii	143.15 (19)
O5—Mo2—K1^iii	39.5 (3)	O1^x—K2—Mo2^iii	115.10 (16)
O6—Mo2—K1^iii	146.1 (2)	O4^xi—K2—Mo2^iii	81.92 (15)
O7—Mo2—K1^iii	91.6 (2)	O2—K2—Mo2^iii	69.98 (14)
O8—Mo2—K1^iii	78.3 (2)	O5^iii—K2—Mo2^iii	27.90 (14)
K2^iii—Mo2—K1^iii	89.70 (7)	O3^xi—K2—Mo2^iii	139.74 (15)
O9—Mo3—O10	105.9 (3)	O1—K2—Mo2^iii	81.27 (14)
O9—Mo3—O11	105.7 (4)	O6^iii—K2—Mo2^iii	28.87 (13)
O10—Mo3—O11	112.7 (3)	Mo1^xi—K2—Mo2^iii	111.68 (7)
O9—Mo3—O12	106.0 (3)	Mo1—K2—Mo2^iii	71.85 (5)
O10—Mo3—O12	113.5 (3)	O9—K2—Mo3	21.44 (15)
O11—Mo3—O12	112.2 (3)	O1^x—K2—Mo3	105.95 (16)
O9—Mo3—K3^ii	53.4 (3)	O4^xi—K2—Mo3	127.84 (16)
O10—Mo3—K3^ii	75.6 (2)	O2—K2—Mo3	65.35 (14)
O11—Mo3—K3^ii	158.9 (2)	O5^iii—K2—Mo3	132.02 (17)
O12—Mo3—K3^ii	79.5 (2)	O3^xi—K2—Mo3	70.81 (14)
O9—Mo3—K2	37.2 (3)	O1—K2—Mo3	79.42 (15)
O10—Mo3—K2	142.6 (2)	O6^iii—K2—Mo3	133.26 (16)
O11—Mo3—K2	82.0 (2)	Mo1^xi—K2—Mo3	100.75 (7)
O12—Mo3—K2	89.5 (2)	Mo1—K2—Mo3	71.75 (5)
K3^ii—Mo3—K2	80.61 (9)	Mo2^iii—K2—Mo3	135.09 (8)
O4^iv—Co1—O2	100.3 (3)	K3^ii—K3—O3	78.8 (3)
O4^iv—Co1—O6	89.3 (3)	K3^ii—K3—O7^v	76.4 (3)
O2—Co1—O6	90.4 (3)	O3—K3—O7^v	69.1 (2)
O4^iv—Co1—O8^i	94.1 (3)	K3^ii—K3—O7^xii	70.3 (3)
O2—Co1—O8^i	94.8 (3)	O3—K3—O7^xii	149.1 (3)
O6—Co1—O8^i	173.1 (3)	O7^v—K3—O7^xii	101.7 (3)
O4^iv—Co1—O10^v	95.2 (3)	K3^ii—K3—O3^ii	67.9 (3)
O2—Co1—O10^v	164.5 (3)	O3—K3—O3^ii	104.0 (3)
O6—Co1—O10^v	90.3 (3)	O7^v—K3—O3^ii	144.3 (3)
O8^i—Co1—O10^v	83.5 (3)	O7^xii—K3—O3^ii	65.7 (2)
O4^iv—Co1—O12	173.0 (3)	K3^ii—K3—O9^ii	151.7 (4)
O2—Co1—O12	83.6 (3)	O3—K3—O9^ii	116.4 (3)
O6—Co1—O12	96.5 (3)	O7^v—K3—O9^ii	130.4 (3)
O8^i—Co1—O12	79.7 (2)	O7^xii—K3—O9^ii	92.4 (2)
O10^v—Co1—O12	80.9 (3)	O3^ii—K3—O9^ii	84.7 (2)
O4^iv—Co1—K1^iv	47.22 (19)	K3^ii—K3—O1^ii	104.3 (2)
O2—Co1—K1^iv	147.1 (2)	O3—K3—O1^ii	69.9 (2)
O6—Co1—K1^iv	93.49 (19)	O7^v—K3—O1^ii	137.9 (3)
O8^i—Co1—K1^iv	84.51 (17)	O7^xii—K3—O1^ii	118.5 (3)
O10^v—Co1—K1^iv	48.23 (18)	O3^ii—K3—O1^ii	56.9 (2)
O12—Co1—K1^iv	128.18 (19)	O9^ii—K3—O1^ii	63.6 (2)
O4^iv—Co1—K2^iii	42.38 (19)	K3^ii—K3—O9^i	147.0 (4)
O2—Co1—K2^iii	88.22 (19)	O3—K3—O9^i	70.1 (2)
O6—Co1—K2^iii	48.6 (2)	O7^v—K3—O9^i	82.5 (2)
O8^i—Co1—K2^iii	135.89 (18)	O7^xii—K3—O9^i	139.7 (3)
O10^v—Co1—K2^iii	103.75 (18)	O3^ii—K3—O9^i	129.5 (3)
O12—Co1—K2^iii	144.13 (18)	O9^ii—K3—O9^i	58.2 (3)
K1^iv—Co1—K2^iii	70.55 (6)	O1^ii—K3—O9^i	75.2 (2)
O3—Co2—O7^v	97.5 (3)	K3^ii—K3—Co2	79.0 (3)
O3—Co2—O8^i	89.2 (3)	O3—K3—Co2	34.57 (15)
O7^v—Co2—O8^i	173.2 (3)	O7^v—K3—Co2	34.92 (15)
O3—Co2—O12	95.1 (3)	O7^xii—K3—Co2	132.8 (2)
O7^v—Co2—O12	97.5 (3)	O3^ii—K3—Co2	132.7 (2)
O8^i—Co2—O12	83.3 (2)	O9^ii—K3—Co2	127.5 (2)
O3—Co2—O11^i	101.4 (3)	O1^ii—K3—Co2	103.09 (19)
O7^v—Co2—O11^i	88.4 (3)	O9^i—K3—Co2	69.29 (17)
O8^i—Co2—O11^i	88.9 (2)	K3^ii—K3—Co2^ii	75.4 (4)
O12—Co2—O11^i	161.6 (3)	O3—K3—Co2^ii	137.1 (2)
O3—Co2—O11^v	175.1 (3)	O7^v—K3—Co2^ii	134.2 (2)
O7^v—Co2—O11^v	85.3 (3)	O7^xii—K3—Co2^ii	34.40 (15)
O8^i—Co2—O11^v	88.1 (3)	O3^ii—K3—Co2^ii	34.20 (15)
O12—Co2—O11^v	80.5 (2)	O9^ii—K3—Co2^ii	77.86 (17)
O11^i—Co2—O11^v	82.7 (3)	O1^ii—K3—Co2^ii	84.12 (17)
O3—Co2—K3	48.5 (2)	O9^i—K3—Co2^ii	136.1 (2)
O7^v—Co2—K3	49.7 (2)	Co2—K3—Co2^ii	154.4 (2)
O8^i—Co2—K3	136.6 (2)	K3^ii—K3—Mo1^ii	89.6 (2)
O12—Co2—K3	106.4 (2)	O3—K3—Mo1^ii	90.0 (2)
O11^i—Co2—K3	90.7 (2)	O7^v—K3—Mo1^ii	156.6 (2)
O11^v—Co2—K3	134.82 (19)	O7^xii—K3—Mo1^ii	90.86 (19)
O3—Co2—K3^ii	51.7 (2)	O3^ii—K3—Mo1^ii	29.23 (14)
O7^v—Co2—K3^ii	51.0 (2)	O9^ii—K3—Mo1^ii	67.73 (17)
O8^i—Co2—K3^ii	135.6 (2)	O1^ii—K3—Mo1^ii	28.35 (14)
O12—Co2—K3^ii	80.9 (2)	O9^i—K3—Mo1^ii	100.7 (2)
O11^i—Co2—K3^ii	115.8 (2)	Co2—K3—Mo1^ii	124.54 (15)
O11^v—Co2—K3^ii	129.00 (19)	Co2^ii—K3—Mo1^ii	56.53 (8)
K3—Co2—K3^ii	25.6 (2)	K3^ii—K3—Mo3^ii	132.8 (4)
O4—K1—O4^ii	110.5 (3)	O3—K3—Mo3^ii	142.3 (3)
O4—K1—O10^vi	175.58 (19)	O7^v—K3—Mo3^ii	130.1 (2)
O4^ii—K1—O10^vi	69.28 (19)	O7^xii—K3—Mo3^ii	66.55 (17)
O4—K1—O10^vii	69.28 (19)	O3^ii—K3—Mo3^ii	77.54 (18)
O4^ii—K1—O10^vii	175.58 (19)	O9^ii—K3—Mo3^ii	26.06 (14)
O10^vi—K1—O10^vii	111.3 (3)	O1^ii—K3—Mo3^ii	80.87 (18)
O4—K1—O5^iii	70.78 (19)	O9^i—K3—Mo3^ii	80.10 (19)
O4^ii—K1—O5^iii	99.1 (2)	Co2—K3—Mo3^ii	146.61 (19)
O10^vi—K1—O5^iii	104.8 (2)	Co2^ii—K3—Mo3^ii	58.31 (8)
O10^vii—K1—O5^iii	85.1 (2)	Mo1^ii—K3—Mo3^ii	73.08 (10)
O4—K1—O5^viii	99.1 (2)	Mo1—O1—K2^x	174.5 (4)
O4^ii—K1—O5^viii	70.78 (19)	Mo1—O1—K2	94.8 (3)
O10^vi—K1—O5^viii	85.1 (2)	K2^x—O1—K2	86.8 (2)
O10^vii—K1—O5^viii	104.8 (2)	Mo1—O1—K3^ii	93.5 (3)
O5^iii—K1—O5^viii	162.7 (3)	K2^x—O1—K3^ii	90.8 (2)
O4—K1—Co1^iv	33.63 (14)	K2—O1—K3^ii	111.1 (3)
O4^ii—K1—Co1^iv	144.16 (19)	Mo1—O2—Co1	128.4 (4)
O10^vi—K1—Co1^iv	146.40 (19)	Mo1—O2—K2	97.3 (3)
O10^vii—K1—Co1^iv	35.80 (14)	Co1—O2—K2	121.7 (3)
O5^iii—K1—Co1^iv	72.80 (14)	Mo1—O3—Co2	126.6 (4)
O5^viii—K1—Co1^iv	106.85 (14)	Mo1—O3—K3	122.0 (3)
O4—K1—Co1^ix	144.16 (19)	Co2—O3—K3	97.0 (3)
O4^ii—K1—Co1^ix	33.63 (14)	Mo1—O3—K3^ii	100.0 (3)
O10^vi—K1—Co1^ix	35.80 (14)	Co2—O3—K3^ii	94.1 (3)
O10^vii—K1—Co1^ix	146.40 (19)	K3—O3—K3^ii	33.3 (3)
O5^iii—K1—Co1^ix	106.85 (14)	Mo1—O3—K2^i	92.1 (3)
O5^viii—K1—Co1^ix	72.80 (14)	Co2—O3—K2^i	120.9 (3)
Co1^iv—K1—Co1^ix	177.78 (12)	K3—O3—K2^i	95.8 (2)
O4—K1—Mo1	26.58 (14)	K3^ii—O3—K2^i	124.2 (3)
O4^ii—K1—Mo1	88.66 (17)	Mo1—O4—Co1^iv	134.0 (3)
O10^vi—K1—Mo1	150.41 (15)	Mo1—O4—K1	110.1 (3)
O10^vii—K1—Mo1	92.26 (14)	Co1^iv—O4—K1	99.2 (3)
O5^iii—K1—Mo1	58.06 (15)	Mo1—O4—K2^i	97.4 (3)
O5^viii—K1—Mo1	106.65 (16)	Co1^iv—O4—K2^i	108.1 (3)
Co1^iv—K1—Mo1	57.01 (4)	K1—O4—K2^i	105.7 (2)
Co1^ix—K1—Mo1	120.88 (9)	Mo2—O5—K1^iii	118.6 (4)
O4—K1—Mo1^ii	88.66 (17)	Mo2—O5—K2^iii	98.5 (3)
O4^ii—K1—Mo1^ii	26.58 (14)	K1^iii—O5—K2^iii	134.1 (3)
O10^vi—K1—Mo1^ii	92.26 (14)	Mo2—O6—Co1	144.8 (4)
O10^vii—K1—Mo1^ii	150.41 (15)	Mo2—O6—K2^iii	94.7 (3)
O5^iii—K1—Mo1^ii	106.65 (16)	Co1—O6—K2^iii	100.5 (3)
O5^viii—K1—Mo1^ii	58.06 (15)	Mo2—O7—Co2^v	120.0 (3)
Co1^iv—K1—Mo1^ii	120.88 (9)	Mo2—O7—K3^v	138.4 (3)
Co1^ix—K1—Mo1^ii	57.01 (4)	Co2^v—O7—K3^v	95.3 (3)
Mo1—K1—Mo1^ii	72.73 (7)	Mo2—O7—K3^xiii	144.0 (4)
O4—K1—Mo2^iii	67.74 (13)	Co2^v—O7—K3^xiii	94.6 (3)
O4^ii—K1—Mo2^iii	120.81 (14)	K3^v—O7—K3^xiii	33.3 (3)
O10^vi—K1—Mo2^iii	108.39 (15)	Mo2—O8—Co2^xi	115.0 (3)
O10^vii—K1—Mo2^iii	63.42 (14)	Mo2—O8—Co1^xi	139.4 (3)
O5^iii—K1—Mo2^iii	21.91 (14)	Co2^xi—O8—Co1^xi	98.4 (3)
O5^viii—K1—Mo2^iii	164.37 (14)	Mo3—O9—K2	121.4 (4)
Co1^iv—K1—Mo2^iii	57.53 (2)	Mo3—O9—K3^ii	100.6 (4)
Co1^ix—K1—Mo2^iii	122.77 (3)	K2—O9—K3^ii	116.4 (3)
Mo1—K1—Mo2^iii	65.52 (3)	Mo3—O9—K3^xi	113.5 (4)
Mo1^ii—K1—Mo2^iii	127.07 (8)	K2—O9—K3^xi	87.4 (2)
O4—K1—Mo2^viii	120.81 (14)	K3^ii—O9—K3^xi	118.7 (3)
O4^ii—K1—Mo2^viii	67.74 (13)	Mo3—O10—Co1^v	116.2 (3)
O10^vi—K1—Mo2^viii	63.42 (14)	Mo3—O10—K1^xiv	141.9 (3)
O10^vii—K1—Mo2^viii	108.39 (15)	Co1^v—O10—K1^xiv	96.0 (2)
