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Figure 9
Temperature dependence of Cl K- and Rh L3-edge XANES derived from in-vacuum MOCVD of [RhI(CO)2Cl]2 to γ-Al2O3. At each temperature the sample has been exposed to ca. 1 × 10−2 mbar H2 for 1 min. (a) Complete spectra; (b) Cl K-edge XANES; (c) Rh L3-edge XANES.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 22| Part 6| October 2015| Pages 1426-1439
doi:10.1107/S1600577515016148
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