Figure 3
Bragg intensity decay and further indicators for radiation damage as a function of dose. (a) Changes of the mean I/σ(I) ratios for I > 2σ(I) in the 0.7–0.8 Å resolution shell. (b) Mean Bragg intensity per data set (resolution range 0.7–15.65 Å). (c) Changes of the correlation coefficients between the first and the following data sets. (d) Changes of the R1 values (R1 = Σ||Fo| − |Fc||/Σ|Fo|) from the structure refinement with SHELXL runs as a function of dose. |