O5^iii—K1—Mo2^viii	164.37 (14)	Mo3—O11—Co2^xi	138.9 (4)
O5^viii—K1—Mo2^viii	21.91 (14)	Mo3—O11—Co2^v	114.6 (3)
Co1^iv—K1—Mo2^viii	122.77 (3)	Co2^xi—O11—Co2^v	97.3 (3)
Co1^ix—K1—Mo2^viii	57.53 (2)	Mo3—O12—Co2	133.1 (3)
Mo1—K1—Mo2^viii	127.07 (8)	Mo3—O12—Co1	127.2 (3)
Mo1^ii—K1—Mo2^viii	65.52 (3)	Co2—O12—Co1	97.5 (3)
Mo2^iii—K1—Mo2^viii	166.56 (11)
O1—Mo1—K1—O4	177.6 (4)	O3—Mo1—O2—Co1	−17.7 (6)
O2—Mo1—K1—O4	−83.9 (4)	K2^i—Mo1—O2—Co1	46.1 (6)
O3—Mo1—K1—O4	81.7 (4)	K2—Mo1—O2—Co1	−141.1 (6)
K2^i—Mo1—K1—O4	50.6 (3)	K3^ii—Mo1—O2—Co1	−72.6 (5)
K2—Mo1—K1—O4	−132.7 (3)	K1—Mo1—O2—Co1	149.6 (3)
K3^ii—Mo1—K1—O4	137.2 (3)	K3—Mo1—O2—Co1	−52.3 (6)
K3—Mo1—K1—O4	113.3 (3)	O1—Mo1—O2—K2	5.8 (3)
O1—Mo1—K1—O4^ii	31.4 (3)	O4—Mo1—O2—K2	−116.0 (3)
O2—Mo1—K1—O4^ii	130.0 (3)	O3—Mo1—O2—K2	123.4 (3)
O4—Mo1—K1—O4^ii	−146.2 (2)	K2^i—Mo1—O2—K2	−172.83 (13)
O3—Mo1—K1—O4^ii	−64.4 (3)	K3^ii—Mo1—O2—K2	68.5 (2)
K2^i—Mo1—K1—O4^ii	−95.54 (15)	K1—Mo1—O2—K2	−69.3 (3)
K2—Mo1—K1—O4^ii	81.13 (14)	K3—Mo1—O2—K2	88.7 (3)
K3^ii—Mo1—K1—O4^ii	−8.96 (17)	O4^iv—Co1—O2—Mo1	−114.3 (5)
K3—Mo1—K1—O4^ii	−32.85 (17)	O6—Co1—O2—Mo1	156.4 (5)
O1—Mo1—K1—O10^vi	−9.3 (4)	O8^i—Co1—O2—Mo1	−19.2 (5)
O2—Mo1—K1—O10^vi	89.2 (4)	O10^v—Co1—O2—Mo1	63.8 (12)
O4—Mo1—K1—O10^vi	173.1 (4)	O12—Co1—O2—Mo1	59.9 (5)
O3—Mo1—K1—O10^vi	−105.2 (4)	K1^iv—Co1—O2—Mo1	−106.5 (4)
K2^i—Mo1—K1—O10^vi	−136.3 (3)	K2^iii—Co1—O2—Mo1	−155.1 (4)
K2—Mo1—K1—O10^vi	40.4 (3)	O4^iv—Co1—O2—K2	112.8 (3)
K3^ii—Mo1—K1—O10^vi	−49.7 (3)	O6—Co1—O2—K2	23.5 (3)
K3—Mo1—K1—O10^vi	−73.6 (3)	O8^i—Co1—O2—K2	−152.1 (3)
O1—Mo1—K1—O10^vii	−152.9 (3)	O10^v—Co1—O2—K2	−69.1 (11)
O2—Mo1—K1—O10^vii	−54.4 (3)	O12—Co1—O2—K2	−73.0 (3)
O4—Mo1—K1—O10^vii	29.5 (3)	K1^iv—Co1—O2—K2	120.6 (3)
O3—Mo1—K1—O10^vii	111.2 (3)	K2^iii—Co1—O2—K2	72.0 (3)
K2^i—Mo1—K1—O10^vii	80.14 (15)	O9—K2—O2—Mo1	−76.8 (3)
K2—Mo1—K1—O10^vii	−103.19 (15)	O1^x—K2—O2—Mo1	−17.5 (6)
K3^ii—Mo1—K1—O10^vii	166.71 (18)	O4^xi—K2—O2—Mo1	143.9 (3)
K3—Mo1—K1—O10^vii	142.82 (17)	O5^iii—K2—O2—Mo1	59.1 (3)
O1—Mo1—K1—O5^iii	−70.1 (3)	O3^xi—K2—O2—Mo1	−133.8 (3)
O2—Mo1—K1—O5^iii	28.4 (3)	O1—K2—O2—Mo1	−3.7 (2)
O4—Mo1—K1—O5^iii	112.3 (3)	O6^iii—K2—O2—Mo1	116.2 (3)
O3—Mo1—K1—O5^iii	−166.0 (3)	Mo1^xi—K2—O2—Mo1	−171.74 (16)
K2^i—Mo1—K1—O5^iii	162.91 (17)	Mo2^iii—K2—O2—Mo1	88.3 (2)
K2—Mo1—K1—O5^iii	−20.42 (17)	Mo3—K2—O2—Mo1	−96.4 (2)
K3^ii—Mo1—K1—O5^iii	−110.5 (2)	O9—K2—O2—Co1	67.9 (3)
K3—Mo1—K1—O5^iii	−134.41 (19)	O1^x—K2—O2—Co1	127.2 (4)
O1—Mo1—K1—O5^viii	100.9 (3)	O4^xi—K2—O2—Co1	−71.5 (4)
O2—Mo1—K1—O5^viii	−160.6 (3)	O5^iii—K2—O2—Co1	−156.3 (4)
O4—Mo1—K1—O5^viii	−76.7 (3)	O3^xi—K2—O2—Co1	10.8 (4)
O3—Mo1—K1—O5^viii	5.0 (3)	O1—K2—O2—Co1	140.9 (4)
K2^i—Mo1—K1—O5^viii	−26.06 (16)	O6^iii—K2—O2—Co1	−99.1 (3)
K2—Mo1—K1—O5^viii	150.61 (16)	Mo1^xi—K2—O2—Co1	−27.1 (5)
K3^ii—Mo1—K1—O5^viii	60.52 (18)	Mo1—K2—O2—Co1	144.6 (5)
K3—Mo1—K1—O5^viii	36.62 (18)	Mo2^iii—K2—O2—Co1	−127.0 (3)
O1—Mo1—K1—Co1^iv	−159.5 (3)	Mo3—K2—O2—Co1	48.2 (3)
O2—Mo1—K1—Co1^iv	−61.0 (3)	O1—Mo1—O3—Co2	118.0 (5)
O4—Mo1—K1—Co1^iv	22.9 (3)	O2—Mo1—O3—Co2	−1.0 (5)
O3—Mo1—K1—Co1^iv	104.6 (3)	O4—Mo1—O3—Co2	−122.4 (4)
K2^i—Mo1—K1—Co1^iv	73.53 (5)	K2^i—Mo1—O3—Co2	−131.9 (5)
K2—Mo1—K1—Co1^iv	−109.80 (6)	K2—Mo1—O3—Co2	57.7 (5)
K3^ii—Mo1—K1—Co1^iv	160.10 (11)	K3^ii—Mo1—O3—Co2	102.8 (5)
K3—Mo1—K1—Co1^iv	136.21 (10)	K1—Mo1—O3—Co2	−168.3 (3)
O1—Mo1—K1—Co1^ix	21.3 (3)	K3—Mo1—O3—Co2	129.9 (7)
O2—Mo1—K1—Co1^ix	119.8 (3)	O1—Mo1—O3—K3	−12.0 (5)
O4—Mo1—K1—Co1^ix	−156.3 (3)	O2—Mo1—O3—K3	−130.9 (4)
O3—Mo1—K1—Co1^ix	−74.5 (3)	O4—Mo1—O3—K3	107.7 (4)
K2^i—Mo1—K1—Co1^ix	−105.65 (7)	K2^i—Mo1—O3—K3	98.2 (4)
K2—Mo1—K1—Co1^ix	71.02 (7)	K2—Mo1—O3—K3	−72.2 (4)
K3^ii—Mo1—K1—Co1^ix	−19.07 (12)	K3^ii—Mo1—O3—K3	−27.1 (3)
K3—Mo1—K1—Co1^ix	−42.97 (10)	K1—Mo1—O3—K3	61.8 (4)
O1—Mo1—K1—Mo1^ii	53.1 (3)	O1—Mo1—O3—K3^ii	15.2 (4)
O2—Mo1—K1—Mo1^ii	151.6 (3)	O2—Mo1—O3—K3^ii	−103.8 (3)
O4—Mo1—K1—Mo1^ii	−124.5 (3)	O4—Mo1—O3—K3^ii	134.8 (3)
O3—Mo1—K1—Mo1^ii	−42.8 (3)	K2^i—Mo1—O3—K3^ii	125.3 (3)
K2^i—Mo1—K1—Mo1^ii	−73.90 (5)	K2—Mo1—O3—K3^ii	−45.1 (3)
K2—Mo1—K1—Mo1^ii	102.77 (5)	K1—Mo1—O3—K3^ii	88.9 (3)
K3^ii—Mo1—K1—Mo1^ii	12.68 (11)	K3—Mo1—O3—K3^ii	27.1 (3)
K3—Mo1—K1—Mo1^ii	−11.21 (9)	O1—Mo1—O3—K2^i	−110.1 (3)
O1—Mo1—K1—Mo2^iii	−93.5 (3)	O2—Mo1—O3—K2^i	130.9 (3)
O2—Mo1—K1—Mo2^iii	5.0 (3)	O4—Mo1—O3—K2^i	9.5 (3)
O4—Mo1—K1—Mo2^iii	88.8 (3)	K2—Mo1—O3—K2^i	−170.41 (13)
O3—Mo1—K1—Mo2^iii	170.6 (3)	K3^ii—Mo1—O3—K2^i	−125.3 (3)
K2^i—Mo1—K1—Mo2^iii	139.47 (5)	K1—Mo1—O3—K2^i	−36.4 (3)
K2—Mo1—K1—Mo2^iii	−43.86 (5)	K3—Mo1—O3—K2^i	−98.2 (4)
K3^ii—Mo1—K1—Mo2^iii	−133.95 (11)	O7^v—Co2—O3—Mo1	−129.9 (4)
K3—Mo1—K1—Mo2^iii	−157.85 (10)	O8^i—Co2—O3—Mo1	51.6 (5)
O1—Mo1—K1—Mo2^viii	91.9 (3)	O12—Co2—O3—Mo1	−31.6 (5)
O2—Mo1—K1—Mo2^viii	−169.6 (3)	O11^i—Co2—O3—Mo1	140.3 (4)
O4—Mo1—K1—Mo2^viii	−85.7 (3)	O11^v—Co2—O3—Mo1	−5 (3)
O3—Mo1—K1—Mo2^viii	−3.9 (3)	K3—Co2—O3—Mo1	−139.1 (6)
K2^i—Mo1—K1—Mo2^viii	−35.04 (6)	K3^ii—Co2—O3—Mo1	−105.7 (5)
K2—Mo1—K1—Mo2^viii	141.63 (6)	O7^v—Co2—O3—K3	9.2 (3)
K3^ii—Mo1—K1—Mo2^viii	51.53 (12)	O8^i—Co2—O3—K3	−169.4 (3)
K3—Mo1—K1—Mo2^viii	27.64 (11)	O12—Co2—O3—K3	107.5 (3)
O1—Mo1—K2—O9	−78.8 (3)	O11^i—Co2—O3—K3	−80.7 (3)
O2—Mo1—K2—O9	94.6 (3)	O11^v—Co2—O3—K3	134 (3)
O4—Mo1—K2—O9	−173.2 (3)	K3^ii—Co2—O3—K3	33.3 (3)
O3—Mo1—K2—O9	6.7 (3)	O7^v—Co2—O3—K3^ii	−24.2 (3)
K2^i—Mo1—K2—O9	−117.1 (5)	O8^i—Co2—O3—K3^ii	157.3 (3)
K3^ii—Mo1—K2—O9	−26.57 (18)	O12—Co2—O3—K3^ii	74.1 (3)
K1—Mo1—K2—O9	−136.50 (17)	O11^i—Co2—O3—K3^ii	−114.0 (3)
K3—Mo1—K2—O9	−29.64 (19)	O11^v—Co2—O3—K3^ii	100 (3)
O1—Mo1—K2—O1^x	−3.51 (14)	K3—Co2—O3—K3^ii	−33.3 (3)
O2—Mo1—K2—O1^x	169.9 (3)	O7^v—Co2—O3—K2^i	110.2 (3)
O4—Mo1—K2—O1^x	−97.9 (3)	O8^i—Co2—O3—K2^i	−68.4 (3)
O3—Mo1—K2—O1^x	82.0 (3)	O12—Co2—O3—K2^i	−151.5 (3)
K2^i—Mo1—K2—O1^x	−41.7 (6)	O11^i—Co2—O3—K2^i	20.4 (4)
K3^ii—Mo1—K2—O1^x	48.7 (2)	O11^v—Co2—O3—K2^i	−125 (3)
K1—Mo1—K2—O1^x	−61.18 (19)	K3—Co2—O3—K2^i	101.0 (4)
K3—Mo1—K2—O1^x	45.7 (2)	K3^ii—Co2—O3—K2^i	134.4 (4)
O1—Mo1—K2—O4^xi	117.3 (5)	K3^ii—K3—O3—Mo1	54.8 (4)
O2—Mo1—K2—O4^xi	−69.3 (4)	O7^v—K3—O3—Mo1	134.4 (4)
O4—Mo1—K2—O4^xi	22.9 (3)	O7^xii—K3—O3—Mo1	57.0 (7)
O3—Mo1—K2—O4^xi	−157.2 (4)	O3^ii—K3—O3—Mo1	−8.8 (4)
K2^i—Mo1—K2—O4^xi	79.0 (7)	O9^ii—K3—O3—Mo1	−99.8 (4)
K3^ii—Mo1—K2—O4^xi	169.5 (4)	O1^ii—K3—O3—Mo1	−55.1 (4)
K1—Mo1—K2—O4^xi	59.6 (4)	O9^i—K3—O3—Mo1	−136.2 (4)
K3—Mo1—K2—O4^xi	166.5 (4)	Co2—K3—O3—Mo1	141.7 (6)
O1—Mo1—K2—O2	−173.4 (4)	Co2^ii—K3—O3—Mo1	1.2 (6)
O4—Mo1—K2—O2	92.2 (4)	Mo1^ii—K3—O3—Mo1	−34.8 (4)
O3—Mo1—K2—O2	−87.9 (4)	Mo3^ii—K3—O3—Mo1	−96.4 (5)
K2^i—Mo1—K2—O2	148.4 (6)	K3^ii—K3—O3—Co2	−86.9 (3)
K3^ii—Mo1—K2—O2	−121.2 (3)	O7^v—K3—O3—Co2	−7.3 (2)
K1—Mo1—K2—O2	128.9 (3)	O7^xii—K3—O3—Co2	−84.7 (6)
K3—Mo1—K2—O2	−124.2 (3)	O3^ii—K3—O3—Co2	−150.5 (3)
O1—Mo1—K2—O5^iii	77.4 (3)	O9^ii—K3—O3—Co2	118.5 (3)
