Figure 4
Morphology of matrix and inclusions. (a) Integrated regular SAXS patterns at two locations on the sample. (b) Integrated µSAXS pattern of the matrix only. Five orders of scattering from the lamellar structure can be discerned. (c) Integrated µSAXS pattern of the inclusions with the matrix subtracted. (d) µSAXS azimuthal scans radially integrated over the (10) reflection (top curve) as well as for the (11) and (20) reflections (bottom curve). The angular spacing between peaks of 60° and 30° clearly shows that this scattering signal is due to a hexagonal single-crystalline domain. The top curve was offset by 1500 for clarity. Note that the bottom curve was multiplied by a factor of 100. |