Figure 9
X-ray absorption spectra using the 15 mM solution with (i-pr Ni) from `quick' scans. The uncertainty was determined from the variance of three independent scans, and including the variance of dark-current measurements made for the hybrid transmission XAS under the same experimental conditions. The quick transmission XAS for (i-pr Ni) was affected by detector gain change producing a linear offset, which was scaled with the hybrid transmission XAS determined with the same solution indicated by the red diamond markers. |