O2—Mo1—K2—O5^iii	−109.1 (3)	O1^ii—K3—O3—Co2	163.2 (3)
O4—Mo1—K2—O5^iii	−17.0 (3)	O9^i—K3—O3—Co2	82.1 (3)
O3—Mo1—K2—O5^iii	163.0 (3)	Co2^ii—K3—O3—Co2	−140.5 (3)
K2^i—Mo1—K2—O5^iii	39.2 (6)	Mo1^ii—K3—O3—Co2	−176.5 (2)
K3^ii—Mo1—K2—O5^iii	129.69 (18)	Mo3^ii—K3—O3—Co2	121.9 (4)
K1—Mo1—K2—O5^iii	19.76 (17)	O7^v—K3—O3—K3^ii	79.6 (3)
K3—Mo1—K2—O5^iii	126.62 (18)	O7^xii—K3—O3—K3^ii	2.1 (5)
O1—Mo1—K2—O3^xi	−101.4 (4)	O3^ii—K3—O3—K3^ii	−63.6 (3)
O2—Mo1—K2—O3^xi	72.0 (4)	O9^ii—K3—O3—K3^ii	−154.6 (4)
O4—Mo1—K2—O3^xi	164.2 (3)	O1^ii—K3—O3—K3^ii	−109.9 (3)
O3—Mo1—K2—O3^xi	−15.9 (2)	O9^i—K3—O3—K3^ii	169.0 (3)
K2^i—Mo1—K2—O3^xi	−139.7 (5)	Co2—K3—O3—K3^ii	86.9 (3)
K3^ii—Mo1—K2—O3^xi	−49.2 (3)	Co2^ii—K3—O3—K3^ii	−53.7 (4)
K1—Mo1—K2—O3^xi	−159.1 (3)	Mo1^ii—K3—O3—K3^ii	−89.6 (2)
K3—Mo1—K2—O3^xi	−52.3 (3)	Mo3^ii—K3—O3—K3^ii	−151.2 (4)
O2—Mo1—K2—O1	173.4 (4)	K3^ii—K3—O3—K2^i	151.0 (3)
O4—Mo1—K2—O1	−94.4 (4)	O7^v—K3—O3—K2^i	−129.4 (3)
O3—Mo1—K2—O1	85.5 (4)	O7^xii—K3—O3—K2^i	153.2 (5)
K2^i—Mo1—K2—O1	−38.2 (6)	O3^ii—K3—O3—K2^i	87.4 (2)
K3^ii—Mo1—K2—O1	52.3 (3)	O9^ii—K3—O3—K2^i	−3.6 (3)
K1—Mo1—K2—O1	−57.7 (3)	O1^ii—K3—O3—K2^i	41.1 (2)
K3—Mo1—K2—O1	49.2 (3)	O9^i—K3—O3—K2^i	−40.0 (2)
O1—Mo1—K2—O6^iii	124.1 (3)	Co2—K3—O3—K2^i	−122.1 (3)
O2—Mo1—K2—O6^iii	−62.5 (3)	Co2^ii—K3—O3—K2^i	97.3 (3)
O4—Mo1—K2—O6^iii	29.7 (3)	Mo1^ii—K3—O3—K2^i	61.39 (18)
O3—Mo1—K2—O6^iii	−150.3 (3)	Mo3^ii—K3—O3—K2^i	−0.2 (4)
K2^i—Mo1—K2—O6^iii	85.9 (6)	O1—Mo1—O4—Co1^iv	−128.4 (5)
K3^ii—Mo1—K2—O6^iii	176.37 (16)	O2—Mo1—O4—Co1^iv	−7.4 (6)
K1—Mo1—K2—O6^iii	66.44 (15)	O3—Mo1—O4—Co1^iv	114.1 (5)
K3—Mo1—K2—O6^iii	173.30 (16)	K2^i—Mo1—O4—Co1^iv	124.2 (6)
O1—Mo1—K2—Mo1^xi	−141.8 (6)	K2—Mo1—O4—Co1^iv	−66.0 (5)
O2—Mo1—K2—Mo1^xi	31.6 (6)	K3^ii—Mo1—O4—Co1^iv	166.6 (3)
O4—Mo1—K2—Mo1^xi	123.8 (6)	K1—Mo1—O4—Co1^iv	−126.0 (6)
O3—Mo1—K2—Mo1^xi	−56.2 (6)	K3—Mo1—O4—Co1^iv	151.7 (4)
K2^i—Mo1—K2—Mo1^xi	180.000 (3)	O1—Mo1—O4—K1	−2.4 (4)
K3^ii—Mo1—K2—Mo1^xi	−89.5 (5)	O2—Mo1—O4—K1	118.6 (3)
K1—Mo1—K2—Mo1^xi	160.6 (5)	O3—Mo1—O4—K1	−119.9 (3)
K3—Mo1—K2—Mo1^xi	−92.6 (5)	K2^i—Mo1—O4—K1	−109.8 (3)
O1—Mo1—K2—Mo2^iii	105.3 (3)	K2—Mo1—O4—K1	60.1 (3)
O2—Mo1—K2—Mo2^iii	−81.3 (3)	K3^ii—Mo1—O4—K1	−67.3 (4)
O4—Mo1—K2—Mo2^iii	10.9 (2)	K3—Mo1—O4—K1	−82.2 (3)
O3—Mo1—K2—Mo2^iii	−169.1 (3)	O1—Mo1—O4—K2^i	107.4 (3)
K2^i—Mo1—K2—Mo2^iii	67.1 (5)	O2—Mo1—O4—K2^i	−131.6 (3)
K3^ii—Mo1—K2—Mo2^iii	157.59 (9)	O3—Mo1—O4—K2^i	−10.1 (3)
K1—Mo1—K2—Mo2^iii	47.66 (5)	K2—Mo1—O4—K2^i	169.83 (13)
K3—Mo1—K2—Mo2^iii	154.52 (8)	K3^ii—Mo1—O4—K2^i	42.4 (4)
O1—Mo1—K2—Mo3	−101.4 (3)	K1—Mo1—O4—K2^i	109.8 (3)
O2—Mo1—K2—Mo3	72.0 (3)	K3—Mo1—O4—K2^i	27.5 (3)
O4—Mo1—K2—Mo3	164.2 (2)	O4^ii—K1—O4—Mo1	36.5 (2)
O3—Mo1—K2—Mo3	−15.9 (3)	O10^vi—K1—O4—Mo1	−50 (3)
K2^i—Mo1—K2—Mo3	−139.7 (5)	O10^vii—K1—O4—Mo1	−148.3 (3)
K3^ii—Mo1—K2—Mo3	−49.17 (9)	O5^iii—K1—O4—Mo1	−56.3 (3)
K1—Mo1—K2—Mo3	−159.10 (5)	O5^viii—K1—O4—Mo1	109.2 (3)
K3—Mo1—K2—Mo3	−52.24 (9)	Co1^iv—K1—O4—Mo1	−143.9 (4)
O10—Mo3—K2—O9	12.4 (6)	Co1^ix—K1—O4—Mo1	36.1 (4)
O11—Mo3—K2—O9	129.6 (5)	Mo1^ii—K1—O4—Mo1	51.9 (3)
O12—Mo3—K2—O9	−117.9 (5)	Mo2^iii—K1—O4—Mo1	−79.5 (3)
K3^ii—Mo3—K2—O9	−38.5 (5)	Mo2^viii—K1—O4—Mo1	112.1 (3)
O9—Mo3—K2—O1^x	−32.6 (5)	O4^ii—K1—O4—Co1^iv	−179.6 (3)
O10—Mo3—K2—O1^x	−20.2 (4)	O10^vi—K1—O4—Co1^iv	94 (3)
O11—Mo3—K2—O1^x	97.0 (3)	O10^vii—K1—O4—Co1^iv	−4.4 (2)
O12—Mo3—K2—O1^x	−150.5 (3)	O5^iii—K1—O4—Co1^iv	87.6 (3)
K3^ii—Mo3—K2—O1^x	−71.10 (19)	O5^viii—K1—O4—Co1^iv	−106.9 (3)
O9—Mo3—K2—O4^xi	−115.1 (5)	Co1^ix—K1—O4—Co1^iv	−179.980 (17)
O10—Mo3—K2—O4^xi	−102.7 (4)	Mo1—K1—O4—Co1^iv	143.9 (4)
O11—Mo3—K2—O4^xi	14.5 (3)	Mo1^ii—K1—O4—Co1^iv	−164.2 (2)
O12—Mo3—K2—O4^xi	127.1 (3)	Mo2^iii—K1—O4—Co1^iv	64.41 (19)
K3^ii—Mo3—K2—O4^xi	−153.6 (2)	Mo2^viii—K1—O4—Co1^iv	−104.0 (2)
O9—Mo3—K2—O2	116.8 (5)	O4^ii—K1—O4—K2^i	−67.75 (17)
O10—Mo3—K2—O2	129.2 (4)	O10^vi—K1—O4—K2^i	−154 (3)
O11—Mo3—K2—O2	−113.6 (3)	O10^vii—K1—O4—K2^i	107.5 (3)
O12—Mo3—K2—O2	−1.1 (2)	O5^iii—K1—O4—K2^i	−160.5 (3)
K3^ii—Mo3—K2—O2	78.31 (18)	O5^viii—K1—O4—K2^i	5.0 (3)
O9—Mo3—K2—O5^iii	84.5 (5)	Co1^iv—K1—O4—K2^i	111.9 (3)
O10—Mo3—K2—O5^iii	96.9 (4)	Co1^ix—K1—O4—K2^i	−68.1 (3)
O11—Mo3—K2—O5^iii	−145.9 (3)	Mo1—K1—O4—K2^i	−104.2 (4)
O12—Mo3—K2—O5^iii	−33.4 (3)	Mo1^ii—K1—O4—K2^i	−52.32 (19)
K3^ii—Mo3—K2—O5^iii	46.0 (2)	Mo2^iii—K1—O4—K2^i	176.3 (2)
O9—Mo3—K2—O3^xi	−94.2 (5)	Mo2^viii—K1—O4—K2^i	7.9 (3)
O10—Mo3—K2—O3^xi	−81.8 (4)	O6—Mo2—O5—K1^iii	−168.1 (3)
O11—Mo3—K2—O3^xi	35.4 (2)	O7—Mo2—O5—K1^iii	71.5 (4)
O12—Mo3—K2—O3^xi	147.9 (2)	O8—Mo2—O5—K1^iii	−48.1 (4)
K3^ii—Mo3—K2—O3^xi	−132.68 (17)	K2^iii—Mo2—O5—K1^iii	−151.9 (5)
O9—Mo3—K2—O1	57.1 (5)	O6—Mo2—O5—K2^iii	−16.2 (4)
O10—Mo3—K2—O1	69.5 (4)	O7—Mo2—O5—K2^iii	−136.5 (3)
O11—Mo3—K2—O1	−173.4 (2)	O8—Mo2—O5—K2^iii	103.9 (3)
O12—Mo3—K2—O1	−60.8 (2)	K1^iii—Mo2—O5—K2^iii	151.9 (5)
K3^ii—Mo3—K2—O1	18.59 (17)	O5—Mo2—O6—Co1	−100.1 (7)
O9—Mo3—K2—O6^iii	163.7 (5)	O7—Mo2—O6—Co1	16.9 (8)
O10—Mo3—K2—O6^iii	176.1 (4)	O8—Mo2—O6—Co1	144.1 (6)
O11—Mo3—K2—O6^iii	−66.7 (3)	K2^iii—Mo2—O6—Co1	−115.7 (7)
O12—Mo3—K2—O6^iii	45.8 (3)	K1^iii—Mo2—O6—Co1	−113.7 (6)
K3^ii—Mo3—K2—O6^iii	125.2 (2)	O5—Mo2—O6—K2^iii	15.6 (3)
O9—Mo3—K2—Mo1^xi	−100.6 (5)	O7—Mo2—O6—K2^iii	132.6 (3)
O10—Mo3—K2—Mo1^xi	−88.2 (4)	O8—Mo2—O6—K2^iii	−100.2 (3)
O11—Mo3—K2—Mo1^xi	29.0 (2)	K1^iii—Mo2—O6—K2^iii	2.1 (5)
O12—Mo3—K2—Mo1^xi	141.6 (2)	O4^iv—Co1—O6—Mo2	101.0 (7)
K3^ii—Mo3—K2—Mo1^xi	−139.05 (11)	O2—Co1—O6—Mo2	−158.7 (7)
O9—Mo3—K2—Mo1	85.8 (5)	O8^i—Co1—O6—Mo2	−19 (3)
O10—Mo3—K2—Mo1	98.2 (4)	O10^v—Co1—O6—Mo2	5.8 (7)
O11—Mo3—K2—Mo1	−144.6 (2)	O12—Co1—O6—Mo2	−75.1 (7)
O12—Mo3—K2—Mo1	−32.06 (19)	K1^iv—Co1—O6—Mo2	54.0 (7)
K3^ii—Mo3—K2—Mo1	47.33 (10)	K2^iii—Co1—O6—Mo2	114.0 (7)
O9—Mo3—K2—Mo2^iii	123.1 (5)	O4^iv—Co1—O6—K2^iii	−13.0 (3)
O10—Mo3—K2—Mo2^iii	135.5 (4)	O2—Co1—O6—K2^iii	87.3 (3)
O11—Mo3—K2—Mo2^iii	−107.3 (2)	O8^i—Co1—O6—K2^iii	−133 (2)
O12—Mo3—K2—Mo2^iii	5.2 (2)	O10^v—Co1—O6—K2^iii	−108.2 (2)
K3^ii—Mo3—K2—Mo2^iii	84.63 (14)	O12—Co1—O6—K2^iii	170.8 (2)
O3—Co2—K3—K3^ii	86.1 (3)	K1^iv—Co1—O6—K2^iii	−60.08 (19)
O7^v—Co2—K3—K3^ii	−81.9 (3)	O5—Mo2—O7—Co2^v	−162.7 (4)
O8^i—Co2—K3—K3^ii	101.7 (3)	O6—Mo2—O7—Co2^v	79.5 (4)
O12—Co2—K3—K3^ii	3.99 (19)	O8—Mo2—O7—Co2^v	−47.6 (5)
O11^i—Co2—K3—K3^ii	−169.17 (18)	K2^iii—Mo2—O7—Co2^v	143.2 (2)
O11^v—Co2—K3—K3^ii	−88.8 (3)	K1^iii—Mo2—O7—Co2^v	−125.5 (3)
O7^v—Co2—K3—O3	−168.0 (4)	O5—Mo2—O7—K3^v	−18.5 (6)
O8^i—Co2—K3—O3	15.5 (4)	O6—Mo2—O7—K3^v	−136.3 (5)
O12—Co2—K3—O3	−82.1 (3)	O8—Mo2—O7—K3^v	96.6 (5)
O11^i—Co2—K3—O3	104.7 (3)	K2^iii—Mo2—O7—K3^v	−72.5 (6)
O11^v—Co2—K3—O3	−175.0 (4)	K1^iii—Mo2—O7—K3^v	18.7 (5)
K3^ii—Co2—K3—O3	−86.1 (3)	O5—Mo2—O7—K3^xiii	35.3 (7)
O3—Co2—K3—O7^v	168.0 (4)	O6—Mo2—O7—K3^xiii	−82.5 (6)
O8^i—Co2—K3—O7^v	−176.4 (3)	O8—Mo2—O7—K3^xiii	150.4 (5)
