X-ray spectroscopy for chemistry in the 2-4 keV energy regime at the XMaS beamline: ionic liquids, Rh and Pd catalysts in gas and liquid environments, and Cl contamination in γ-Al2O3

Thompson, P.B.J.; Nguyen, B.N.; Nicholls, R.; Bourne, R.A.; Brazier, J.B.; Lovelock, K.R.J.; Brown, S.D.; Wermeille, D.; Bikondoa, O.; Lucas, C.A.; Hase, T.P.A.; Newton, M.A.

doi:10.1107/S1600577515016148

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Figure 11
(a) Rh L₃-edge XANES and (b) the first derivatives, from the adsorbed monomer species [(O)Rh^I(CO)₂Cl⁻ blue], a sample reduced to 623 K (red), and that obtained from post-reduction room-temperature exposure to CO (black).

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 22| Part 6| October 2015| Pages 1426-1439

doi:10.1107/S1600577515016148

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