Figure 1
(a) General scheme of the solid–liquid reaction cell. (b) Section along the principal solvent channel: 1, thermometer position; 2, reflux system position; 3, powder holder position; 4, powder sample position; 5, liquid channel. (c) Real image of the cell during the experiment (the large CCD detector can be observed in the left part of the image). (d) Cross section of the cell. |