O12—Co2—K3—O7^v	85.9 (3)	K2^iii—Mo2—O7—K3^xiii	−18.8 (8)
O11^i—Co2—K3—O7^v	−87.3 (3)	K1^iii—Mo2—O7—K3^xiii	72.4 (6)
O11^v—Co2—K3—O7^v	−6.9 (4)	O5—Mo2—O8—Co2^xi	164.5 (4)
K3^ii—Co2—K3—O7^v	81.9 (3)	O6—Mo2—O8—Co2^xi	−78.2 (4)
O3—Co2—K3—O7^xii	135.8 (4)	O7—Mo2—O8—Co2^xi	48.7 (4)
O7^v—Co2—K3—O7^xii	−32.3 (4)	K2^iii—Mo2—O8—Co2^xi	−139.1 (3)
O8^i—Co2—K3—O7^xii	151.3 (4)	K1^iii—Mo2—O8—Co2^xi	135.6 (3)
O12—Co2—K3—O7^xii	53.6 (4)	O5—Mo2—O8—Co1^xi	22.4 (6)
O11^i—Co2—K3—O7^xii	−119.5 (4)	O6—Mo2—O8—Co1^xi	139.7 (5)
O11^v—Co2—K3—O7^xii	−39.2 (5)	O7—Mo2—O8—Co1^xi	−93.3 (6)
K3^ii—Co2—K3—O7^xii	49.6 (3)	K2^iii—Mo2—O8—Co1^xi	78.8 (5)
O3—Co2—K3—O3^ii	40.6 (4)	K1^iii—Mo2—O8—Co1^xi	−6.5 (5)
O7^v—Co2—K3—O3^ii	−127.5 (4)	O10—Mo3—O9—K2	−172.2 (4)
O8^i—Co2—K3—O3^ii	56.1 (4)	O11—Mo3—O9—K2	−52.4 (5)
O12—Co2—K3—O3^ii	−41.6 (4)	O12—Mo3—O9—K2	66.9 (5)
O11^i—Co2—K3—O3^ii	145.3 (3)	K3^ii—Mo3—O9—K2	130.1 (5)
O11^v—Co2—K3—O3^ii	−134.4 (3)	O10—Mo3—O9—K3^ii	57.7 (4)
K3^ii—Co2—K3—O3^ii	−45.6 (3)	O11—Mo3—O9—K3^ii	177.5 (3)
O3—Co2—K3—O9^ii	−82.7 (4)	O12—Mo3—O9—K3^ii	−63.2 (3)
O7^v—Co2—K3—O9^ii	109.2 (4)	K2—Mo3—O9—K3^ii	−130.1 (5)
O8^i—Co2—K3—O9^ii	−67.2 (4)	O10—Mo3—O9—K3^xi	−70.2 (4)
O12—Co2—K3—O9^ii	−164.9 (3)	O11—Mo3—O9—K3^xi	49.6 (4)
O11^i—Co2—K3—O9^ii	22.0 (3)	O12—Mo3—O9—K3^xi	168.9 (3)
O11^v—Co2—K3—O9^ii	102.3 (4)	K3^ii—Mo3—O9—K3^xi	−127.9 (4)
K3^ii—Co2—K3—O9^ii	−168.9 (3)	K2—Mo3—O9—K3^xi	102.0 (5)
O3—Co2—K3—O1^ii	−16.2 (3)	O1^x—K2—O9—Mo3	148.8 (5)
O7^v—Co2—K3—O1^ii	175.8 (4)	O4^xi—K2—O9—Mo3	83.0 (5)
O8^i—Co2—K3—O1^ii	−0.6 (4)	O2—K2—O9—Mo3	−56.7 (4)
O12—Co2—K3—O1^ii	−98.3 (3)	O5^iii—K2—O9—Mo3	−112.8 (4)
O11^i—Co2—K3—O1^ii	88.5 (3)	O3^xi—K2—O9—Mo3	78.9 (5)
O11^v—Co2—K3—O1^ii	168.9 (3)	O1—K2—O9—Mo3	−117.6 (5)
K3^ii—Co2—K3—O1^ii	−102.3 (2)	O6^iii—K2—O9—Mo3	−27.1 (8)
O3—Co2—K3—O9^i	−84.6 (3)	Mo1^xi—K2—O9—Mo3	84.1 (4)
O7^v—Co2—K3—O9^i	107.3 (3)	Mo1—K2—O9—Mo3	−87.0 (4)
O8^i—Co2—K3—O9^i	−69.1 (3)	Mo2^iii—K2—O9—Mo3	−80.4 (5)
O12—Co2—K3—O9^i	−166.7 (2)	O1^x—K2—O9—K3^ii	−88.3 (3)
O11^i—Co2—K3—O9^i	20.1 (2)	O4^xi—K2—O9—K3^ii	−154.1 (3)
O11^v—Co2—K3—O9^i	100.4 (3)	O2—K2—O9—K3^ii	66.2 (3)
K3^ii—Co2—K3—O9^i	−170.74 (16)	O5^iii—K2—O9—K3^ii	10.1 (4)
O3—Co2—K3—Co2^ii	87.8 (5)	O3^xi—K2—O9—K3^ii	−158.2 (3)
O7^v—Co2—K3—Co2^ii	−80.2 (4)	O1—K2—O9—K3^ii	5.3 (3)
O8^i—Co2—K3—Co2^ii	103.3 (4)	O6^iii—K2—O9—K3^ii	95.8 (5)
O12—Co2—K3—Co2^ii	5.7 (5)	Mo1^xi—K2—O9—K3^ii	−153.0 (2)
O11^i—Co2—K3—Co2^ii	−167.5 (4)	Mo1—K2—O9—K3^ii	35.9 (2)
O11^v—Co2—K3—Co2^ii	−87.2 (5)	Mo2^iii—K2—O9—K3^ii	42.5 (4)
K3^ii—Co2—K3—Co2^ii	1.7 (4)	Mo3—K2—O9—K3^ii	122.9 (6)
O3—Co2—K3—Mo1^ii	4.3 (3)	O1^x—K2—O9—K3^xi	32.6 (2)
O7^v—Co2—K3—Mo1^ii	−163.7 (4)	O4^xi—K2—O9—K3^xi	−33.1 (4)
O8^i—Co2—K3—Mo1^ii	19.8 (4)	O2—K2—O9—K3^xi	−172.8 (2)
O12—Co2—K3—Mo1^ii	−77.8 (3)	O5^iii—K2—O9—K3^xi	131.0 (3)
O11^i—Co2—K3—Mo1^ii	109.0 (3)	O3^xi—K2—O9—K3^xi	−37.22 (19)
O11^v—Co2—K3—Mo1^ii	−170.7 (3)	O1—K2—O9—K3^xi	126.3 (2)
K3^ii—Co2—K3—Mo1^ii	−81.8 (2)	O6^iii—K2—O9—K3^xi	−143.2 (4)
O3—Co2—K3—Mo3^ii	−109.4 (4)	Mo1^xi—K2—O9—K3^xi	−32.02 (19)
O7^v—Co2—K3—Mo3^ii	82.5 (4)	Mo1—K2—O9—K3^xi	156.9 (2)
O8^i—Co2—K3—Mo3^ii	−93.9 (4)	Mo2^iii—K2—O9—K3^xi	163.5 (2)
O12—Co2—K3—Mo3^ii	168.4 (3)	Mo3—K2—O9—K3^xi	−116.1 (5)
O11^i—Co2—K3—Mo3^ii	−4.7 (3)	O9—Mo3—O10—Co1^v	171.4 (4)
O11^v—Co2—K3—Mo3^ii	75.6 (4)	O11—Mo3—O10—Co1^v	56.3 (4)
K3^ii—Co2—K3—Mo3^ii	164.5 (3)	O12—Mo3—O10—Co1^v	−72.7 (4)
O2—Mo1—O1—K2^x	−113 (4)	K3^ii—Mo3—O10—Co1^v	−144.1 (4)
O4—Mo1—O1—K2^x	8 (4)	K2—Mo3—O10—Co1^v	163.64 (12)
O3—Mo1—O1—K2^x	127 (4)	O9—Mo3—O10—K1^xiv	26.7 (6)
K2^i—Mo1—O1—K2^x	66 (4)	O11—Mo3—O10—K1^xiv	−88.3 (6)
K2—Mo1—O1—K2^x	−108 (4)	O12—Mo3—O10—K1^xiv	142.6 (5)
K3^ii—Mo1—O1—K2^x	141 (4)	K3^ii—Mo3—O10—K1^xiv	71.2 (5)
K1—Mo1—O1—K2^x	7 (4)	K2—Mo3—O10—K1^xiv	18.9 (8)
K3—Mo1—O1—K2^x	120 (4)	O9—Mo3—O11—Co2^xi	−28.2 (6)
O2—Mo1—O1—K2	−5.6 (3)	O10—Mo3—O11—Co2^xi	87.0 (6)
O4—Mo1—O1—K2	116.0 (3)	O12—Mo3—O11—Co2^xi	−143.3 (5)
O3—Mo1—O1—K2	−125.3 (3)	K3^ii—Mo3—O11—Co2^xi	−22.6 (10)
K2^i—Mo1—O1—K2	173.34 (11)	K2—Mo3—O11—Co2^xi	−57.1 (5)
K3^ii—Mo1—O1—K2	−111.5 (3)	O9—Mo3—O11—Co2^v	−165.6 (3)
K1—Mo1—O1—K2	114.3 (2)	O10—Mo3—O11—Co2^v	−50.4 (4)
K3—Mo1—O1—K2	−132.5 (2)	O12—Mo3—O11—Co2^v	79.3 (4)
O2—Mo1—O1—K3^ii	105.9 (3)	K3^ii—Mo3—O11—Co2^v	−160.0 (4)
O4—Mo1—O1—K3^ii	−132.5 (3)	K2—Mo3—O11—Co2^v	165.4 (3)
O3—Mo1—O1—K3^ii	−13.8 (3)	O9—Mo3—O12—Co2	78.7 (5)
K2^i—Mo1—O1—K3^ii	−75.2 (2)	O10—Mo3—O12—Co2	−37.2 (6)
K2—Mo1—O1—K3^ii	111.5 (3)	O11—Mo3—O12—Co2	−166.4 (4)
K1—Mo1—O1—K3^ii	−134.2 (3)	K3^ii—Mo3—O12—Co2	31.9 (4)
K3—Mo1—O1—K3^ii	−21.01 (19)	K2—Mo3—O12—Co2	112.5 (4)
O9—K2—O1—Mo1	90.5 (3)	O9—Mo3—O12—Co1	−80.4 (5)
O1^x—K2—O1—Mo1	177.00 (12)	O10—Mo3—O12—Co1	163.7 (4)
O4^xi—K2—O1—Mo1	−122.0 (4)	O11—Mo3—O12—Co1	34.4 (5)
O2—K2—O1—Mo1	3.8 (2)	K3^ii—Mo3—O12—Co1	−127.2 (4)
O5^iii—K2—O1—Mo1	−85.0 (3)	K2—Mo3—O12—Co1	−46.7 (4)
O3^xi—K2—O1—Mo1	115.0 (3)	O3—Co2—O12—Mo3	−83.2 (5)
O6^iii—K2—O1—Mo1	−61.1 (3)	O7^v—Co2—O12—Mo3	15.1 (5)
Mo1^xi—K2—O1—Mo1	163.8 (3)	O8^i—Co2—O12—Mo3	−171.8 (5)
Mo2^iii—K2—O1—Mo1	−68.0 (2)	O11^i—Co2—O12—Mo3	122.8 (8)
Mo3—K2—O1—Mo1	71.3 (2)	O11^v—Co2—O12—Mo3	99.0 (5)
O9—K2—O1—K2^x	−94.7 (2)	K3—Co2—O12—Mo3	−35.1 (5)
O1^x—K2—O1—K2^x	−8.2 (3)	K3^ii—Co2—O12—Mo3	−33.3 (4)
O4^xi—K2—O1—K2^x	52.8 (5)	O3—Co2—O12—Co1	80.2 (3)
O2—K2—O1—K2^x	178.6 (3)	O7^v—Co2—O12—Co1	178.5 (3)
O5^iii—K2—O1—K2^x	89.7 (2)	O8^i—Co2—O12—Co1	−8.4 (3)
O3^xi—K2—O1—K2^x	−70.3 (4)	O11^i—Co2—O12—Co1	−73.8 (9)
O6^iii—K2—O1—K2^x	113.68 (19)	O11^v—Co2—O12—Co1	−97.6 (3)
Mo1^xi—K2—O1—K2^x	−21.4 (5)	K3—Co2—O12—Co1	128.3 (2)
Mo1—K2—O1—K2^x	174.7 (4)	K3^ii—Co2—O12—Co1	130.0 (2)
Mo2^iii—K2—O1—K2^x	106.75 (15)	O4^iv—Co1—O12—Mo3	−158.9 (18)
Mo3—K2—O1—K2^x	−114.00 (15)	O2—Co1—O12—Mo3	76.9 (4)
O9—K2—O1—K3^ii	−5.1 (2)	O6—Co1—O12—Mo3	−12.8 (5)
O1^x—K2—O1—K3^ii	81.4 (3)	O8^i—Co1—O12—Mo3	173.0 (4)
O4^xi—K2—O1—K3^ii	142.4 (4)	O10^v—Co1—O12—Mo3	−102.0 (4)
O2—K2—O1—K3^ii	−91.8 (3)	K1^iv—Co1—O12—Mo3	−112.5 (4)
O5^iii—K2—O1—K3^ii	179.3 (3)	K2^iii—Co1—O12—Mo3	−1.1 (6)
O3^xi—K2—O1—K3^ii	19.3 (4)	O4^iv—Co1—O12—Co2	36 (2)
O6^iii—K2—O1—K3^ii	−156.7 (2)	O2—Co1—O12—Co2	−87.9 (3)
Mo1^xi—K2—O1—K3^ii	68.2 (5)	O6—Co1—O12—Co2	−177.6 (3)
Mo1—K2—O1—K3^ii	−95.6 (3)	O8^i—Co1—O12—Co2	8.2 (3)
Mo2^iii—K2—O1—K3^ii	−163.6 (2)	O10^v—Co1—O12—Co2	93.2 (3)
Mo3—K2—O1—K3^ii	−24.4 (2)	K1^iv—Co1—O12—Co2	82.7 (3)
O1—Mo1—O2—Co1	−135.3 (5)	K2^iii—Co1—O12—Co2	−165.85 (13)
O4—Mo1—O2—Co1	102.9 (5)

Symmetry codes: (i) x+1, y, z; (ii) −x+1, y, −z+1/2; (iii) −x, −y+1, −z+1; (iv) −x+1, −y+1, −z+1; (v) −x+1/2, −y+3/2, −z+1; (vi) −x+1/2, y−1/2, −z+1/2; (vii) x+1/2, y−1/2, z; (viii) x+1, −y+1, z−1/2; (ix) x, −y+1, z−1/2; (x) −x, y, −z+1/2; (xi) x−1, y, z; (xii) x+1/2, −y+3/2, z−1/2; (xiii) x−1/2, −y+3/2, z+1/2; (xiv) x−1/2, y+1/2, z.

(II)

Crystal data

Co2K2Mo3O12	F(000) = 2512
Mr = 675.88	Dx = 4.754 Mg m^−3
Monoclinic, P21/c	Mo Kα radiation, λ = 0.71073 Å
a = 13.5237 (8) Å	Cell parameters from 4390 reflections
b = 7.6440 (4) Å	θ = 2.1–25.9°
c = 18.850 (1) Å	µ = 8.26 mm^−1
β = 104.260 (6)°	T = 298 K
V = 1888.58 (18) Å^3	Plate, purple
Z = 8	0.11 × 0.05 × 0.03 mm

Data collection

Oxford Diffraction Xcalibur (TM) Single Crystal X-ray Diffractometer with Sapphire CCD Detector.	791 reflections with I > 2σ(I)
Radiation source: Enhance (Mo) X-ray Source	Rint = 0.130
Graphite monochromator	θmax = 26.0°, θmin = 2.2°
Detector resolution: 8.4012 pixels mm^-1	h = −16→16
Rotation method data acquisition using ω and phi scans.	k = −3→2
7020 measured reflections	l = −20→22
1154 independent reflections

Refinement

Refinement on F^2	0 restraints
Least-squares matrix: full	Primary atom site location: structure-invariant direct methods
R[F^2 > 2σ(F^2)] = 0.047	Secondary atom site location: difference Fourier map
wR(F^2) = 0.110	w = 1/[σ^2(Fo^2) + (0.0538P)^2] where P = (Fo^2 + 2Fc^2)/3
S = 1.05	(Δ/σ)max < 0.001
1154 reflections	Δρmax = 1.07 e Å^−3
195 parameters	Δρmin = −0.89 e Å^−3

Special details

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F² against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F², conventional R-factors R are based on F, with F set to zero for negative F². The threshold expression of F² > σ(F²) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F² are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq
Mo1A	0.24962 (11)	0.3685 (7)	0.26601 (11)	0.010 (4)
Mo1B	0.25987 (11)	0.7825 (8)	0.24996 (10)	0.019 (4)
Mo2A	0.67270 (12)	0.7542 (7)	0.39151 (11)	0.011 (3)
Mo2B	0.12143 (11)	0.7131 (7)	0.40837 (10)	0.010 (3)
Mo3A	0.53078 (11)	0.2909 (7)	0.44848 (11)	0.014 (3)
Mo3B	0.04318 (11)	0.3513 (7)	0.45044 (10)	0.014 (3)
Co1A	0.41748 (18)	0.6830 (11)	0.38075 (16)	0.026 (5)
Co1B	0.10865 (17)	0.4358 (11)	0.65596 (16)	0.0133 (8)*
Co2A	0.28968 (17)	0.4449 (11)	0.44681 (17)	0.012 (5)
Co2B	0.22303 (18)	0.6460 (11)	0.57217 (17)	0.016 (5)
K1A	0.2852 (3)	0.023 (2)	0.4158 (3)	0.026 (10)
K1B	0.0983 (3)	0.0195 (19)	0.5872 (3)	0.017 (9)
K2A	0.4974 (3)	−0.0323 (19)	0.2553 (3)	0.025 (7)
K2B	0.0147 (3)	0.1841 (18)	0.2842 (3)	0.028 (9)
O1A	0.3390 (8)	0.231 (5)	0.2443 (8)	0.0161 (9)*
O1B	0.1707 (9)	0.587 (5)	0.2295 (8)	0.0161 (9)*
O2A	0.3453 (9)	0.553 (5)	0.2893 (8)	0.0161 (9)*
O2B	0.1599 (9)	0.929 (5)	0.2485 (8)	0.0161 (9)*
O3A	0.2327 (9)	0.307 (5)	0.3534 (7)	0.0161 (9)*
O3B	0.3064 (8)	0.803 (5)	0.1726 (8)	0.0161 (9)*
O4A	0.1366 (8)	0.287 (5)	0.2067 (8)	0.0161 (9)*
O4B	0.3588 (8)	0.879 (5)	0.3176 (8)	0.0161 (9)*
O5A	0.7007 (9)	0.964 (6)	0.3654 (8)	0.0161 (9)*
O5B	0.0577 (9)	0.875 (5)	0.3525 (8)	0.0161 (9)*
O6A	0.5470 (8)	0.689 (5)	0.3518 (7)	0.0161 (9)*
O6B	−0.0426 (9)	0.487 (5)	0.6401 (8)	0.0161 (9)*
O7A	0.6779 (8)	0.764 (5)	0.4848 (7)	0.0161 (9)*
O7B	0.1686 (8)	0.825 (5)	0.4936 (7)	0.0161 (9)*
O8A	0.7737 (9)	0.608 (5)	0.3860 (8)	0.0161 (9)*
O8B	0.2376 (9)	0.685 (5)	0.3822 (8)	0.0161 (9)*
O9A	0.5077 (9)	0.158 (5)	0.3755 (7)	0.0161 (9)*
O9B	0.0954 (9)	0.156 (5)	0.4392 (8)	0.0161 (9)*
O10A	0.5389 (9)	0.164 (5)	0.5276 (7)	0.0161 (9)*
O10B	0.0173 (8)	0.335 (5)	0.5413 (7)	0.0161 (9)*
O11A	0.6512 (8)	0.403 (5)	0.4600 (7)	0.0161 (9)*
O11B	0.1593 (8)	0.493 (5)	0.4795 (8)	0.0161 (9)*
O12A	0.4307 (8)	0.452 (5)	0.4344 (8)	0.0161 (9)*
O12B	−0.0886 (9)	0.321 (5)	0.3996 (8)	0.0161 (9)*

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
Mo1A	0.0114 (9)	0.008 (12)	0.0122 (13)	−0.0004 (16)	0.0048 (7)	0.000 (2)
Mo1B	0.0120 (9)	0.035 (12)	0.0108 (12)	−0.0010 (17)	0.0038 (7)	0.001 (2)
Mo2A	0.0121 (9)	0.007 (10)	0.0130 (12)	−0.0006 (17)	0.0032 (7)	0.003 (2)
Mo2B	0.0132 (9)	0.009 (10)	0.0085 (12)	−0.0008 (16)	0.0046 (7)	0.000 (2)
Mo3A	0.0105 (8)	0.020 (10)	0.0130 (12)	−0.0023 (16)	0.0030 (7)	0.001 (2)
Mo3B	0.0099 (9)	0.025 (11)	0.0085 (12)	−0.0001 (16)	0.0052 (7)	−0.002 (2)
Co1A	0.0137 (14)	0.057 (17)	0.0094 (18)	−0.003 (3)	0.0050 (11)	0.000 (4)
Co2A	0.0108 (13)	0.008 (16)	0.018 (2)	−0.001 (2)	0.0071 (11)	0.001 (4)
Co2B	0.0149 (14)	0.022 (17)	0.012 (2)	0.003 (2)	0.0075 (11)	0.005 (3)
K1A	0.033 (3)	0.02 (3)	0.024 (4)	0.001 (5)	0.013 (2)	−0.001 (7)
K1B	0.020 (2)	0.02 (3)	0.009 (3)	−0.015 (4)	0.0061 (18)	−0.001 (6)
K2A	0.019 (2)	0.04 (2)	0.022 (3)	0.002 (5)	0.0081 (18)	0.015 (6)
K2B	0.023 (2)	0.05 (3)	0.014 (3)	−0.001 (4)	0.0086 (19)	−0.011 (6)

Geometric parameters (Å, º)

Mo1A—O1A	1.73 (3)	K1A—O7A^v	2.44 (3)
Mo1A—O4A	1.769 (18)	K1A—O3A	2.49 (4)
Mo1A—O3A	1.781 (17)	K1A—O4B^xi	2.55 (2)
Mo1A—O2A	1.89 (3)	K1A—O8B^xi	2.69 (4)
Mo1A—O1B	2.01 (3)	K1A—O10A^vii	2.75 (2)
Mo1A—Mo1B	3.185 (7)	K1A—O7B^xi	2.84 (3)
Mo1A—K2B	3.568 (7)	K1A—O9B	2.90 (2)
Mo1A—K1B^i	3.589 (6)	K1A—O5B^xi	3.219 (19)
Mo1A—K2A^ii	3.622 (6)	K1A—Mo2B^xi	3.220 (12)
Mo1A—K1A	3.811 (12)	K1A—O2B^xi	3.270 (17)
Mo1B—O3B	1.731 (15)	K1A—Co1A^xi	3.310 (14)
Mo1B—O2B	1.75 (3)	K1B—O12B^viii	2.63 (4)
Mo1B—O4B	1.77 (2)	K1B—O4A^ix	2.64 (3)
Mo1B—O1B	1.90 (3)	K1B—O5A^v	2.646 (13)
Mo1B—O2A	2.13 (3)	K1B—O7B^xi	2.66 (3)
Mo1B—Co1A	2.934 (4)	K1B—O10B	2.70 (4)
Mo1B—K2A^iii	3.489 (8)	K1B—O1B^ix	2.74 (2)
Mo1B—K1A^iii	3.568 (10)	K1B—O5B^vi	2.753 (18)
Mo1B—K2B^iv	3.687 (5)	K1B—O9B^viii	2.88 (2)
Mo1B—K1B^i	4.027 (10)	K1B—O9B	2.97 (2)
Mo1B—K2A^ii	4.091 (10)	K1B—O8A^v	3.30 (4)
Mo2A—O5A	1.74 (4)	K1B—Co2B^xi	3.363 (15)
Mo2A—O7A	1.744 (14)	K1B—Mo3B^viii	3.396 (13)
Mo2A—O6A	1.752 (15)	K2A—O4B^xi	2.537 (17)
Mo2A—O8A	1.79 (3)	K2A—O2A^xii	2.556 (17)
Mo2A—K2A^iii	3.446 (9)	K2A—O6A^xii	2.59 (3)
Mo2A—K1B^v	3.483 (8)	K2A—O9A	2.67 (3)
Mo2A—K2A^ii	3.822 (10)	K2A—O6A^xi	2.77 (3)
Mo2A—K1A^v	3.925 (9)	K2A—O1A^xii	2.86 (3)
Mo2B—O5B	1.71 (3)	K2A—O1A	2.91 (3)
Mo2B—O8B	1.772 (14)	K2A—O3B^xi	2.95 (2)
Mo2B—O7B	1.79 (2)	K2A—O5A^xi	3.010 (13)
Mo2B—O6B^vi	1.96 (3)	K2A—O9A^xii	3.41 (3)
Mo2B—O11B	2.14 (3)	K2A—Mo2A^xi	3.446 (9)
Mo2B—O10B^vi	2.330 (14)	K2A—Co1A^xii	3.473 (9)
Mo2B—Co2A	3.015 (7)	K2B—O1B^xiii	2.567 (17)
Mo2B—Co2B	3.097 (4)	K2B—O4A	2.581 (19)
Mo2B—Mo3B	3.132 (7)	K2B—O5B^xi	2.69 (4)
Mo2B—K1A^iii	3.220 (12)	K2B—O9B	2.864 (15)
Mo2B—K1B^vi	3.625 (10)	K2B—O6B^vi	2.87 (4)
Mo2B—K2B^iv	3.651 (5)	K2B—O5B^xiii	2.91 (2)
Mo3A—O9A	1.68 (3)	K2B—O6B^i	2.94 (2)
Mo3A—O10A	1.76 (2)	K2B—O2B^xi	2.96 (3)
Mo3A—O12A	1.80 (3)	K2B—O2B^xiii	2.96 (3)
Mo3A—O11A	1.81 (2)	K2B—O12B	3.05 (2)
Mo3A—K1A	3.822 (10)	K2B—O3A	3.062 (17)
Mo3A—K1A^vii	3.917 (11)	K2B—Co1B^i	3.132 (7)
Mo3A—K2A^ii	4.000 (8)	O1A—K2A^ii	2.86 (3)
Mo3B—O9B	1.68 (4)	O1B—K2B^iv	2.567 (17)
Mo3B—O12B	1.818 (13)	O1B—K1B^i	2.742 (19)
Mo3B—O10B	1.835 (14)	O2A—K2A^ii	2.556 (17)
Mo3B—O11B	1.87 (3)	O2B—Co1B^xiv	2.00 (2)
Mo3B—O6B^vi	2.10 (3)	O2B—K2B^iii	2.96 (3)
Mo3B—Co1B^vi	2.976 (6)	O2B—K2B^iv	2.96 (3)
Mo3B—K2B	3.317 (7)	O2B—K1A^iii	3.270 (17)
Mo3B—K1B^viii	3.396 (13)	O3B—Co2B^xiv	1.989 (15)
Mo3B—K1B	3.562 (12)	O3B—K2A^iii	2.95 (2)
Co1A—O4B	1.96 (3)	O4A—Co1B^i	1.95 (4)
Co1A—O6A	1.960 (13)	O4A—K1B^i	2.64 (3)
Co1A—O12A	2.02 (3)	O4B—K2A^iii	2.537 (17)
Co1A—O2A	2.02 (2)	O4B—K1A^iii	2.55 (2)
Co1A—O10A^v	2.05 (2)	O5A—K1B^v	2.646 (13)
Co1A—Co2A	2.985 (8)	O5A—K2A^iii	3.010 (13)
Co1A—K1A^iii	3.310 (14)	O5B—K2B^iii	2.69 (4)
Co1A—K2A^ii	3.473 (9)	O5B—K1B^vi	2.753 (18)
Co1A—K2A^iii	3.571 (11)	O5B—K2B^iv	2.91 (2)
Co1B—O4A^ix	1.95 (4)	O5B—K1A^iii	3.219 (19)
Co1B—O8A^v	1.971 (15)	O6A—K2A^ii	2.59 (3)
Co1B—O2B^x	2.00 (2)	O6A—K2A^iii	2.77 (3)
Co1B—O6B	2.032 (14)	O6B—Mo2B^vi	1.96 (3)
Co1B—O12B^vi	2.11 (4)	O6B—Mo3B^vi	2.10 (3)
Co1B—O10B	2.342 (19)	O6B—K2B^vi	2.87 (4)
Co1B—Co2B	2.945 (7)	O6B—K2B^ix	2.94 (2)
Co1B—Mo3B^vi	2.976 (6)	O7A—Co2A^v	2.03 (3)
Co1B—K2B^ix	3.132 (7)	O7A—K1A^v	2.44 (3)
Co1B—K1B	3.426 (16)	O7B—K1B^iii	2.66 (3)
Co1B—K2B^vi	3.664 (13)	O7B—K1A^iii	2.84 (3)
Co2A—O12A	1.979 (12)	O8A—Co1B^v	1.971 (15)
Co2A—O7A^v	2.03 (3)	O8A—Co2B^v	2.09 (4)
Co2A—O3A	2.03 (2)	O8A—K1B^v	3.30 (4)
Co2A—O11B	2.039 (15)	O8B—K1A^iii	2.69 (4)
Co2A—O11A^v	2.09 (2)	O9A—K2A^ii	3.41 (3)
Co2A—O8B	2.22 (3)	O9B—K1B^viii	2.88 (2)
Co2A—K1A	3.278 (16)	O10A—Co1A^v	2.05 (2)
Co2B—O11A^v	1.977 (15)	O10A—K1A^vii	2.75 (2)
Co2B—O3B^x	1.989 (15)	O10B—Mo2B^vi	2.330 (14)
Co2B—O7B	2.02 (3)	O11A—Co2B^v	1.977 (15)
Co2B—O12B^vi	2.032 (14)	O11A—Co2A^v	2.09 (2)
Co2B—O8A^v	2.09 (4)	O12B—Co2B^vi	2.032 (14)
Co2B—O11B	2.10 (3)	O12B—Co1B^vi	2.11 (4)
Co2B—K1B^iii	3.363 (15)	O12B—K1B^viii	2.63 (4)
O1A—Mo1A—O4A	100.5 (12)	O11A^v—Co2B—Co1B	131.7 (11)
O1A—Mo1A—O3A	108.4 (12)	O3B^x—Co2B—Co1B	81.2 (7)
O4A—Mo1A—O3A	101.8 (9)	O7B—Co2B—Co1B	128.2 (4)
O1A—Mo1A—O2A	91.8 (12)	O12B^vi—Co2B—Co1B	45.9 (10)
O4A—Mo1A—O2A	147.5 (13)	O8A^v—Co2B—Co1B	42.0 (4)
O3A—Mo1A—O2A	102.6 (10)	O11B—Co2B—Co1B	88.8 (7)
O1A—Mo1A—O1B	140.3 (9)	O11A^v—Co2B—Mo2B	86.0 (4)
O4A—Mo1A—O1B	76.8 (13)	O3B^x—Co2B—Mo2B	157.6 (11)
O3A—Mo1A—O1B	111.0 (11)	O7B—Co2B—Mo2B	33.3 (9)
O2A—Mo1A—O1B	74.6 (11)	O12B^vi—Co2B—Mo2B	92.0 (4)
O1A—Mo1A—Mo1B	122.3 (10)	O8A^v—Co2B—Mo2B	119.5 (6)
O4A—Mo1A—Mo1B	109.8 (12)	O11B—Co2B—Mo2B	43.5 (10)
O3A—Mo1A—Mo1B	111.6 (12)	Co1B—Co2B—Mo2B	117.54 (15)
O2A—Mo1A—Mo1B	40.3 (8)	O11A^v—Co2B—K1B^iii	132.4 (11)
O1B—Mo1A—Mo1B	34.3 (7)	O3B^x—Co2B—K1B^iii	86.0 (10)
O1A—Mo1A—K2B	118.3 (10)	O7B—Co2B—K1B^iii	52.1 (7)
O4A—Mo1A—K2B	43.2 (5)	O12B^vi—Co2B—K1B^iii	51.3 (11)
O3A—Mo1A—K2B	59.1 (5)	O8A^v—Co2B—K1B^iii	136.1 (5)
O2A—Mo1A—K2B	147.9 (7)	O11B—Co2B—K1B^iii	115.6 (8)
O1B—Mo1A—K2B	87.2 (6)	Co1B—Co2B—K1B^iii	94.4 (2)
Mo1B—Mo1A—K2B	117.5 (2)	Mo2B—Co2B—K1B^iii	80.50 (18)
O1A—Mo1A—K1B^i	101.1 (5)	O7A^v—K1A—O3A	76.1 (10)
O4A—Mo1A—K1B^i	44.5 (10)	O7A^v—K1A—O4B^xi	143.1 (7)
O3A—Mo1A—K1B^i	139.3 (4)	O3A—K1A—O4B^xi	98.6 (9)
O2A—Mo1A—K1B^i	103.8 (7)	O7A^v—K1A—O8B^xi	144.3 (9)
O1B—Mo1A—K1B^i	49.3 (6)	O3A—K1A—O8B^xi	134.4 (6)
Mo1B—Mo1A—K1B^i	72.7 (2)	O4B^xi—K1A—O8B^xi	62.1 (8)
K2B—Mo1A—K1B^i	82.50 (16)	O7A^v—K1A—O10A^vii	93.1 (8)
O1A—Mo1A—K2A^ii	50.7 (10)	O3A—K1A—O10A^vii	138.9 (8)
O4A—Mo1A—K2A^ii	134.1 (5)	O4B^xi—K1A—O10A^vii	66.7 (6)
O3A—Mo1A—K2A^ii	119.9 (4)	O8B^xi—K1A—O10A^vii	74.3 (9)
O2A—Mo1A—K2A^ii	42.1 (7)	O7A^v—K1A—O7B^xi	89.7 (9)
O1B—Mo1A—K2A^ii	102.9 (6)	O3A—K1A—O7B^xi	125.3 (7)
Mo1B—Mo1A—K2A^ii	73.6 (2)	O4B^xi—K1A—O7B^xi	120.7 (12)
K2B—Mo1A—K2A^ii	168.8 (3)	O8B^xi—K1A—O7B^xi	58.8 (8)
K1B^i—Mo1A—K2A^ii	100.46 (16)	O10A^vii—K1A—O7B^xi	93.5 (8)
O1A—Mo1A—K1A	77.6 (8)	O7A^v—K1A—O9B	70.6 (6)
O4A—Mo1A—K1A	99.0 (11)	O3A—K1A—O9B	66.6 (7)
O3A—Mo1A—K1A	32.2 (11)	O4B^xi—K1A—O9B	141.3 (5)
O2A—Mo1A—K1A	113.0 (7)	O8B^xi—K1A—O9B	101.8 (8)
O1B—Mo1A—K1A	142.2 (4)	O10A^vii—K1A—O9B	146.9 (6)
Mo1B—Mo1A—K1A	139.38 (19)	O7B^xi—K1A—O9B	58.9 (9)
K2B—Mo1A—K1A	66.90 (18)	O7A^v—K1A—O5B^xi	121.0 (6)
K1B^i—Mo1A—K1A	143.1 (3)	O3A—K1A—O5B^xi	89.8 (8)
K2A^ii—Mo1A—K1A	106.09 (19)	O4B^xi—K1A—O5B^xi	95.0 (6)
O3B—Mo1B—O2B	111.6 (11)	O8B^xi—K1A—O5B^xi	54.9 (7)
O3B—Mo1B—O4B	101.7 (8)	O10A^vii—K1A—O5B^xi	128.1 (11)
O2B—Mo1B—O4B	100.8 (12)	O7B^xi—K1A—O5B^xi	53.3 (5)
O3B—Mo1B—O1B	104.0 (11)	O9B—K1A—O5B^xi	51.6 (8)
O2B—Mo1B—O1B	93.0 (11)	O7A^v—K1A—Mo2B^xi	122.2 (5)
O4B—Mo1B—O1B	143.7 (12)	O3A—K1A—Mo2B^xi	120.5 (4)
O3B—Mo1B—O2A	95.0 (11)	O4B^xi—K1A—Mo2B^xi	92.3 (8)
O2B—Mo1B—O2A	152.0 (9)	O8B^xi—K1A—Mo2B^xi	33.4 (3)
O4B—Mo1B—O2A	81.0 (12)	O10A^vii—K1A—Mo2B^xi	99.0 (8)
O1B—Mo1B—O2A	71.7 (10)	O7B^xi—K1A—Mo2B^xi	33.7 (5)
O3B—Mo1B—Co1A	113.0 (5)	O9B—K1A—Mo2B^xi	68.9 (7)
O2B—Mo1B—Co1A	125.3 (5)	O5B^xi—K1A—Mo2B^xi	30.8 (6)
O4B—Mo1B—Co1A	40.4 (11)	O7A^v—K1A—O2B^xi	147.7 (10)
O1B—Mo1B—Co1A	105.1 (7)	O3A—K1A—O2B^xi	73.4 (9)
O2A—Mo1B—Co1A	43.5 (6)	O4B^xi—K1A—O2B^xi	53.8 (4)
O3B—Mo1B—Mo1A	101.6 (13)	O8B^xi—K1A—O2B^xi	61.8 (8)
O2B—Mo1B—Mo1A	125.9 (10)	O10A^vii—K1A—O2B^xi	117.0 (8)
O4B—Mo1B—Mo1A	113.0 (12)	O7B^xi—K1A—O2B^xi	99.2 (6)
O1B—Mo1B—Mo1A	36.6 (8)	O9B—K1A—O2B^xi	87.5 (5)
O2A—Mo1B—Mo1A	35.1 (7)	O5B^xi—K1A—O2B^xi	49.1 (4)
Co1A—Mo1B—Mo1A	72.69 (19)	Mo2B^xi—K1A—O2B^xi	67.1 (5)
O3B—Mo1B—K2A^iii	57.7 (6)	O7A^v—K1A—Co2A	38.2 (7)
O2B—Mo1B—K2A^iii	116.2 (10)	O3A—K1A—Co2A	38.3 (6)
O4B—Mo1B—K2A^iii	44.1 (5)	O4B^xi—K1A—Co2A	123.9 (9)
O1B—Mo1B—K2A^iii	149.2 (8)	O8B^xi—K1A—Co2A	167.6 (4)
O2A—Mo1B—K2A^iii	84.7 (6)	O10A^vii—K1A—Co2A	117.7 (7)
Co1A—Mo1B—K2A^iii	66.91 (17)	O7B^xi—K1A—Co2A	114.8 (8)
Mo1A—Mo1B—K2A^iii	117.5 (2)	O9B—K1A—Co2A	66.6 (8)
O3B—Mo1B—K1A^iii	135.7 (11)	O5B^xi—K1A—Co2A	112.7 (7)
O2B—Mo1B—K1A^iii	65.9 (6)	Mo2B^xi—K1A—Co2A	135.5 (2)
O4B—Mo1B—K1A^iii	42.3 (6)	O2B^xi—K1A—Co2A	111.6 (7)
O1B—Mo1B—K1A^iii	120.1 (5)	O7A^v—K1A—Co1A^xi	131.2 (5)
O2A—Mo1B—K1A^iii	101.1 (6)	O3A—K1A—Co1A^xi	134.1 (4)
Co1A—Mo1B—K1A^iii	60.3 (2)	O4B^xi—K1A—Co1A^xi	36.2 (7)
Mo1A—Mo1B—K1A^iii	115.1 (2)	O8B^xi—K1A—Co1A^xi	46.6 (4)
K2A^iii—Mo1B—K1A^iii	82.94 (19)	O10A^vii—K1A—Co1A^xi	38.1 (6)
O3B—Mo1B—K2B^iv	115.5 (4)	O7B^xi—K1A—Co1A^xi	94.7 (8)
O2B—Mo1B—K2B^iv	52.3 (10)	O9B—K1A—Co1A^xi	148.2 (9)
O4B—Mo1B—K2B^iv	139.7 (5)	O5B^xi—K1A—Co1A^xi	99.5 (7)
O1B—Mo1B—K2B^iv	40.7 (8)	Mo2B^xi—K1A—Co1A^xi	79.3 (4)
O2A—Mo1B—K2B^iv	109.2 (7)	O2B^xi—K1A—Co1A^xi	79.3 (6)
Co1A—Mo1B—K2B^iv	125.87 (18)	Co2A—K1A—Co1A^xi	145.1 (2)
Mo1A—Mo1B—K2B^iv	75.4 (2)	O12B^viii—K1B—O4A^ix	118.6 (8)
K2A^iii—Mo1B—K2B^iv	165.5 (3)	O12B^viii—K1B—O5A^v	95.0 (10)
K1A^iii—Mo1B—K2B^iv	97.66 (16)	O4A^ix—K1B—O5A^v	73.5 (7)
O3B—Mo1B—K1B^i	69.6 (9)	O12B^viii—K1B—O7B^xi	62.7 (9)
O2B—Mo1B—K1B^i	94.8 (8)	O4A^ix—K1B—O7B^xi	148.7 (4)
O4B—Mo1B—K1B^i	164.2 (9)	O5A^v—K1B—O7B^xi	75.3 (7)
O1B—Mo1B—K1B^i	36.5 (5)	O12B^viii—K1B—O10B	153.0 (6)
O2A—Mo1B—K1B^i	86.5 (7)	O4A^ix—K1B—O10B	75.7 (9)
Co1A—Mo1B—K1B^i	129.6 (3)	O5A^v—K1B—O10B	111.5 (11)
Mo1A—Mo1B—K1B^i	58.30 (19)	O7B^xi—K1B—O10B	118.0 (8)
K2A^iii—Mo1B—K1B^i	125.27 (16)	O12B^viii—K1B—O1B^ix	68.0 (9)
K1A^iii—Mo1B—K1B^i	151.58 (12)	O4A^ix—K1B—O1B^ix	51.9 (10)
K2B^iv—Mo1B—K1B^i	54.25 (16)	O5A^v—K1B—O1B^ix	66.1 (6)
O3B—Mo1B—K2A^ii	64.7 (9)	O7B^xi—K1B—O1B^ix	112.5 (9)
O2B—Mo1B—K2A^ii	175.6 (9)	O10B—K1B—O1B^ix	126.7 (9)
O4B—Mo1B—K2A^ii	78.1 (9)	O12B^viii—K1B—O5B^vi	101.0 (9)
O1B—Mo1B—K2A^ii	90.3 (8)	O4A^ix—K1B—O5B^vi	59.4 (5)
O2A—Mo1B—K2A^ii	32.3 (4)	O5A^v—K1B—O5B^vi	132.4 (7)
Co1A—Mo1B—K2A^ii	56.41 (14)	O7B^xi—K1B—O5B^vi	151.0 (8)
Mo1A—Mo1B—K2A^ii	58.12 (18)	O10B—K1B—O5B^vi	65.1 (8)
K2A^iii—Mo1B—K2A^ii	60.05 (6)	O1B^ix—K1B—O5B^vi	79.0 (6)
K1A^iii—Mo1B—K2A^ii	114.79 (16)	O12B^viii—K1B—O9B^viii	59.2 (8)
K2B^iv—Mo1B—K2A^ii	131.0 (3)	O4A^ix—K1B—O9B^viii	112.9 (6)
K1B^i—Mo1B—K2A^ii	86.12 (19)	O5A^v—K1B—O9B^viii	153.8 (12)
O5A—Mo2A—O7A	106.7 (14)	O7B^xi—K1B—O9B^viii	94.7 (8)
O5A—Mo2A—O6A	113.3 (11)	O10B—K1B—O9B^viii	94.6 (9)
O7A—Mo2A—O6A	103.7 (7)	O1B^ix—K1B—O9B^viii	97.0 (7)
O5A—Mo2A—O8A	109.6 (12)	O5B^vi—K1B—O9B^viii	56.7 (9)
O7A—Mo2A—O8A	104.1 (10)	O12B^viii—K1B—O9B	116.7 (9)
O6A—Mo2A—O8A	118.2 (14)	O4A^ix—K1B—O9B	124.0 (11)
O5A—Mo2A—K2A^iii	60.8 (5)	O5A^v—K1B—O9B	94.3 (6)
O7A—Mo2A—K2A^iii	125.5 (9)	O7B^xi—K1B—O9B	59.8 (10)
O6A—Mo2A—K2A^iii	53.0 (10)	O10B—K1B—O9B	58.3 (7)
O8A—Mo2A—K2A^iii	130.4 (5)	O1B^ix—K1B—O9B	160.4 (4)
O5A—Mo2A—K1B^v	47.7 (5)	O5B^vi—K1B—O9B	116.8 (8)
O7A—Mo2A—K1B^v	92.8 (7)	O9B^viii—K1B—O9B	101.6 (6)
O6A—Mo2A—K1B^v	158.7 (9)	O12B^viii—K1B—O8A^v	151.3 (5)
O8A—Mo2A—K1B^v	69.3 (10)	O4A^ix—K1B—O8A^v	53.2 (7)
K2A^iii—Mo2A—K1B^v	106.2 (3)	O5A^v—K1B—O8A^v	56.7 (10)
O5A—Mo2A—K2A^ii	117.1 (5)	O7B^xi—K1B—O8A^v	108.9 (7)
O7A—Mo2A—K2A^ii	128.4 (10)	O10B—K1B—O8A^v	55.7 (7)
O6A—Mo2A—K2A^ii	35.0 (8)	O1B^ix—K1B—O8A^v	93.4 (8)
O8A—Mo2A—K2A^ii	86.1 (8)	O5B^vi—K1B—O8A^v	96.3 (9)
K2A^iii—Mo2A—K2A^ii	63.32 (5)	O9B^viii—K1B—O8A^v	148.1 (9)
K1B^v—Mo2A—K2A^ii	136.67 (15)	O9B—K1B—O8A^v	74.1 (7)
O5A—Mo2A—K1A^v	82.5 (7)	O12B^viii—K1B—Co2B^xi	37.1 (3)
O7A—Mo2A—K1A^v	24.2 (13)	O4A^ix—K1B—Co2B^xi	123.4 (6)
O6A—Mo2A—K1A^v	115.0 (6)	O5A^v—K1B—Co2B^xi	64.9 (9)
O8A—Mo2A—K1A^v	112.8 (5)	O7B^xi—K1B—Co2B^xi	36.8 (6)
K2A^iii—Mo2A—K1A^v	113.6 (3)	O10B—K1B—Co2B^xi	154.6 (4)
K1B^v—Mo2A—K1A^v	75.84 (17)	O1B^ix—K1B—Co2B^xi	76.4 (7)
K2A^ii—Mo2A—K1A^v	147.47 (14)	O5B^vi—K1B—Co2B^xi	137.3 (9)
O5B—Mo2B—O8B	105.1 (11)	O9B^viii—K1B—Co2B^xi	92.5 (8)
O5B—Mo2B—O7B	102.8 (14)	O9B—K1B—Co2B^xi	96.4 (7)
O8B—Mo2B—O7B	99.3 (8)	O8A^v—K1B—Co2B^xi	119.3 (4)
O5B—Mo2B—O6B^vi	98.2 (10)	O12B^viii—K1B—Mo3B^viii	32.0 (3)
O8B—Mo2B—O6B^vi	101.2 (12)	O4A^ix—K1B—Mo3B^viii	128.9 (6)
O7B—Mo2B—O6B^vi	145.5 (11)	O5A^v—K1B—Mo3B^viii	126.2 (10)
O5B—Mo2B—O11B	164.2 (7)	O7B^xi—K1B—Mo3B^viii	70.7 (7)
O8B—Mo2B—O11B	89.4 (11)	O10B—K1B—Mo3B^viii	121.0 (5)
O7B—Mo2B—O11B	80.6 (11)	O1B^ix—K1B—Mo3B^viii	90.2 (8)
O6B^vi—Mo2B—O11B	72.2 (10)	O5B^vi—K1B—Mo3B^viii	83.2 (8)
O5B—Mo2B—O10B^vi	91.7 (9)	O9B^viii—K1B—Mo3B^viii	29.7 (7)
O8B—Mo2B—O10B^vi	162.4 (14)	O9B—K1B—Mo3B^viii	102.8 (6)
O7B—Mo2B—O10B^vi	81.6 (7)	O8A^v—K1B—Mo3B^viii	176.2 (4)
O6B^vi—Mo2B—O10B^vi	70.6 (9)	Co2B^xi—K1B—Mo3B^viii	62.8 (3)
O11B—Mo2B—O10B^vi	73.4 (8)	O4B^xi—K2A—O2A^xii	171.7 (5)
O5B—Mo2B—Co2A	150.9 (5)	O4B^xi—K2A—O6A^xii	118.6 (7)
O8B—Mo2B—Co2A	47.0 (11)	O2A^xii—K2A—O6A^xii	68.2 (7)
O7B—Mo2B—Co2A	91.6 (9)	O4B^xi—K2A—O9A	69.0 (8)
O6B^vi—Mo2B—Co2A	82.7 (8)	O2A^xii—K2A—O9A	105.5 (8)
O11B—Mo2B—Co2A	42.5 (4)	O6A^xii—K2A—O9A	105.0 (11)
O10B^vi—Mo2B—Co2A	115.6 (8)	O4B^xi—K2A—O6A^xi	65.1 (7)
O5B—Mo2B—Co2B	139.9 (9)	O2A^xii—K2A—O6A^xi	108.9 (8)
O8B—Mo2B—Co2B	93.0 (5)	O6A^xii—K2A—O6A^xi	170.3 (11)
O7B—Mo2B—Co2B	38.1 (12)	O9A—K2A—O6A^xi	84.7 (8)
O6B^vi—Mo2B—Co2B	113.1 (7)	O4B^xi—K2A—O1A^xii	119.3 (10)
O11B—Mo2B—Co2B	42.7 (7)	O2A^xii—K2A—O1A^xii	57.0 (10)
O10B^vi—Mo2B—Co2B	76.8 (3)	O6A^xii—K2A—O1A^xii	116.6 (6)
Co2A—Mo2B—Co2B	61.62 (14)	O9A—K2A—O1A^xii	117.7 (5)
O5B—Mo2B—Mo3B	130.0 (8)	O6A^xi—K2A—O1A^xii	56.6 (6)
O8B—Mo2B—Mo3B	110.1 (12)	O4B^xi—K2A—O1A	66.5 (9)
O7B—Mo2B—Mo3B	105.2 (11)	O2A^xii—K2A—O1A	117.3 (11)
O6B^vi—Mo2B—Mo3B	41.3 (7)	O6A^xii—K2A—O1A	57.8 (6)
O11B—Mo2B—Mo3B	35.7 (5)	O9A—K2A—O1A	64.3 (6)
O10B^vi—Mo2B—Mo3B	53.3 (10)	O6A^xi—K2A—O1A	129.2 (5)
Co2A—Mo2B—Mo3B	67.72 (16)	O1A^xii—K2A—O1A	174.1 (9)
Co2B—Mo2B—Mo3B	72.30 (16)	O4B^xi—K2A—O3B^xi	58.7 (5)
O5B—Mo2B—K1A^iii	74.5 (9)	O2A^xii—K2A—O3B^xi	128.8 (6)
O8B—Mo2B—K1A^iii	56.8 (12)	O6A^xii—K2A—O3B^xi	82.1 (8)
O7B—Mo2B—K1A^iii	61.4 (8)	O9A—K2A—O3B^xi	122.5 (5)
O6B^vi—Mo2B—K1A^iii	152.1 (5)	O6A^xi—K2A—O3B^xi	93.3 (8)
O11B—Mo2B—K1A^iii	119.8 (6)	O1A^xii—K2A—O3B^xi	107.9 (9)
O10B^vi—Mo2B—K1A^iii	135.3 (9)	O1A—K2A—O3B^xi	74.0 (8)
Co2A—Mo2B—K1A^iii	91.1 (2)	O4B^xi—K2A—O5A^xi	109.4 (5)
Co2B—Mo2B—K1A^iii	86.95 (18)	O2A^xii—K2A—O5A^xi	62.4 (5)
Mo3B—Mo2B—K1A^iii	155.41 (18)	O6A^xii—K2A—O5A^xi	122.8 (9)
O5B—Mo2B—K1B^vi	46.9 (5)	O9A—K2A—O5A^xi	64.7 (6)
O8B—Mo2B—K1B^vi	149.5 (12)	O6A^xi—K2A—O5A^xi	60.5 (8)
O7B—Mo2B—K1B^vi	79.8 (7)	O1A^xii—K2A—O5A^xi	54.3 (8)
O6B^vi—Mo2B—K1B^vi	95.5 (7)	O1A—K2A—O5A^xi	126.0 (9)
O11B—Mo2B—K1B^vi	120.1 (4)	O3B^xi—K2A—O5A^xi	153.1 (12)
O10B^vi—Mo2B—K1B^vi	48.1 (9)	O4B^xi—K2A—O9A^xii	105.3 (9)
Co2A—Mo2B—K1B^vi	162.22 (18)	O2A^xii—K2A—O9A^xii	79.0 (8)
Co2B—Mo2B—K1B^vi	103.61 (14)	O6A^xii—K2A—O9A^xii	86.1 (7)
Mo3B—Mo2B—K1B^vi	99.3 (2)	O9A—K2A—O9A^xii	168.9 (12)
K1A^iii—Mo2B—K1B^vi	98.3 (3)	O6A^xi—K2A—O9A^xii	84.2 (9)
O5B—Mo2B—K2B^iv	51.5 (10)	O1A^xii—K2A—O9A^xii	55.9 (5)
O8B—Mo2B—K2B^iv	88.9 (4)	O1A—K2A—O9A^xii	123.1 (5)
O7B—Mo2B—K2B^iv	154.3 (12)	O3B^xi—K2A—O9A^xii	57.4 (5)
O6B^vi—Mo2B—K2B^iv	53.5 (7)	O5A^xi—K2A—O9A^xii	110.1 (7)
O11B—Mo2B—K2B^iv	124.1 (8)	O4B^xi—K2A—Mo2A^xi	88.8 (5)
O10B^vi—Mo2B—K2B^iv	97.8 (3)	O2A^xii—K2A—Mo2A^xi	83.7 (5)
Co2A—Mo2B—K2B^iv	111.3 (2)	O6A^xii—K2A—Mo2A^xi	151.1 (4)
Co2B—Mo2B—K2B^iv	166.5 (3)	O9A—K2A—Mo2A^xi	75.1 (6)
Mo3B—Mo2B—K2B^iv	94.5 (2)	O6A^xi—K2A—Mo2A^xi	30.3 (4)
K1A^iii—Mo2B—K2B^iv	105.1 (2)	O1A^xii—K2A—Mo2A^xi	46.2 (3)
K1B^vi—Mo2B—K2B^iv	80.88 (17)	O1A—K2A—Mo2A^xi	137.7 (4)
O9A—Mo3A—O10A	108.7 (15)	O3B^xi—K2A—Mo2A^xi	122.9 (8)
O9A—Mo3A—O12A	108.2 (10)	O5A^xi—K2A—Mo2A^xi	30.4 (8)
O10A—Mo3A—O12A	113.0 (10)	O9A^xii—K2A—Mo2A^xi	95.6 (5)
O9A—Mo3A—O11A	111.5 (9)	O4B^xi—K2A—Co1A^xii	152.3 (6)
O10A—Mo3A—O11A	107.1 (8)	O2A^xii—K2A—Co1A^xii	35.2 (5)
O12A—Mo3A—O11A	108.4 (14)	O6A^xii—K2A—Co1A^xii	33.9 (3)
O9A—Mo3A—K1A	64.1 (6)	O9A—K2A—Co1A^xii	114.3 (8)
O10A—Mo3A—K1A	73.2 (6)	O6A^xi—K2A—Co1A^xii	141.0 (4)
O12A—Mo3A—K1A	75.6 (10)	O1A^xii—K2A—Co1A^xii	84.6 (5)
O11A—Mo3A—K1A	175.1 (10)	O1A—K2A—Co1A^xii	89.5 (5)
O9A—Mo3A—K1A^vii	97.2 (10)	O3B^xi—K2A—Co1A^xii	102.6 (4)
O10A—Mo3A—K1A^vii	38.0 (5)	O5A^xi—K2A—Co1A^xii	95.8 (5)
O12A—Mo3A—K1A^vii	148.0 (5)	O9A^xii—K2A—Co1A^xii	75.3 (5)
O11A—Mo3A—K1A^vii	78.7 (9)	Mo2A^xi—K2A—Co1A^xii	118.83 (14)
K1A—Mo3A—K1A^vii	99.43 (14)	O1B^xiii—K2B—O4A	140.9 (5)
O9A—Mo3A—K2A^ii	57.5 (11)	O1B^xiii—K2B—O5B^xi	83.4 (9)
O10A—Mo3A—K2A^ii	166.2 (11)	O4A—K2B—O5B^xi	116.6 (9)
O12A—Mo3A—K2A^ii	74.7 (5)	O1B^xiii—K2B—O9B	101.4 (5)
O11A—Mo3A—K2A^ii	79.9 (5)	O4A—K2B—O9B	117.7 (5)
K1A—Mo3A—K2A^ii	98.81 (16)	O5B^xi—K2B—O9B	57.5 (9)
K1A^vii—Mo3A—K2A^ii	136.77 (16)	O1B^xiii—K2B—O6B^vi	108.0 (8)
O9B—Mo3B—O12B	102.1 (14)	O4A—K2B—O6B^vi	89.4 (10)
O9B—Mo3B—O10B	103.7 (13)	O5B^xi—K2B—O6B^vi	123.1 (6)
O12B—Mo3B—O10B	95.5 (6)	O9B—K2B—O6B^vi	65.6 (9)
O9B—Mo3B—O11B	101.5 (12)	O1B^xiii—K2B—O5B^xiii	87.0 (6)
O12B—Mo3B—O11B	150.3 (16)	O4A—K2B—O5B^xiii	57.9 (5)
O10B—Mo3B—O11B	96.1 (9)	O5B^xi—K2B—O5B^xiii	148.2 (12)
O9B—Mo3B—O6B^vi	109.6 (11)	O9B—K2B—O5B^xiii	154.2 (12)
O12B—Mo3B—O6B^vi	80.7 (10)	O6B^vi—K2B—O5B^xiii	88.6 (10)
O10B—Mo3B—O6B^vi	146.6 (14)	O1B^xiii—K2B—O6B^i	75.5 (6)
O11B—Mo3B—O6B^vi	74.6 (9)	O4A—K2B—O6B^i	70.9 (8)
O9B—Mo3B—Co1B^vi	129.8 (5)	O5B^xi—K2B—O6B^i	91.5 (10)
O12B—Mo3B—Co1B^vi	44.7 (12)	O9B—K2B—O6B^i	148.9 (11)
O10B—Mo3B—Co1B^vi	114.1 (7)	O6B^vi—K2B—O6B^i	145.2 (12)
O11B—Mo3B—Co1B^vi	105.8 (10)	O5B^xiii—K2B—O6B^i	56.7 (8)
O6B^vi—Mo3B—Co1B^vi	43.0 (4)	O1B^xiii—K2B—O2B^xi	118.3 (12)
O9B—Mo3B—Mo2B	124.8 (8)	O4A—K2B—O2B^xi	61.3 (9)
O12B—Mo3B—Mo2B	109.0 (12)	O5B^xi—K2B—O2B^xi	56.8 (6)
O10B—Mo3B—Mo2B	116.9 (12)	O9B—K2B—O2B^xi	94.4 (7)
O11B—Mo3B—Mo2B	41.7 (9)	O6B^vi—K2B—O2B^xi	132.6 (5)
O6B^vi—Mo3B—Mo2B	37.9 (8)	O5B^xiii—K2B—O2B^xi	103.0 (6)
Co1B^vi—Mo3B—Mo2B	64.32 (15)	O6B^i—K2B—O2B^xi	62.3 (5)
O9B—Mo3B—K2B	59.7 (5)	O1B^xiii—K2B—O2B^xiii	56.8 (9)
O12B—Mo3B—K2B	65.3 (6)	O4A—K2B—O2B^xiii	106.1 (9)
O10B—Mo3B—K2B	148.2 (11)	O5B^xi—K2B—O2B^xiii	136.4 (6)
O11B—Mo3B—K2B	113.1 (5)	O9B—K2B—O2B^xiii	110.1 (7)
O6B^vi—Mo3B—K2B	58.9 (9)	O6B^vi—K2B—O2B^xiii	63.2 (7)
Co1B^vi—Mo3B—K2B	71.0 (2)	O5B^xiii—K2B—O2B^xiii	54.7 (5)
Mo2B—Mo3B—K2B	93.9 (2)	O6B^i—K2B—O2B^xiii	94.3 (7)
O9B—Mo3B—K1B^viii	57.8 (7)	O2B^xi—K2B—O2B^xiii	155.5 (2)
O12B—Mo3B—K1B^viii	49.9 (12)	O1B^xiii—K2B—O12B	64.1 (7)
O10B—Mo3B—K1B^viii	84.8 (10)	O4A—K2B—O12B	140.2 (12)
O11B—Mo3B—K1B^viii	158.6 (11)	O5B^xi—K2B—O12B	92.6 (8)
O6B^vi—Mo3B—K1B^viii	115.5 (8)	O9B—K2B—O12B	54.8 (5)
Co1B^vi—Mo3B—K1B^viii	93.2 (2)	O6B^vi—K2B—O12B	51.0 (8)
Mo2B—Mo3B—K1B^viii	153.16 (13)	O5B^xiii—K2B—O12B	110.2 (8)
K2B—Mo3B—K1B^viii	63.4 (2)	O6B^i—K2B—O12B	138.5 (4)
O9B—Mo3B—K1B	56.0 (6)	O2B^xi—K2B—O12B	146.7 (7)
O12B—Mo3B—K1B	107.2 (11)	O2B^xiii—K2B—O12B	56.4 (5)
O10B—Mo3B—K1B	47.8 (11)	O1B^xiii—K2B—O3A	161.0 (5)
O11B—Mo3B—K1B	100.8 (8)	O4A—K2B—O3A	57.7 (4)
O6B^vi—Mo3B—K1B	164.3 (7)	O5B^xi—K2B—O3A	89.7 (7)
Co1B^vi—Mo3B—K1B	149.74 (13)	O9B—K2B—O3A	60.2 (5)
Mo2B—Mo3B—K1B	142.04 (15)	O6B^vi—K2B—O3A	61.6 (7)
K2B—Mo3B—K1B	111.4 (3)	O5B^xiii—K2B—O3A	107.6 (7)
K1B^viii—Mo3B—K1B	64.12 (15)	O6B^i—K2B—O3A	122.5 (5)
O4B—Co1A—O6A	93.9 (10)	O2B^xi—K2B—O3A	71.1 (8)
O4B—Co1A—O12A	161.2 (8)	O2B^xiii—K2B—O3A	122.0 (10)
O6A—Co1A—O12A	100.7 (11)	O12B—K2B—O3A	98.8 (6)
O4B—Co1A—O2A	79.6 (11)	O1B^xiii—K2B—Co1B^i	114.2 (6)
O6A—Co1A—O2A	92.9 (7)	O4A—K2B—Co1B^i	38.3 (8)
O12A—Co1A—O2A	87.8 (12)	O5B^xi—K2B—Co1B^i	91.8 (5)
O4B—Co1A—O10A^v	93.7 (12)	O9B—K2B—Co1B^i	129.8 (5)
O6A—Co1A—O10A^v	97.5 (8)	O6B^vi—K2B—Co1B^i	127.7 (5)
O12A—Co1A—O10A^v	96.1 (10)	O5B^xiii—K2B—Co1B^i	64.9 (5)
O2A—Co1A—O10A^v	168.0 (8)	O6B^i—K2B—Co1B^i	38.9 (3)
O4B—Co1A—Mo1B	35.8 (8)	O2B^xi—K2B—Co1B^i	38.1 (4)
O6A—Co1A—Mo1B	105.9 (5)	O2B^xiii—K2B—Co1B^i	118.6 (4)
O12A—Co1A—Mo1B	127.1 (6)	O12B—K2B—Co1B^i	175.1 (6)
O2A—Co1A—Mo1B	46.6 (10)	O3A—K2B—Co1B^i	83.6 (4)
O10A^v—Co1A—Mo1B	124.0 (8)	Mo1A—O1A—K2A^ii	101.5 (16)
O4B—Co1A—Co2A	122.1 (5)	Mo1A—O1A—K2A	162.0 (9)
O6A—Co1A—Co2A	141.3 (11)	K2A^ii—O1A—K2A	83.2 (3)
O12A—Co1A—Co2A	41.2 (4)	Mo1B—O1B—Mo1A	109.1 (6)
O2A—Co1A—Co2A	81.3 (7)	Mo1B—O1B—K2B^iv	110.4 (16)
O10A^v—Co1A—Co2A	94.2 (7)	Mo1A—O1B—K2B^iv	134.2 (14)
Mo1B—Co1A—Co2A	97.65 (13)	Mo1B—O1B—K1B^i	119.3 (10)
O4B—Co1A—K1A^iii	50.4 (6)	Mo1A—O1B—K1B^i	96.9 (13)
O6A—Co1A—K1A^iii	126.9 (11)	K2B^iv—O1B—K1B^i	83.3 (4)
O12A—Co1A—K1A^iii	124.8 (6)	Mo1A—O2A—Co1A	136.4 (10)
O2A—Co1A—K1A^iii	112.6 (8)	Mo1A—O2A—Mo1B	104.6 (6)
O10A^v—Co1A—K1A^iii	56.0 (7)	Co1A—O2A—Mo1B	89.9 (15)
Mo1B—Co1A—K1A^iii	69.40 (17)	Mo1A—O2A—K2A^ii	108.1 (15)
Co2A—Co1A—K1A^iii	89.9 (2)	Co1A—O2A—K2A^ii	98.0 (5)
O4B—Co1A—K2A^ii	94.2 (7)	Mo1B—O2A—K2A^ii	121.3 (11)
O6A—Co1A—K2A^ii	47.5 (8)	Mo1B—O2B—Co1B^xiv	116.4 (8)
O12A—Co1A—K2A^ii	87.2 (7)	Mo1B—O2B—K2B^iii	166.1 (7)
O2A—Co1A—K2A^ii	46.8 (4)	Co1B^xiv—O2B—K2B^iii	75.6 (9)
O10A^v—Co1A—K2A^ii	144.5 (4)	Mo1B—O2B—K2B^iv	99.8 (15)
Mo1B—Co1A—K2A^ii	78.86 (15)	Co1B^xiv—O2B—K2B^iv	93.3 (6)
Co2A—Co1A—K2A^ii	110.5 (3)	K2B^iii—O2B—K2B^iv	85.6 (3)
K1A^iii—Co1A—K2A^ii	144.4 (3)	Mo1B—O2B—K1A^iii	84.8 (5)
O4B—Co1A—K2A^iii	43.4 (4)	Co1B^xiv—O2B—K1A^iii	135.7 (16)
O6A—Co1A—K2A^iii	50.5 (9)	K2B^iii—O2B—K1A^iii	81.5 (6)
O12A—Co1A—K2A^iii	149.3 (6)	K2B^iv—O2B—K1A^iii	122.4 (7)
O2A—Co1A—K2A^iii	84.0 (8)	Mo1A—O3A—Co2A	123.8 (17)
O10A^v—Co1A—K2A^iii	98.0 (8)	Mo1A—O3A—K1A	125.5 (14)
Mo1B—Co1A—K2A^iii	63.99 (14)	Co2A—O3A—K1A	92.3 (7)
Co2A—Co1A—K2A^iii	161.53 (13)	Mo1A—O3A—K2B	91.0 (5)
K1A^iii—Co1A—K2A^iii	85.5 (3)	Co2A—O3A—K2B	130.4 (7)
K2A^ii—Co1A—K2A^iii	65.82 (6)	K1A—O3A—K2B	93.8 (10)
O4A^ix—Co1B—O8A^v	88.3 (11)	Mo1B—O3B—Co2B^xiv	125.5 (7)
O4A^ix—Co1B—O2B^x	92.3 (11)	Mo1B—O3B—K2A^iii	92.6 (7)
O8A^v—Co1B—O2B^x	107.3 (8)	Co2B^xiv—O3B—K2A^iii	129.4 (13)
O4A^ix—Co1B—O6B	108.0 (11)	Mo1A—O4A—Co1B^i	130.6 (16)
O8A^v—Co1B—O6B	148.9 (6)	Mo1A—O4A—K2B	108.8 (7)
O2B^x—Co1B—O6B	98.6 (9)	Co1B^i—O4A—K2B	86.4 (12)
O4A^ix—Co1B—O12B^vi	176.2 (5)	Mo1A—O4A—K1B^i	107.5 (14)
O8A^v—Co1B—O12B^vi	88.2 (11)	Co1B^i—O4A—K1B^i	95.6 (6)
O2B^x—Co1B—O12B^vi	87.4 (12)	K2B—O4A—K1B^i	129.5 (7)
O6B—Co1B—O12B^vi	75.9 (11)	Mo1B—O4B—Co1A	103.9 (19)
O4A^ix—Co1B—O10B	99.1 (12)	Mo1B—O4B—K2A^iii	107.0 (7)
O8A^v—Co1B—O10B	82.4 (6)	Co1A—O4B—K2A^iii	104.5 (7)
O2B^x—Co1B—O10B	165.4 (11)	Mo1B—O4B—K1A^iii	110.0 (6)
O6B—Co1B—O10B	69.2 (7)	Co1A—O4B—K1A^iii	93.5 (6)
O12B^vi—Co1B—O10B	81.9 (11)	K2A^iii—O4B—K1A^iii	133.3 (15)
O4A^ix—Co1B—Co2B	132.7 (4)	Mo2A—O5A—K1B^v	103.1 (12)
O8A^v—Co1B—Co2B	45.2 (11)	Mo2A—O5A—K2A^iii	88.8 (8)
O2B^x—Co1B—Co2B	94.1 (8)	K1B^v—O5A—K2A^iii	156.9 (7)
O6B—Co1B—Co2B	117.3 (9)	Mo2B—O5B—K2B^iii	161.2 (12)
O12B^vi—Co1B—Co2B	43.6 (4)	Mo2B—O5B—K1B^vi	106.2 (8)
O10B—Co1B—Co2B	85.0 (6)	K2B^iii—O5B—K1B^vi	80.9 (9)
O4A^ix—Co1B—Mo3B^vi	145.9 (6)	Mo2B—O5B—K2B^iv	101.1 (15)
O8A^v—Co1B—Mo3B^vi	108.3 (7)	K2B^iii—O5B—K2B^iv	91.8 (5)
O2B^x—Co1B—Mo3B^vi	109.9 (9)	K1B^vi—O5B—K2B^iv	112.8 (5)
O6B—Co1B—Mo3B^vi	45.0 (7)	Mo2B—O5B—K1A^iii	74.6 (5)
O12B^vi—Co1B—Mo3B^vi	37.2 (4)	K2B^iii—O5B—K1A^iii	86.7 (9)
O10B—Co1B—Mo3B^vi	55.9 (9)	K1B^vi—O5B—K1A^iii	120.2 (10)
Co2B—Co1B—Mo3B^vi	72.94 (17)	K2B^iv—O5B—K1A^iii	125.9 (5)
O4A^ix—Co1B—K2B^ix	55.3 (5)	Mo2A—O6A—Co1A	136.7 (10)
O8A^v—Co1B—K2B^ix	141.3 (9)	Mo2A—O6A—K2A^ii	122.2 (10)
O2B^x—Co1B—K2B^ix	66.2 (7)	Co1A—O6A—K2A^ii	98.6 (9)
O6B—Co1B—K2B^ix	65.5 (6)	Mo2A—O6A—K2A^iii	96.6 (13)
O12B^vi—Co1B—K2B^ix	127.7 (6)	Co1A—O6A—K2A^iii	96.5 (9)
O10B—Co1B—K2B^ix	113.2 (6)	K2A^ii—O6A—K2A^iii	91.1 (4)
Co2B—Co1B—K2B^ix	160.1 (3)	Mo2B^vi—O6B—Co1B	109.3 (16)
Mo3B^vi—Co1B—K2B^ix	109.67 (17)	Mo2B^vi—O6B—Mo3B^vi	100.8 (6)
O4A^ix—Co1B—K1B	50.0 (7)	Co1B—O6B—Mo3B^vi	92.0 (7)
O8A^v—Co1B—K1B	69.6 (11)	Mo2B^vi—O6B—K2B^vi	155.1 (8)
O2B^x—Co1B—K1B	141.5 (10)	Co1B—O6B—K2B^vi	95.3 (10)
O6B—Co1B—K1B	100.3 (11)	Mo3B^vi—O6B—K2B^vi	82.1 (13)
O12B^vi—Co1B—K1B	129.7 (6)	Mo2B^vi—O6B—K2B^ix	94.1 (13)
O10B—Co1B—K1B	51.7 (9)	Co1B—O6B—K2B^ix	75.6 (7)
Co2B—Co1B—K1B	106.4 (2)	Mo3B^vi—O6B—K2B^ix	163.1 (10)
Mo3B^vi—Co1B—K1B	107.20 (17)	K2B^vi—O6B—K2B^ix	87.6 (5)
K2B^ix—Co1B—K1B	91.9 (3)	Mo2A—O7A—Co2A^v	123.8 (19)
O4A^ix—Co1B—K2B^vi	126.3 (6)	Mo2A—O7A—K1A^v	138.7 (19)
O8A^v—Co1B—K2B^vi	137.1 (12)	Co2A^v—O7A—K1A^v	93.8 (6)
O2B^x—Co1B—K2B^vi	53.7 (7)	Mo2B—O7B—Co2B	109 (2)
O6B—Co1B—K2B^vi	51.2 (10)	Mo2B—O7B—K1B^iii	139.1 (6)
O12B^vi—Co1B—K2B^vi	56.2 (6)	Co2B—O7B—K1B^iii	91.0 (6)
O10B—Co1B—K2B^vi	111.7 (7)	Mo2B—O7B—K1A^iii	84.9 (6)
Co2B—Co1B—K2B^vi	94.1 (3)	Co2B—O7B—K1A^iii	126.2 (5)
Mo3B^vi—Co1B—K2B^vi	58.87 (16)	K1B^iii—O7B—K1A^iii	112.4 (14)
K2B^ix—Co1B—K2B^vi	72.10 (15)	Mo2A—O8A—Co1B^v	146.5 (19)
K1B—Co1B—K2B^vi	150.90 (17)	Mo2A—O8A—Co2B^v	120.2 (10)
O12A—Co2A—O7A^v	91.9 (10)	Co1B^v—O8A—Co2B^v	92.8 (14)
O12A—Co2A—O3A	94.7 (8)	Mo2A—O8A—K1B^v	80.3 (13)
O7A^v—Co2A—O3A	96.9 (12)	Co1B^v—O8A—K1B^v	76.4 (9)
O12A—Co2A—O11B	164.0 (14)	Co2B^v—O8A—K1B^v	141.3 (6)
O7A^v—Co2A—O11B	90.9 (11)	Mo2B—O8B—Co2A	97.4 (11)
O3A—Co2A—O11B	100.5 (8)	Mo2B—O8B—K1A^iii	89.9 (13)
O12A—Co2A—O11A^v	84.5 (8)	Co2A—O8B—K1A^iii	129.6 (6)
O7A^v—Co2A—O11A^v	85.7 (10)	Mo3A—O9A—K2A	171.0 (10)
O3A—Co2A—O11A^v	177.4 (13)	Mo3A—O9A—K2A^ii	98.0 (15)
O11B—Co2A—O11A^v	80.0 (8)	K2A—O9A—K2A^ii	77.1 (4)
O12A—Co2A—O8B	95.5 (10)	Mo3B—O9B—K2B	89.8 (9)
O7A^v—Co2A—O8B	171.2 (7)	Mo3B—O9B—K1B^viii	92.5 (6)
O3A—Co2A—O8B	87.3 (10)	K2B—O9B—K1B^viii	75.9 (4)
O11B—Co2A—O8B	80.6 (11)	Mo3B—O9B—K1A	138.3 (15)
O11A^v—Co2A—O8B	90.3 (11)	K2B—O9B—K1A	90.0 (5)
O12A—Co2A—Co1A	42.2 (10)	K1B^viii—O9B—K1A	127.7 (14)
O7A^v—Co2A—Co1A	133.4 (4)	Mo3B—O9B—K1B	95.9 (7)
O3A—Co2A—Co1A	95.1 (7)	K2B—O9B—K1B	153.9 (10)
O11B—Co2A—Co1A	130.5 (12)	K1B^viii—O9B—K1B	78.4 (6)
O11A^v—Co2A—Co1A	82.6 (7)	K1A—O9B—K1B	102.2 (8)
O8B—Co2A—Co1A	53.5 (4)	Mo3A—O10A—Co1A^v	110.1 (18)
O12A—Co2A—Mo2B	130.2 (11)	Mo3A—O10A—K1A^vii	118.8 (6)
O7A^v—Co2A—Mo2B	136.0 (4)	Co1A^v—O10A—K1A^vii	85.8 (5)
O3A—Co2A—Mo2B	92.4 (7)	Mo3B—O10B—Mo2B^vi	138.5 (7)
O11B—Co2A—Mo2B	45.1 (9)	Mo3B—O10B—Co1B	131.3 (11)
O11A^v—Co2A—Mo2B	86.2 (7)	Mo2B^vi—O10B—Co1B	88.3 (5)
O8B—Co2A—Mo2B	35.6 (3)	Mo3B—O10B—K1B	101.9 (12)
Co1A—Co2A—Mo2B	88.0 (2)	Mo2B^vi—O10B—K1B	92.0 (11)
O12A—Co2A—K1A	89.0 (11)	Co1B—O10B—K1B	85.3 (7)
O7A^v—Co2A—K1A	48.0 (8)	Mo3A—O11A—Co2B^v	133.7 (18)
O3A—Co2A—K1A	49.4 (9)	Mo3A—O11A—Co2A^v	120.7 (7)
O11B—Co2A—K1A	104.5 (12)	Co2B^v—O11A—Co2A^v	100.5 (7)
O11A^v—Co2A—K1A	133.0 (9)	Mo3B—O11B—Co2A	122.3 (17)
O8B—Co2A—K1A	136.7 (7)	Mo3B—O11B—Co2B	135.0 (7)
Co1A—Co2A—K1A	120.9 (2)	Co2A—O11B—Co2B	98.2 (7)
Mo2B—Co2A—K1A	130.31 (17)	Mo3B—O11B—Mo2B	102.5 (7)
O11A^v—Co2B—O3B^x	90.0 (6)	Co2A—O11B—Mo2B	92.4 (9)
O11A^v—Co2B—O7B	95.2 (9)	Co2B—O11B—Mo2B	93.8 (16)
O3B^x—Co2B—O7B	125.7 (14)	Mo3A—O12A—Co2A	132.4 (19)
O11A^v—Co2B—O12B^vi	175.2 (14)	Mo3A—O12A—Co1A	130.0 (9)
O3B^x—Co2B—O12B^vi	93.4 (6)	Co2A—O12A—Co1A	96.6 (11)
O7B—Co2B—O12B^vi	85.5 (9)	Mo3B—O12B—Co2B^vi	132.1 (10)
O11A^v—Co2B—O8A^v	90.0 (11)	Mo3B—O12B—Co1B^vi	98.1 (15)
O3B^x—Co2B—O8A^v	82.5 (12)	Co2B^vi—O12B—Co1B^vi	90.5 (12)
O7B—Co2B—O8A^v	151.2 (10)	Mo3B—O12B—K1B^viii	98.0 (13)
O12B^vi—Co2B—O8A^v	87.2 (12)	Co2B^vi—O12B—K1B^viii	91.6 (12)
O11A^v—Co2B—O11B	81.2 (8)	Co1B^vi—O12B—K1B^viii	156.2 (9)
O3B^x—Co2B—O11B	156.9 (14)	Mo3B—O12B—K2B	81.8 (5)
O7B—Co2B—O11B	76.6 (10)	Co2B^vi—O12B—K2B	145.8 (9)
O12B^vi—Co2B—O11B	94.3 (8)	Co1B^vi—O12B—K2B	88.5 (6)
O8A^v—Co2B—O11B	76.2 (11)	K1B^viii—O12B—K2B	76.6 (9)

Symmetry codes: (i) x, −y+1/2, z−1/2; (ii) −x+1, y+1/2, −z+1/2; (iii) x, y+1, z; (iv) −x, y+1/2, −z+1/2; (v) −x+1, −y+1, −z+1; (vi) −x, −y+1, −z+1; (vii) −x+1, −y, −z+1; (viii) −x, −y, −z+1; (ix) x, −y+1/2, z+1/2; (x) x, −y+3/2, z+1/2; (xi) x, y−1, z; (xii) −x+1, y−1/2, −z+1/2; (xiii) −x, y−1/2, −z+1/2; (xiv) x, −y+3/2, z−1/2.